FREEZE DRYER LYOPHILIZER PRODUCTS LABFREEZ INSTRUMENTS CO., LTD

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1 FREEZE DRYER LYOPHILIZER PRODUCTS LABFREEZ INSTRUMENTS CO., LTD Addr1: 2D, Building 3, Century City Chenyue Park, Haidian district BeiJing, China Addr2: No.72 Renmin road, Yuhu district, Xiangtan city, Hunan province, China Phone: , Fax:

2 CONTENT FD-10 Series Desktop Freeze Dryer... 2 FD-12 Series Vertical Freeze Dryer... 5 FD-18 Series Vertical Freeze Dryer... 7 FD-18S Vertical Freeze Dryer Shelf Heating... 9 FD-18S Automatic In-situ Freeze Dryer FD-10F Series (-70 C) Electric-heating Freeze Dryer FD-30F Series Electric-heating Freeze Dryer FD-30F Series Automatic Freeze Dryer FD-50F Series In-Situ Freeze Dryer FD-100F Series Silicone oil-heating freeze dryer FD-200F Auto Silicone Oil-heating Freeze Dryer FD-P Series Production Freeze Dryer (Customization)

3 Company Profile LABFREEZ was established in 1996, as a professional technology enterprise specialized in manufacturer & OEM the technical instruments and equipment for the life sciences and laboratory refrigeration fields. Our company has an excellent research and development team which marvelously applies the leading technologies to designing, developing and producing Ultra-low temperature freezer, Freeze dryer, ice maker and chillers products. Our products are specifically designed for and welcomed by Scientific Research Institutes, Medical and Health, Aviation & Military, Biological Pharmacy, College Research Institutes of Electronics, Metal Process, Electronic Industry, Chemical Industry, Offshore Fishing Industry and Food processing. Our company has acquired certificates of ISO9001, CE, CMD and the products have been welcomed all over the world, such as USA, Australia, Russia, Singapore, Malaysia, Turkey and India, etc. With high performance-price ratio and our fast response service team have earned approval and praise both from the domestic and international markets. -1-

4 Certificate -1-

5 FD-10 Series Desktop Freeze Dryer Description: FD-10 Freezing Dryer is applicable for freeze-drying test of laboratory samples and suitable for small amount of production. Characteristics: Microprocessor controls; Environment-friendly, conform to international standard (CE, ISO); Communication interface & LCD display include drying curve, vacuum, condenser temp., run time, ambient temperature; With pre-freezing for samples, widely open condenser, without inner coil; Large refrigerating capacity and slight noise of Danfoss compressor; The pre-cooling shelf can be used as draft tube to accelerate drying speed; Condenser and the operation panel are made of 304 stainless steel, which is corrosion-resistant and easy to clean; Transparent bell-cap drying kiln is safe and easy to observe; Stainless steel sample shelf, the space among common sample tray can be adjusted; Novel design, small size and simple operation; For water based samples, the -55 C condenser is the perfect choice with effective cost. For samples containing solvents or with low eutectic points, the -80 C condenser provides maximum performance

6 For labs that needs quick turn-around, electric heating defrost is optional. Nitrogen inflation valve is optional. It includes the following types: Regular type, Top-press type, multi-manifold T type and multi-manifold Top-press type to meet the various requirements. Built - in heat exchanger Green compound refrigerant Oilless vacuum pump Danfoss compressor DSC-5 Controller is very convenient LCD display drying curve with English & Chinese language Parameters: Order Id FD-10-TP FD-10-R FD-10-MT FD-10-MTP FD-10-MR Top-press Description samples in vials can be stoppered under Regular 24 ports column manifold T type 8 ports manifold Top-press 8 ports manifold Regular vacuum Freeze Dry Area 0.08 M M M M M 2 Cold Trap Temp. <-55 C <-55 C <-55 C / -80 C (optional) Vacuum Degree <10 Pa Water Capture Capability 3-4 Kg/24h 3 Kg/24h 3-4 Kg/24h Material Tray φ180*3mm φ200*4m m φ180*3mm φ200*4mm Power 970W - 3 -

7 Dimensions Material Capacity Exiling Bottle φ12mm 565*420*( )mm 0.7L 1.2L 1.2L 560 Pcs 920 Pcs Exiling Bottle φ16mm 285 Pcs 480 Pcs Exiling Bottle φ22mm 165 Pcs 260 Pcs Notice: The temperature of cold trap may reach -80 Caccording to the user s needs. Configuration: Order Id FD-10-TP FD-10-R FD-10-MT FD-10-MTP FD-10-MR Freeze Dryer Synthetic glass Anti oil back vacuum pump Gland device Freeze-dryed flask - 4 -

8 FD-12 Series Vertical Freeze Dryer Description: FD-12 Freezing Dryer is applicable for freeze-drying test of laboratory samples and suitable for small amount of production. Characteristics: Microprocessor controls; Environment-friendly, conform to international standard (CE, ISO); Communication interface & liquid crystal display include drying curve, vacuum, condenser temp., run time, ambient temperature; With pre-freezing for samples, widely open condenser, without inner coil; Large refrigerating capacity and slight noise of Danfoss compressor; The pre-cooling shelf can be used as draft tube to accelerate drying speed; Condenser and the operation panel are made of 304 stainless steel, which is corrosion-resistant and easy to clean; - 5 -

9 Transparent bell-cap drying kiln is safe and easy to observe; Stainless steel sample shelf, the space among common sample tray can be adjusted; Novel design, small size and simple operation; For water based samples, the -55 C condenser is the perfect choice with effective cost. For samples containing solvents or with low eutectic points, the -80 C condenser provides maximum performance. For labs that needs quick turn-around, electric heating defrost is optional. Nitrogen inflation valve is optional. FD-12 series include the following types: Regular type, Top-press type, multi-manifold Regular type and multi-manifold Top-press type to meet the various requirements. Parameters: Order Id FD-12-TP FD-12-R FD-12-MR FD-12-MTP Type Top-press Regular Multi-manifold Multi-manifold Regular Top-press Freeze Dry Area 0.08 M M M 2 Cold Trap Temp. <-55 C <-55 C /-80 C (optional) Vacuum Degree <10 Pa Water Capture Capability 3-4 Kg/24h 3 Kg/24h Material Tray φ180*3mm φ200*4mm Φ200*3/Φ200*6/Φ200*4(optional)mm Power 1070 W Dimensions 565*460*( )mm Material Capacity 0.7L 1.2L Exiling Bottle φ12mm 560 Pcs 920 Pcs Exiling Bottle φ16mm 285 Pcs 480 Pcs Exiling Bottle φ22mm 165 Pcs 260 Pcs Notice: The temperature of cold trap may reach -80 C according to the user s needs. Configuration: Order Id FD-12-TP FD-12-R FD-12-MR FD-12-MTP Freeze Dryer Synthetic glass Anti oil back vacuum pump Gland device 8 pcs Freeze-dryed flask - 6 -

10 FD-18 Series Vertical Freeze Dryer Description: FD-18 Freezing Dryer is applicable for freeze-drying test of laboratory samples and suitable for small amount of production. Characteristics: Microprocessor controls; Environment-friendly, conform to international standard (CE, ISO); Communication interface & liquid crystal display include drying curve, vacuum, condenser temp., run time, ambient temperature; With pre-freezing for samples, widely open condenser, without inner coil; Large refrigerating capacity and slight noise of Danfoss compressor; The pre-cooling shelf can be used as draft tube to accelerate drying speed; - 7 -

11 Characteristics: Condenser and the operation panel are made of 304 stainless steel, which is corrosion-resistant and easy to clean; Cold trap and the operation panel are made of stainless steel, which is corrosion-resistant and easy to clean; Transparent bell-cap drying kiln is safe and intuitive; Stainless steel sample shelf, the space among common sample tray can be adjusted; Novel design, small size and simple operation; Nitrogen-charging valve can be added. FD-18 series include the following types: Regular type, Top-press type, multi-manifold Regular type and multi-manifold Top-press type to meet the various requirements. Parameters: Order Id FD-18-TP FD-18-R FD-18-MR FD-18-MTP Type Top-press Regular multi-manifold Regular Freeze Dry Area 0.12 M M M 2 multi-manifold Top-press Cold Trap Temp. <-55 ºC <-55 ºC /-80 ºC (optional) Vacuum Degree Water Capture Capability <10 Pa 6 Kg/24h 6 Kg/24h Material Tray Φ200*3mm φ240*4mm Φ240*3/Φ240*6/Φ240*4(optional)mm Power Dimensions 1400W 635*540*( )mm Material Capacity 0.9 L 1.8 L L Exiling Bottle φ12mm Exiling Bottle φ16mm Exiling Bottle φ22mm 990 Pcs 1320 Pcs Pcs 740 Pcs Pcs 360 Pcs - Notice: The temperature of cold trap may reach -80 Caccording to the user s needs. Configuration: Order Id FD-18-TP FD-18-R FD-18-MR FD-18-MTP Freeze Dryer Synthetic glass Anti oil back vacuum pump Gland device 8 pcs Freeze-dryed flask - 8 -

12 FD-18S Vertical Freeze Dryer Shelf Heating Description: FD-18S freezing dryer is small vertical freeze-drying equipment with heating shelf and programmable function. This instrument is suitable for freeze-dryer experiment in laboratory and a small amount production. Characteristics: Can stored 32 program, each program can be set up 36segments, correct program data in computing, memorize the drying curve. The touch-screen display function keys, o operation keys, so reduce the wrong operation, improve the reliability and stability of the instrument Communication interface & LCD display include drying curve, vacuum, condenser temp., run time, ambient temperature; Microprocessor controls; Environment-friendly, conform to international standard (CE, ISO); With pre-freezing for samples, widely open condenser, without inner coil; Large refrigerating capacity and slight noise of Danfoss compressor; The pre-cooling shelf can be used as draft tube to accelerate drying speed; Condenser and the operation panel are made of 304 stainless steel, which is corrosion-resistant and easy to clean; Transparent bell-cap drying kiln is safe and easy to observe; Stainless steel sample shelf, the space among common sample tray can be adjusted; Novel design, small size and simple operation; For water based samples, the -55 C condenser is the perfect choice with effective cost. For samples containing solvents or with low eutectic points, the -80 C condenser provides maximum performance. For labs that needs quick turn-around, electric heating defrost is optional. Nitrogen inflation valve is optional. FD-18s series include the following types: Regular type, Top-press type, multi-manifold Regular type and multi-manifold Top-press type to meet the various requirements

13 Technical indices: Order Id FD-18S-R FD-18S-TP FD-18S-MR FD-18S-MTP Type Regular Top-press multi-manifold multi-manifold Regular Top-press Temp. of cold trap coil <-60 C or -80 C(optical) Partition board temperature C Vacuum <10 Pa Freeze-dry area M 2 Water-capture capability 6 Kg/24h Φ240mm 4 Specifications of layers, space Φ200mm, material tray is 70mm(bulk 3layers Φ240mm 4 layers Φ200mm 3 layers material) Power 1600 W Dimension 640*540*( ) mm Notice: The temperature of cold trap may reach -80 Caccording to the user s needs. Configuration: Order Id FD-18S-TP FD-18S-R FD-18S-MR FD-18S-MTP Freeze Dryer Synthetic glass Anti oil back vacuum pump Gland device 8 pcs Freeze-dryed flask

14 FD-18S Automatic In-situ Freeze Dryer Description: FD-18S freezing dryer is small vertical freeze-drying equipment with heating shelf and programmable function. This instrument is suitable for freeze-dryer experiment in laboratory and a small amount production. FD-18S in-situ freeze dryer that puts the material into drying chamber and the drying process can be completed automatic, so it reduces the traditional tedious operation. Main Characteristics: 1. LCD Display: partition board temperature curve, cold trap temperature curve, sample temperature curve. 2. Can stored 32 program, each program can be set up 36segments, correct program data in computing, memorize the drying curve. 3. The touch-screen display function keys, o operation keys, so reduce the wrong operation, improve the reliability and stability of the instrument, 4. PID control circuit system so that more precise control accuracy.; 5. Imported compressor, the refrigeration speed is quick and dry effect is good. Technical Parameters Order Id FD-18S-RA FD-18S-TPA Cold trap coil temperature <-60 C, -80 C (optional) <-60 C, -80 C (optional) Vacuum <10Pa <10Pa Freeze-dried area m m 2 Water harvesting capacity 6Kg/24h 6Kg/24h Disk loading material 1.8 liters 0.9 liters Material plate ф240mm 4 layers ф200mm total of 3 layers Dimensions ( ) (mm) ( ) (mm) Notice: The temperature of cold trap may reach -80 Caccording to the user s needs. Configuration Order Id FD-18S-RA FD-18S-TPA Freeze Dryer In-situ Freeze-dried Anti oil back vacuum pump Gland device

15 FD-10F Series (-70 C) Electric-heating Freeze Dryer Description: FD-10F electric-heating freeze dryer is freeze-dried in situ. It changes the traditional complicated operation, prevents the pollution of the material and realizes the dry sublimation automation. The freeze dryer has heating and programmable function. It may remember freeze drying curve so the users can observe freeze-drying process of material. Main Characteristics: 1. The process of pre-freezing and drying finishes in situ, the freeze dryer is equipped with observation windows and the drying process is intuitive. 2. The partition board temperature is adjustable and controlled. 3. Touching-screen operation, PID controlling, displaying drying curve. 4. The sample tray is square so it s easy to clean and operate. 5. Valve with nitrogen is optional

16 Technical Parameters: FD-10F Series Drying chamber Cold trap Basic parameters Model FD-10F-R2 FD-10F-TP2 Specification Regular Top-press Freeze-drying area 0.2 m m 2 Layers of partition board 2 layer 1 layer Temperature scope of partition board -45~55 C Partition board space 70mm Size of partition board 265*400*25mm φ22 Bottle (piece) φ16bottle (piece) φ14 Bottle (piece) φ12 Bottle (piece) Cold trap temperature -70 C (no-load) Water-capture capability 3 Kg/24h 1.5 Kg/24h Material 2 L 1 L Electric defrost None Vacuum degree 10 Pa Style of cooling Wind Cooling room temperature 25 C Dimension 660*700*1200mm Configuration Order Id FD-10F-R2 FD-10F-TP2 Freeze Dryer In-situ Freeze-dried Anti oil back vacuum pump Gland device

17 FD-30F Series Electric-heating Freeze Dryer Description: FD-30F-E electric-heating freeze dryer is freeze-dried in situ. It changes the traditional complicated operation, prevents the pollution of the material and realizes the dry sublimation automation. The freeze dryer has heating and programmable function. It may remember freeze drying curve so the users can observe freeze-drying process of material. Main Characteristics: The process of pre-freezing and drying finishes in situ, the freeze dryer is equipped with observation windows and the drying process is intuitive. The partition board temperature is adjustable and controlled. Touching-screen operation, PID controlling, displaying drying curve. The sample tray is square so it s easy to clean and operate. Valve with nitrogen is optional. Technical Parameters: FD-30F-E Model FD-30F-ER Specification Regular Freeze-drying area 0.3 m 2 Layers of partition board 3 layer Temperature Drying chamber scope of partition -50~60 C board Partition board space 70mm Size of partition board 310*310*15mm

18 Cold trap Basic parameters φ22 Bottle (piece) 546 φ16bottle (piece) 1080 φ14 Bottle (piece) 1452 φ12 Bottle (piece) 1950 Cold trap temperature <=-70 C (no-load) Water-capture capability 6 Kg/24h Material 3 L Electric defrost None Vacuum degree <=10 Pa Style of cooling Wind Cooling room temperature<=25 C Dimension 630*800*1400 mm Configuration Order Id Freeze Dryer In-situ Freeze-dried Anti oil back vacuum pump FD-30F-ER

19 FD-30F Series Automatic Freeze Dryer Description: FD-30F Silicone oil-heating freeze dryer is which freeze dried in situ (Patented product).it changes the traditional complicated operation,prevents the pollution of the material realizes the dry sublimation automation. It is suitable for unit production. The freeze dryer has heating shelf and programmable function. It may remember freeze drying curve so the users can observe this freeze-drying process of material. Basic Type Main Characteristics: The process of pre-freezing and drying finishes in situ, the freeze dryer is equipped with observation windows and the drying process is intuitive. With silicone oil as a medium, the temperature error is less than or equal 1 C, the drying effect is uniform. The shelf temperature is adjustable, controllable, can be explored in the pilot and production processes; Bulk or stoppering(stoppering is optional,for seal the vial); The drying chamber and cold trap is separated therefore the water-capture capability is higher and drying time is shorter. Touching-screen operation, PID controlling, displaying curve, Can be equipped with a recorder. The sample tray is square so it s easy to clean and operate. Valve with nitrogen is optional, dry and inert gas can be filled The drying chamber adopts transparent organic glass door the changing process of material is clear. The eutectic point test device & automatic tamponade device is optional Stainless steel materials Stopper type

20 Technical Parameters: Model FD-30F-SR FD-30F-STP FD-30F-S Stopper (for seal the Specification Regular vial) Freeze-drying area 0.4 m m 2 Layers of partition board 4+1 layer 3+1 layer Temperature scope of partition board -50~70 C Partition board s temperature +/-1 C (balance) Drying chamber difference Size of partition board 300*320*15mm 300*340*15mm Partition board space 50mm 70mm φ22 Bottle (piece) φ16bottle (piece) φ14 Bottle (piece) Cold trap temperature -70 C Cold trap Water-capture capability 6 Kg/24h Material 4 L 3 L Electric defrost - Style of top-press - hydraulic pressure Basic parameters Ultimate vacuum 10Pa 10Pa Dimension 630*800*1400 mm 1060*700*1500 mm vial load capacity Φ22mm 46pcs, Φ16mm 1080pcs, Φ12mm 1960pcs Φ22mm 546pcs, Φ16mm 1080pcs, Φ12mm 1960pcs Configuration Order Id FD-30F-SR FD-30F-STP Freeze Dryer In-situ Freeze-dried Anti oil back vacuum pump Hydraulic pressure stopper device

21 FD-50F Series In-Situ Freeze Dryer Description FD-50F freeze dryer is which freeze dried in situ (Patented product).it changes the traditional complicated operation, prevents the pollution of the material realizes the dry sublimation automation. It s suitable for unit production. The freeze dryer has heating shelf and programmable function. It may remember freeze drying curve so the users can observe this freeze-drying process of material. Main Characteristics With silicone oil as a medium, the temperature error is less than or equal 1 C, The drying effect is uniform. The shelf temperature is adjustable, controllable, can be explored in the pilot and production processes; The drying chamber and cold trap is separated so the water-capture capability is higher and drying time is shorter. Touching-screen operation, PID controlling, displaying curve, Can be equipped with a recorder. The sample tray is square so it s easy to clean and operate. Valve with nitrogen is optional. dry and inert gas can be filled The drying chamber adopts transparent organic glass door the changing process of material is clear. The test device is optional. The eutectic point test device & automatic tamponade device is optional All stainless steel type is optional. The process of pre-freezing and drying finishes in situ, the freeze dryer is equipped with observation windows and the drying process is intuitive

22 Technical Parameters: FD-50F Series Model FD-50F-R FD-50F-TP Specification Regular Top-press Freeze-drying area 0.7 m m 2 Layers of partition board 4+1 layer 3+1 layer Temperature scope of partition board -50~70 C Partition board s temperature +/-1 C (balance) Drying chamber difference Size of partition board 360*500*15mm 360*480*15mm Partition board space 50mm 70mm φ22 Bottle (piece) φ16bottle (piece) φ14 Bottle (piece) Cold trap temperature <=-70 C Cold trap Water-capture capability 10 Kg/24h Material 10 L 10 L Electric defrost - Yes Vacuum degree 10Pa Style of top-press - Hydraulic pressure Basic parameters Wind Cooling Style of cooling room temperature<=25 C Dimension 700*1030*1500 mm 1220*1100*1700 mm Configuration Order Id FD-50F-R FD-50F-TP Freeze Dryer In-situ Freeze-dried Anti oil back vacuum pump Gland device

23 FD-100F Series Silicone oil-heating freeze dryer Features: FD-100F freeze dryer, which the freeze-drying area is 1.0 and 2.0, square box structure, is suitable for freeze-dryer of lab samples for units production. FD-100F freeze dryer is that large-screen LCD display and the freeze-drying curve is programmable. FD-100F freeze dryer adopts double compressor, cold trap temperature is -70 C,samples may be pre-freeze and dried directly on the board FD-100F freeze dryer include two types: Regular and top-press. Main characteristics: The process of pre-freezing and drying finishes in situ, the freeze dryer is equipped with observation windows and the drying process is intuitive. The temperature is less than or equal 1 C.The drying effect is uniform. The partition-board temperature is adjustable and controlled. The drying chamber and cold trap is separated so the water-capture capability is higher and the drying time is shorter. Touching-screen operation, PID controlling, display drying curve. The sample trap is square so it s easy to clean and operate. Valve with nitrogen is optional. The drying chamber adopts transparent organic glass door the changing process of material is clear. The automatic top-press device and test device are optional

24 Technical Parameters: FD-100F Series Model FD-100F-R FD-100F-TP Specification Regular Top-press Freeze-drying area 1.0 m 2 Layers of partition board 6+1 layer 4+1 layer Temperature scope of partition -50~70 C board Drying chamber Partition board s temperature difference +/-1 C (balance) Size of partition board 360*480*15mm 600*480*15mm Partition board space 70mm 100mm φ22 Bottle (piece) 2016 φ16bottle (piece) 3960 φ14 Bottle (piece) 7200 Cold trap temperature <=-70 C Cold trap Water-capture capability 15 Kg/24h Material 15 L Electric defrost Yes Vacuum degree <=10 Pa Style of top-press - hydraulic pressure Basic Wind Cooling parameters Style of cooling room temperature<=25 C Dimension 1030*750*1700 mm 1300*1200*2200 mm Configuration Order Id FD-50F-R FD-50F-TP Freeze Dryer In-situ Freeze-dried Anti oil back vacuum pump Gland device

25 FD-200F Auto Silicone Oil-heating Freeze Dryer Major Characteristics: The process of prefreezing and drying finishes in one chamber without transfer. It equipped with observation windows and the drying process is intuitive. The temperature error is less than or equal 1.The drying effect is uniform. The shelves temperature is adjustable and controlled. Hollow flooded shelves provide uniform temperature on shelf surfaces Fast turn-around time defrost from smooth wall condenser The drying chamber and condenser is separated, higher water-capture capability and the drying time is shorter. PID control, drying curve could be displayed. The sample trays are square, it s easy to clean and operate. Valve with nitrogen is optional. The drying chamber adopts transparent organic glass door the changing process of material is clear. Technical Specifications: FD-200F Series Drying chamber Vials load capacity Cold trap Basic parameters Model FD-200F-R FD-200F-TP Specification Normal type Stopper for seal the vials Freeze-drying area 2.25 m m 2 Shelves 5+1 layer 4+1 layer Shelf Temperature -50~70 C Shelf Temp. Accuracy +/- 1 C Distance between trays 100mm Size of shelves 500*900*15 mm 810*610 φ22 Bottle (PCS) φ16bottle (PCS) φ12 Bottle (PCS) Cold trap temperature -70 C Water-capture capability 25 Kg/24h 25 Kg/24h Material Capacity 25L 25L Defrost Electric spray + soaking Vacuum degree 10 Pa 10 Pa (Range:1~300Pa) Style of cooling Wind Cooling (Water Cooling is optional) room temperature 25 C Water Cooling Dimension 2100*1200*1700 mm 2700*1500*2500 (mm) Power 10000VA 17000VA Data Process RS232 Interface with software

26 FD-P Series Production Freeze Dryer (Customization) Parameters: Model Unit FD-P3 FD-P4 FD-P5 FD-P8 FD-P10 FD-P15 FD-P20 FD-P25 FD-P30 FD-P40 Parameters m Effective diaphragm area m Cold trap capacity, MAX KG / batch Small amount of bottled (mm) Φ22 pcs Φ16 pcs Φ12 pcs MAX panel mounted liquid L Partition size Long mm Wide mm Baffle spacing mm The number of partitions Block Maximum temperature +70 partition Minimum temperature -50 partition Partition ± 1 (equilibrium)

27 temperature The lowest temperature cold -70 (No load) trap Minimum vacuum No load <10Pa() Cooling water, <30, Mpa (for m3 / h water-cooled units) Cooling (for air-cooled units) CIP-WIP,>65, MPa Compressed air Mpa 2 m above the water-cooled units L / min 100 m3/min 0.1 Defrost water (soak) 50, Mpa KG / batch Installed power KW Weight KG Long mm Wide mm High mm Note: The device dimensions are for reference only, as the customer actually needs to be adjusted. Parts Introduction German Bitzer Compressor

28 France Taikang compressor Leybold Vacuum Germany Germany's Wilo pump Danish Grundfos circulation pump Danfoss solenoid valve Danfoss expansion valve

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