API 2000 LC/MS/MS TurboIonSpray Ion Source Manual
|
|
- Domenic Daniels
- 6 years ago
- Views:
Transcription
1 Table of Contents API 2000 LC/MS/MS TurboIonSpray Ion Source Manual Table of Contents API 2000 TurboIonSpray Ion Source Manual....1 AboutThisManual...1 Introduction...1 TurboIonSpraySourceComponents...3 Installation...6 OptimizingtheTurboIonSpray...7 ChangingThePeekTubingTransferLine...12 ChangingTheStainlessSteelSprayerTube...14 Changing The Grounded Union/Splitter Fitting...14 AppendixA-ConsumableParts...16 AppendixB-Troubleshooting...17 Introduction...17 i
2 Table of Contents ii
3 API 2000 TurboIonSpray Ion Source Manual About This Manual Conventions This manual contains the instructions required to operate the API 2000 TurboIonSpray ion source. Within this manual, the following conventions are used: WARNING! Indicates an operation that may cause personal injury if precautions are not followed. CAUTION! Indicates an operation that may cause damage to the instrument if precautions are not followed. Introduction NOTE: Emphasizes significant information in a procedure or description. TurboIonSpray is an Atmospheric Pressure Ion Source in which pre-formed ions in solution are emitted into the gas phase with or without the application of heat. In this way, quasi-molecular ions can be generated from very labile and high molecular weight compounds with no thermal degradation. TurboIonSpray is the technique by which a liquid sample is pumped by a liquid chromatograph (LC) pump or syringe drive through a sprayer probe, which is maintained at a high voltage, and is nebulized into the Ion Source creating a mist of highly charged droplets. Once inside the Ion Source, the droplets evaporate causing the ions to enter the gas phase by a low energy process called Ion Evaporation. The use of an orthogonal heated gas extends the rugged and versatile technique of TurboIonSpray to accept higher flow rates with improved sensitivity. TurboIonSpray will accept flows from 5 to 1000 µl/min of solvent compositions from 100% aqueous to 100% organic, such as acetonitrile, without splitting. This allows the use of 1 mm, 2 mm, and 4.6 mm analytical columns with or without splitting. A heater probe directs a jet of heated dry gas (up to a maximum of 500 C) at the mist produced by the sprayer. The gas is sprayed across the orifice at an angle of approximately 45 with respect to the Curtain Plate. The liquid spray emerging from the TurboIonSpray is directed at an angle of about 45 from the opposite direction (or 135 ). The TurboIonSpray effluent and the heated dry gas intersect at an angle of approximately 90 near the orifice. This interaction helps focus the TurboIonSpray stream and increases the rate of droplet evaporation resulting in an increased ion signal. 1
4 Features Specifications TurboIonSpray Setup TurboIonSpray is ideally suited for LC/MS/MS quantitative analyses. The sensitivity increases that are achieved with this technique are both flow rate and analyte dependent. In the conventional IonSpray source sensitivity decreases with increased flow rate, while the heated TurboIonSpray process increases ionization efficiency, especially at the higher flow rates; this results in improved sensitivity. Sensitivity is compound dependent and compounds of extremely high polarity and low surface activity usually show the greatest sensitivity increases. The TurboIonSpray technique is mild enough to be used with labile compounds such as peptides, proteins, and thermally labile pharmaceuticals. NOTE: The difference between conventional IonSpray and TurboIonSpray is that in the TurboIonSpray, the ionization of the sample is achieved with additional heater gas delivered to aid in the desolvation of the spray. Typically the TurboIonSpray is used at higher flow rates (greater than or equal to 40 µl/min). The following list outlines the features of the TurboIonSpray ion source: Able to function as conventional IonSpray source when the Heater Gas is turned off. Able to function with flow rates from 1 µl/min to 1000 µl/min. Able to vaporize 100% aqueous to 100% organic solvents. Temperature Range Probe temperature from 0 to 500 C Liquid Chromatograph Interfaces to any liquid chromatograph system 2
5 TurboIonSpray Nebulizer and Heater Gases (Gas 1 and 2) Zero Grade Air regulated to 100 psi TurboIonSpray Source Components Ion Source Housing API 2000 TurboIonSpray Ion Source Manual The ion source housing forms a seal with the instrument interface assembly to prevent any solvent or sample from escaping into the laboratory environment. Any liquid or vapour entering the source is safely transferred to a waste receptacle and fume hood with the aid of the source exhaust pump. The source housing incorporates two motion mechanisms (that adjust the position of the sprayer, described below), two windows to allow the user to view the position and condition of the sprayer, a Peek tubing transfer line, a grounded union/splitter fitting, two latches used for locking the source in place and integrated voltage/gas connectors. The connections for the voltage, heater and gases are made automatically once the source is locked to the interface.. TurboIonSpray Ion Source Sprayer Probe The TurboIonSpray source contains a fixed angle adjustable sprayer probe. The sprayer probe is adjustable in two directions: towards the orifice from a scale of 0 to 12 (adjusted by the horizontal adjusting ring mounted on the TurboIonSpray probe), and up and down towards the orifice from 0 to 12 by the Lateral Adjustment control on the top of the Ion Source. 3
6 Sprayer Probe Sprayer Probe and Adjustments The TurboIonSpray probe gas, or Nebulizer gas (Gas 1) and voltage (IS) are set at the applications computer using the software. The connections for the voltage and gas are made automatically once the source is locked to the interface. Transfer Line and Grounded Union/Splitter A short piece of Peek tubing (30 cm, ID) connects the sprayer probe inlet to a grounded fitting that can be used either as a union or splitter. Since the liquid being sprayed from the source is in contact with high voltages, the transfer line must be connected to the grounded fitting. Peek Tubing Grounded Union/Splitter PEEK Tubing and Grounded Union/Splitter 4
7 WARNING! The use of the Peek tubing transfer line connected to the grounded fitting is mandatory since it prevents any exposed peripherals connected to the source from floating at high voltage. Heater Probe WARNING! Peek tubing (or fused silica) with Peek fittings must be used as the transfer line. Metal tubing or fittings must not be used. The use of metal may result in the exposure of high voltage to the user. Refer to the procedure for changing the grounded fitting from a union connection to a splitter described later in this document. The heater probe temperature is set in the applications computer software by modifying the TEM parameter. The correlation between the parameter value of TEM and the actual heater temperature is direct (for example TEM 350 is equal to 350 C at the heater). The heater gas is also set in the applications computer software. The connections for the heater and gas are made automatically once the source is locked to the interface. The heater probe temperature is maintained by the Temperature Control Board (TCB) mounted behind the IonSource panel (below the IonSource housing). The TCB adjusts the flow of power to the heater element as a function of the difference between the actual heater temperature and the temperature setting in the applications computer. The probe temperature is monitored by a thermocouple connected directly to the heater element which maintains the temperature within ±5 degrees of the applications computer setting. The operating range for the probe is from approximately 100 to 500 C. NOTE: The temperature is controlled by monitoring the output of a thermocouple connected to the heater surrounding the metal tube. At the temperature control board the thermocouple output is compared with the temperature setting, the difference determines the power flow to the heater. The operating temperature should be adjusted relative to LC mobile phase composition and flow rate. In general, a combination of heat and gas flow that just allows the liquid spray to reach dryness before reaching the curtain plate will provide optimum performance. Heater gas flows of approximately 6 L/min can be considered optimum for conditions where heat is required. Ionization efficiency is improved with the input of heat for all liquid flow rates. However, at lower flow rates (<20 µl/min) the gains are small. Heat inputs may be desirable under low flow conditions for the additional reason of enhancing in-source (orifice-skimmer) fragmentation. Temperatures as low as C have proven useful for enhancing this capability (phosphopeptide mapping for instance) when operating at low flow rates. 5
8 Exhaust Pump The TurboIonSpray Source requires that the Source Exhaust system is properly connected and functioning (refer to the figure Exhaust Supply Connection Points under Source Exhaust Pump in the Optimizing the TurboIonSpray section). A filtered nitrogen or air gas supply (free from pump oil) is delivered to the Source Exhaust pump at 60 psi pressure at a flow of at least 4 L per minute. The Source Exhaust pump is used to vent solvent vapors which develop in the Ion Source plenum. It is recommended that these vapors be passed through a trap vented to a fume hood or outside port. WARNING! Failure to provide proper ventilation of the ion source can result in hazardous vapors being released into the laboratory environment. Installation The TurboIonSpray source connects to the Vacuum Interface housing. Two latches mounted on the source housing secure the TurboIonSpray against the vacuum interface. To install the TurboIonSpray on the API instrument: 1. Ensure that the two source latches are in the unlocked (up) position. 2. Align the two guide pins on the source with the vacuum interface receptacles. Guide Pins Guide Pin Alignment 3. Slide the source along the guide pins towards the interface as far as it can go without using excessive force. 4. Turn the two source latches to the locked (down) position. 5. The TurboIonSpray Nebulizer and Heater Gas (Gas 1 and 2), the sprayer high voltage and heater connectors are automatically engaged once the source is locked in position. 6
9 6. Connect the liquid sample tubing to the grounded fitting which is connected to the inlet end of the sprayer probe. Ensure that all fittings are properly seated in order to minimize dead volumes. NOTE: In order to reduce the band broadening of sample with solvent, thus maximizing sensitivity, the use of ID Peek, or fused silica tubing between the TurboIonSpray source and the injector is recommended. To remove the TurboIonSpray from the API instrument: WARNING! Ion source may be hot for several minutes after it is removed from the instrument. 1. Stop all scans and place the instrument in Standby or Overnight Quit status. 2. Turn off the liquid flow entering the ion source. 3. Disconnect the liquid sample tubing from the grounded fitting. 4. Turn the two source latches to the unlocked (up) position. The sprayer high voltage and heater connectors are automatically disengaged once the source is unlocked. 5. Slide the source along the guide pins away from the interface to remove it. Optimizing the TurboIonSpray The following section outlines the practical considerations which must be made when optimizing the TurboIonSpray performance. It is intended to provide the qualitative information necessary to aid the operator in quantifying the separate operating parameters. TurboIonSpray performance depends on the following factors: Sprayer position TurboIonSpray (IS) voltage Nebulizer gas (NEB) Curtain gas (CUR) Heater Gas flow and Temperature (Gas 2 and TEM) Declustering Potential (DP) and Focusing Potential (FP) voltage (compound dependent) Solvent Composition Optimum performance on standard compounds is relatively easy to achieve and little adjustment or tuning is required once the Source is optimized. With experience, the operator will develop a personal optimization method which works best. In general, once the sprayer is set up and optimum factors have been determined, little or no readjustment of the values is required on a day-to-day basis. For tuning purposes a compound with a known molecular ion should be introduced either by continuous infusion or flow injection. Infusion is preferred because it provides a continuous flow of sample. The tuning compound should have characteristics similar to the sample to be analyzed during normal operation and should be introduced at the same liquid flow rate. 7
10 CAUTION! When optimizing the Sprayer position make certain not to spray directly down the orifice. Spraying down the orifice may contaminate the Vacuum Interface and Vacuum Chamber ion optics and could impact instrument performance. CAUTION! To avoid possible damage to the instrument, always view the sprayer tip through the side port when adjusting its position. CAUTION! If unattended user operation is intended through the use of sample control, Ensure that LC shut-off is in use to prevent flooding of the plenum chamber. TurboIonSpray Probe Position The position of the TurboIonSpray Probe relative to the Orifice and to the Heater Probe is an important factor in optimizing the TurboIonSpray performance. The probe should point between 5 and 10 mm off axis with respect to the center of the orifice. The distance of the Heater Probe from the orifice plane is fixed, but the TurboIonSpray can be adjusted using the scale on the side of the Sample inlet arm. Changing from low solvent flow rates (40µL/min) to high solvent flow rates (1mL/min) requires that the TurboIonSpray be repositioned further away from the orifice to prevent solvent penetration through the orifice into the mass spectrometer. OPTIMAL TURBOIONSPRAY TARGET CURTAIN PLATE 40 µl/min ORIFICE 200 µl/min 1mL/min TurboIonSpray Positioning Across the Orifice Also as the aqueous composition of the carrier solvent increases at high flow rates (1 ml/ min), the more visible the spray becomes and the further away from the orifice it should be directed. See the figure above where the areas indicated in the diagram for the different flow rates are the optimum target areas for the TurboIonSpray liquid spray. The circle immediately around the orifice (for example the part of the orifice plate which is visible when viewing the front of the interface) should remain clear of solvent or solvent drops at all times. 8
11 The best position is usually a few millimeters off axis to the bottom of the curtain plate aperture. Multiply charged proteins and peptides introduced at a few microliters per minute usually require the sprayer to be as close as possible to the Curtain Plate. TurboIonSpray Voltage (IS) In positive mode, singly charged compounds usually require a high probe voltage of between 4000 to 5500 V. In negative mode, compounds usually require a lower voltage, between 3000 to V. NOTE: If the TurboIonSpray voltage is set too high a blue glow can be seen at the tip of the TurboIonSpray indicating a corona discharge. This will result in decreased sensitivity and stability of the ion signal. Nebulizer Gas (Gas 1) Optimize for signal stability and sensitivity. Typically a value of 10 to 45 psi is used as applied by the applications computer. Curtain Gas Flow (CUR) The Curtain Gas ensures a stable clean environment for the sample ions entering the mass spectrometer. The gas curtain prevents air or solvent from entering the analyzer region of the instrument while permitting the sample ions to be drawn into the vacuum chamber by the electrical fields generated between the Vacuum Interface and the TurboIonSpray needle. The presence of the solvent vapor or moisture in the analyzer region of the mass spectrometer contaminates the Q0 Rod Set causing a reduction in resolution, stability, sensitivity, and an increase in chemical background noise. As a general rule, the Curtain Gas flow should be set as high as possible without reducing the signal significantly (for example start at a lower value and increase the flow until the signal starts to decrease). In order to prevent instrument contamination the Curtain Gas flow should be optimized at the highest possible setting, but never below 11 psi, that does not result in a significant reduction in signal intensity. It is suggested that the TurboIonSpray be operated with curtain gas settings adjusted to the highest flow rate possible (never below 11) without signal loss. Heater Gas (Gas 2) The Heater Gas (Gas 2) aids in the evaporation of solvent which aids in increasing the ionization of the sample. The higher the liquid flow or the higher the aqueous composition of the solvent, the higher the Heater Gas temperature and gas flow required. However, too high a temperature can cause premature vaporization of the solvent, and result in a high chemical background noise, while too high a Heater Gas flow can produce a noisy, or unstable signal. 9
12 The table below provides recommended operating conditions for the TurboIonSpray at three different flow rates. For each flow rate, the Curtain Gas flow rate (from setting 11 to 45 at the applications computer) should be as high as possible. The solvent composition used for optimization was 1/1 Water/Acetonitrile. These conditions represent a starting point from which to optimize TurboIonSpray. By an iterative process, the various settings can be optimized using Flow Injection Analysis to obtain maximum signal-to-noise for the compound of interest. TurboIonSpray Suggested Operating Settings Table Flow Rate µl/min TurboProbe Temp. ( C) 40 µl/min. 300 (200 to 500) 200 µl/min. 400 (300 to 500) 1 ml/min. 475 (450 to 500) Heater Gas (GAS2) Flow (L/min) PSI 6 65 (4 to 8) (40-90) 7 75 (4 to 8) (40-90) 8 90 (4 to 8) (40-90) V = Vertical position H = Horizontal position Nebulizer Setting (GAS 1) 20 (10-30) 30 (15-35) 50 (20-55) Position V H Turbo Temperature (TEM) The quantity and type of sample affect the optimal TurboIonSpray temperature. At higher flow rates the optimal temperature increases. A more significant factor is the composition of the solvent. As the organic content of the solvent increases the optimal probe temperature should decrease. With solvents consisting of 100 percent methanol or acetonitrile the probe performance may optimize as low as 300 C. Aqueous solvents consisting of 100 per cent water at flows approximately 1mL/min require a minimum probe temperature of 425 C. Normal optimization is usually performed in increments of 25 C. The TurboIonSpray is normally used with sample flow rates of 40 µl/min to 1000 µl/ min. The heat is used to increase the rate of evaporation and this improves ionization efficiency resulting in increased sensitivity. See the table above for recommended temperatures. CAUTION! Do not operate the TurboIonSpray with probe temperatures greater than 500 o C. Declustering Potential (DP) and Focusing Potential (FP) Voltages Optimal Declustering Potential and Focusing Potential operating conditions with the TurboIonSpray source should be set high enough to reduce the chemical noise but low enough to avoid fragmentation. Start with the Focusing Potential (FP) at 300V and the Declustering Potential (DP) at 20V. 10
13 NOTE: The fragmentation energy of a compound is a function of its structure and molecular weight. Generally lower molecular weight compounds require less energy - lower Declustering Potential and Focusing Potential voltages to induce fragmentation. For some labile compounds, DP values of between 5 to 10 may be required with the TurboIonSpray. In general terms, the higher the Declustering Potential and Focusing Potential voltages, the greater the energy imparted to the ions entering the analyzing region of the mass spectrometer. The energy helps to decluster the ions and to reduce the chemical noise in the spectrum resulting in an increase in sensitivity. Increasing the voltages beyond optimal conditions can induce fragmentation before the ions enter the mass filters resulting in a decrease in sensitivity. In some instances this fragmentation can prove a valuable tool providing additional structural information. Solvent Composition Commonly used solvents and modifiers are acetonitrile, methanol, propanol, water, acetic acid, formic acid, ammonium formate and ammonium acetate. The modifiers such as TEA, sodium phosphate, TFA and dodecyl sodium sulfate are not commonly used because they complicate the spectrum with their ion mixtures and cluster combinations. They may also suppress the strength of the target compound ion signal. The standard concentration of ammonium formate or ammonium acetate is from 2 to 10 millimole per liter for positive ions and 2 to 50 millimole per liter for negative ions. The concentration of the organic acids is 0.01% to 0.5% by volume. Source Exhaust Pump The Source Exhaust system is required for TurboIonSpray operation. The exhaust pump draws the solvent vapors from the enclosed source chamber and delivers them to a trap at the rear of the instrument chassis where they can be collected. The Source Exhaust system is interlocked to the system electronics, such that if the source exhaust pump is not operating to specification the instrument electronics are disabled. The exhaust system lowers the pressure in the source slightly below atmospheric. If the pressure in the source rises beyond a preset trip point, the instrument High Voltage Power Supply is disabled. 11
14 . e Curtain Gas Supply Exhaust Supply Valve Waste Out Gas1/Gas2 Exhaust Supply Connection Points Exhaust Waste Out Operating Tips 1. When running the TurboIonSpray, with or without the Heater Probe on, run the Curtain Gas at as high a flow rate as possible. The Curtain Gas should optimize about 30% higher when TurboIonSpray is in use. This will help to: a) prevent penetration of the Curtain Gas which can produce a noisy signal, b) prevent contamination of the orifice, and c) increase the overall signal to noise ratio 2. The liquid spray from the TurboIonSpray should be directed away from the orifice in order to: a) prevent contamination of the orifice, b) prevent piercing of the Curtain Gas which can create an unstable signal, and c) prevent electrical shorting due to the presence of the liquid. 3. The higher the liquid flow or the higher the aqueous composition of the solvent, the higher the temperature and Heater Gas (Gas 2) flow required. However, too high a temperature can cause thermal degradation of the compound, and result in a high chemical background noise, while too high a heater gas flow can produce a noisy, or unstable signal. Changing The Peek Tubing Transfer Line A Peek tubing transfer line is used to carry the sample and solvent from the Sample Inlet to the metal sprayer tube where it is nebulized and ionized. The standard TurboIonSpray set-up uses a 30 cm, (65 µm) ID Peek tubing transfer line. 12
15 WARNING! The use of the Peek tubing transfer line connected to the grounded fitting is mandatory since it prevents any exposed peripherals connected to the source from floating at high voltage. To exchange the Peek tubing transfer lines in the TurboIonSpray in the event of blockage of the existing line: 1. Remove the TurboIonSpray and set on its side. 2. Unscrew the Peek tubing fittings from the probe inlet and grounded union/splitter fitting and discard the old tubing (the fittings may be re-used if they have not been over-tightened and damaged). Peek Tubing 3. Obtain a new piece of Peek tubing (it must be at least 30 cm long) and place Peek connection fittings on each end. WARNING! Peek tubing (or fused silica) with Peek fittings must be used as the transfer line. Metal tubing or fittings must not be used. The use of metal may expose the user to high voltage. 4. Connect the Peek tubing to the probe inlet and grounded union/splitter fitting. 13
16 Changing The Stainless Steel Sprayer Tube The standard TurboIonSpray set-up uses a (100 µm) ID metal sprayer tube. The procedure outlined below should be used to exchange the metal tube in the TurboIonSpray in the event of blockage or degradation of the sprayer tip. 1. Remove the TurboIonSpray and set on its side. 2. Disconnect the Peek transfer line from the probe inlet. 3. Unscrew and remove the black inlet probe fitting. A Peek union, metal spring and the metal sprayer tube can now be removed from the probe. 4. Unscrew the fitting holding the metal tube to the Peek union. Remove the tube from the fitting and discard. Do not discard the fittings. Metal Sprayer tube removed 5. Place a new sprayer tube and ferrule in the fitting and screw into the Peek union. Ensure that the sprayer tube is placed as far as it can go into the Peek union to guarantee a leak-proof seal (two wrenches should also be used to tighten the fittings). 6. Place the metal spring and metal tube/peek union back into the probe. 7. Place the black inlet probe fitting over the Peek union and tighten. This fitting is used to adjust the protrusion of the metal sprayer tube tip at the end of the probe. The metal tube should protrude approximately 0.75 mm, although a protrusion between 0.5 to 1.25 mm is also acceptable. Changing The Grounded Union/Splitter Fitting A Peek tubing transfer line connects the sprayer probe inlet to a grounded fitting that can be used either as a union or splitter. Since the liquid being sprayed from the source is in contact with high voltages, the transfer line must be connected to the grounded fitting. 14
17 WARNING! The use of the Peek tubing transfer line connected to the grounded fitting is mandatory since it prevents any exposed peripherals connected to the source from floating at high voltage. To change between the union and splitter insert fittings: 1. Remove the TurboIonSpray and set on its side. 2. Disconnect the Peek transfer line from the ground fitting. 3. Disconnect any other fittings or tubing that may be connected to the grounded fitting. 4. The insert within the grounded fitting should now move freely and can be removed by tilting the source and allowing it to fall out. 5. Place the new insert into the fitting and align it such that all the openings match. 6. Connect the Peek transfer line to the grounded fitting and any other fittings or tubing that may be used. WARNING! Peek tubing (or fused silica) with Peek fittings must be used as the transfer line. Metal tubing or fittings must not be used. The use of metal may result in the exposure of high voltage to the user. 15
18 Appendix A - Consumable Parts Appendix A - Consumable Parts The following is a list of parts included in the Kit of consumable parts (part number ) supplied with the TurboIonSpray assembly. Item Part No. Description (Quantity) Probe Spring (1) ID Peek Tubing (60 cm) Probe Inlet Nut (1) Viton O-Ring, 7/64 ID (2) Viton O-Ring, 4 mm ID (2) Metal Electrode Tube (2) Peek LC Fitting (2) Peek Union (1) Splitter Tee Insert, 0.25 mm bore (1) Peek Ferrule (4) Viton O-Ring, 2 mm ID (2) 16
19 Appendix B - Troubleshooting Appendix B - Troubleshooting Introduction The troubleshooting procedures given here are suitable for use by operators who have access to an ohm meter and are familiar with its use. These procedures do not require removal of the instrument covers and do not expose the operator to hazardous voltages. The heater control circuits are protected by a resetable over current device. This device may be tripped by excessive heater current or by failure to approach the desired operating temperature within about 5 minutes. When tripped the device will remove power from the heater. To reset the protective device turn power off the system for about one minute or remove the ionizer from the system for about one minute. Diagnosis of the nature of the fault is done by means of ohm meter readings taken across the pins of the ionizer 24 pin connector on the ionizer which is shown below. Ionizer 24 Pin Connector 17
20 Appendix B - Troubleshooting FAILURE MODES HEATED IONIZER Table # CAUSE SYMPTOMS DIAGNOSIS CURE 1 Short circuit in heater. No heat. Heater resistance measured across pins 7 and 19 is less than 15 ohms. 2 Open circuit in heater. No heat. Heater resistance measured across pins 7 and 19 is greater than 25 ohms. 3 Heater grounded. No heat. Heater resistance from pin 9 to ionizer frame is less than 100K ohms. 4 RTD short circuit. No heat. RTD resistance measured across pins 9 and 10 is less than 100 ohms. 5 RTD open circuit. No heat. RTD resistance measured across pins 9 and 10 is greater than 300 ohms. 6 RTD grounded. No heat. RTD resistance from pin 10 to ionizer frame is less than 100K ohms. 7 Poor thermal contact between the RTD and the heater. When starting the heater with the temperature set to greater than 300 C, the heat comes on for about 5 minutes and then goes off. The heater works normally when the temperature is set to 150 C Call service to replace heater. Call service to replace heater. Call service to replace heater. Call service to replace RTD. Call service to replace RTD. Call service to replace RTD. Call service to correct clips attaching the RTD to the heater. 18
Q Trap LC/MS/MS TurboIonSpray Ion Source Manual. About This Manual... 1 Conventions Introduction... 3 Features... 4
Q Trap LC/MS/MS TurboIonSpray Ion Source Manual Table of Contents Table of Contents About This Manual................................................ 1 Conventions.........................................................
More informationAPI LC/MS/MS TurboIonSpray Ion Source Manual Table of Contents
Table of Contents API LC/MS/MS TurboIonSpray Ion Source Manual Table of Contents TurboIonSpray Ion Source Manual...1 AboutThisManual...1 Conventions....1 Introduction...1 Features...2 TurboIonSpray Components...2
More informationInstalling the Agilent CE ESI-MS Sprayer Kit (G1607A)
s1 Installing the Agilent CE ESI-MS Sprayer Kit (G1607A) This note describes how to connect an Agilent capillary electrophoresis system to an Agilent mass selective detector (G1946A). Typical method parameters
More informationApex E Quick Installation Guide
ELEMENTAL SCIENTIFIC INC. Apex E Quick Installation Guide Apex E Quick Installation Guide ã Elemental Scientific Inc. 2440 Cuming Street Omaha, NE 68131 USA Phone 402.991.7800 Fax 402.991.7799 Table of
More informationMariner Microspray and Low-Flow Electrospray Fused Silica Spray Tip and Capillary Kit. Operating Instructions. 1 Product Description.
Mariner Microspray and Low-Flow Electrospray Fused Silica Spray Tip and Capillary Kit Operating Instructions 1 Product Description The Mariner Microspray and Low-Flow Electrospray Fused Silica Spray Tip
More informationHISTORY OF VARIAN CAPILLARY INJECTORS
HISTORY OF VARIAN CAPILLARY INJECTORS by Randall Bramston-Cook Lotus Consulting 5781 Campo Walk Long Beach, Ca 90803 310/569-0128 714/898-7461 Fax and Herb Neumann Varian, Inc. 2700 Mitchell Drive Walnut
More informationAgilent 6400 Series. Maintenance Guide. Agilent Technologies
Agilent 6400 Series Triple Quad LC/MS Maintenance Guide Agilent Technologies Notices Agilent Technologies, Inc. 2010 No part of this manual may be reproduced in any form or by any means (including electronic
More informationAn Introduction to Mass Spectrometry
An Introduction to Mass Spectrometry Guy Wilson UPC 2 & Purification Business Development, Northern Europe, Waters Ltd 2013 Waters Corporation 1 What is a Mass Spectrometer? Data System Sample Introduction
More informationEldex Column Heater. Operator s Manual
Eldex Eldex Column Heater Operator s Manual Eldex Laboratories, Inc. 30 Executive Court Napa, CA 94558 Tel: (707) 224-8800 Fax: (707) 224-0688 www.eldex.com Rev. B: 081700 2000Eldex Laboratories, Inc.
More informationOptimizing the Performance of the Agilent 1290 Infinity Evaporative Light Scattering Detector
Optimizing the Performance of the Agilent 129 Infinity Evaporative Light Scattering Detector Technical Overview Author Bettina Schuhn Agilent Technologies, Inc. Waldbronn, Germany Abstract This Technical
More informationHigh Volume Injection up to 5 ml with the Agilent 1200 Infinity Series Online SPE Solution for Highest Sensitivity
High Volume Injection up to ml with the Agilent 00 Infinity Series Online SPE Solution for Highest Sensitivity Technical Overview Author Bettina Schuhn Agilent Technologies, Inc. Waldbronn, Germany Abstract
More informationAnalysis of Pharmaceuticals and Personal Care Products in Groundwater by Online SPE and LC/MS/MS
Analysis of Pharmaceuticals and Personal Care Products in Groundwater by Online SPE and LC/MS/MS Application note Water analysis Authors E. Michael Thurman, Imma Ferrer, and Karl Mauch University of Colorado,
More informationSolid Phase Extraction using the 96-well Format ISOLUTE -96 Fixed Well Plates and ISOLUTE Array 96-well Plates
TN114 Solid Phase Extraction using the 96-well Format ISOLUTE -96 Fixed Well Plates and ISOLUTE Array 96-well Plates New approaches to the quantitation of drugs and metabolites in biological fluids have
More informationOn-line SPE Enrichment of Trace Organic Contaminants in Water and Juices
On-line SPE Enrichment of Trace Organic Contaminants in Water and Juices Application Note Environment and Food Authors E. Michael Thurman, Imma Ferrer Center for Environmental Mass Spectrometry Department
More informationTIMS TIMS. Thermal Ionisation Mass Spectrometry.
TIMS Thermal Ionisation Mass Spectrometry www.nu-ins.com Incorporating our field-proven Zoom lens multi-collector technology, the TIMS improves the versatility and overall performance of this long established
More informationDART-Thermo LTQ/Orbitrap Interface Manual
DART-Thermo LTQ/Orbitrap Interface Manual For Thermo LTQ (Orbitrap) Velos, LTQ Orbitrap XL, LTQ Ion Trap, Exactive High Performance, and all other instruments that utilize the Ion Max Source Version 20120423
More informationApplication Note. The Agilent 1200 Infinity Series Online SPE Solution for the Highest Sensitivity. Author. Abstract.
Comparison of Online SPE Analysis and Direct Injection of Trace Level Estrogens in Drinking Water with the Agilent 646 and Agilent 649 Triple Quadrupole s The Agilent 1 Infinity Series Online SPE Solution
More informationACQUITY UPLC HT Column Heater Instructions
ACQUITY UPLC HT Column Heater Instructions Note: This document is an addendum to Revision C of the ACQUITY UPLC System Operator s Guide. Contents: Topic Page Overview 1 Connecting the cable 4 Installing
More informationTechnical specifications of FT-IR Spectrometer
Technical specifications of FT-IR Spectrometer We would like to buy a FT-IR spectrometer which has to be integrated with a Gas Chromatograph with the following technical specifications. 1. The spectrometer
More informationUniversal NanoFlow Sprayer Installation and Maintenance Guide
Universal NanoFlow Sprayer Installation and Maintenance Guide 71500110107/Revision C Copyright Waters Corporation 2007 All rights reserved Copyright notice 2007 WATERS CORPORATION. PRINTED IN THE UNITED
More informationAquamax KF Oil Evaporator. User Manual
Aquamax KF Oil Evaporator User Manual Edition 1.1 - April 2015 Contents Chapter 1 Introduction... 2 1.1 Instrument Description... 2 1.2 Principle of Measurement... 2 1.3 Instrument Connections... 2 Chapter
More informationIMPROVING THE QUANTITATIVE REPRODUCIBILITY OF AN ATMOSPHERIC PRESSURE CHEMICAL IONISATION SOURCE FOR GC/MS AND GC MS/MS ANALYSIS
IMPROVING THE QUANTITATIVE REPRODUCIBILITY OF AN ATMOSPHERIC PRESSURE CHEMICAL IONISATION SOURCE FOR GC/MS AND GC MS/MS ANALYSIS Jones GR 1, Douce D 1 1 Waters Corporation, Stamford Avenue, Wilmslow, United
More informationCentriVap. Centrifugal Vacuum Concentrators and Cold Traps
CentriVap Centrifugal Vacuum Concentrators and Cold Traps 2 CENTRIVAP VACUUM CONCENTRATORS & COLD TRAPS Page An Overview 2 CentriVap Benchtop Vacuum Concentrators 4 Refrigerated CentriVap Vacuum Concentrators
More informationDirect Injection and Online SPE LC/MS/MS for the Determination of Pharmaceuticals and Personal Care Products (PPCPs) in Water Samples
Application Note Environmental Direct Injection and Online SPE LC/MS/MS for the Determination of Pharmaceuticals and Personal Care Products (PPCPs) in Water Samples Using the Agilent InfinityLab Online
More informationChemistry Instrumental Analysis Lecture 29. Chem 4631
Chemistry 4631 Instrumental Analysis Lecture 29 Gas Chromatography Detectors Gas Chromatography Monitors the column effluent and produces an electrical signal that is proportional to the amount of analyte
More informationEnhancing Throughput of Online SPE Analysis of Pesticides in Wastewater The Agilent 1200 Infi nity Series Online SPE Solution
Enhancing Throughput of Online SPE Analysis of Pesticides in Wastewater The Agilent 00 Infi nity Series Online SPE Solution Technical Overview Author Bettina Schuhn Agilent Technologies, Inc. Waldbronn,
More informationAgilent InfinityLab Online SPE Solution
Agilent InfinityLab Online SPE Solution Instruction Agilent Online SPE Solution - Instruction Technical Information about the Agilent InfinityLab Online SPE Solution. The following possible set-ups are
More informationAUC Cell Washer. User Manual
AUC Cell Washer User Manual WARRANTY Spin Analytical Inc., warrants this product to be defect free in both material and workmanship for 90 days from the date of shipment. Labor services are guaranteed
More informationFPD - Flame Photometric Detector
FPD - Flame Photometric Detector FPD Overview - The FPD detector is can be configured for 2 modes of operation, one is highly selective for Sulfur compounds and the other mode highly selective for Phosphorus
More informationCone Calorimeter. (ISO 5660 ASTM E 1354) The most comprehensive bench scale fire test THE BENCHMARK IN FIRE TESTING
Cone Calorimeter (ISO 5660 ASTM E 1354) The most comprehensive bench scale fire test THE BENCHMARK IN FIRE TESTING Cone Calorimeter (ISO 5660 ASTM E 1354) The most comprehensive bench scale fire test The
More informationTekmar-DOHRMANN The 3100 Sample Concentrator From ManualLib.com
Tekmar-DOHRMANN The 3100 Sample Concentrator http://www.manuallib.com/file/2660162 From ManualLib.com ManualLib.com collects and classifies the global product instrunction manuals to help users access
More informationApplication Note. Authors. Abstract
Analysis of Four β-lactam Antibiotics in Water Using an Agilent 0 Infinity II LC and an Agilent 0 Triple Quadrupole LC/MS with Direct Injection and Online SPE Application Note Authors Alexander Timm, Rafael
More informationAir Server & Multi Channel Samplers (MCS06 & MCS08)
Air Server & Multi Channel Samplers (MCS06 & MCS08) Operators Manual AUGUST 2006 QUI-0004 VERSION 6.1 Ltd. T: +44 (0)1443 230935 F: +44 (0)1443 231531 E: enquiries@markes.com This page left intentionally
More informationTHERMAX Efficiency Monitor
INSTALLATION & OPERATION INSTRUCTIONS THERMAX Efficiency Monitor Oil & Gas Fired Heating Equipment Efficiency Monitoring Instrument Important Safety Instructions Read and safe these instructions before
More informationWaters Xevo G2 QTof Operator s Overview and Maintenance Guide
Waters Xevo G2 QTof Operator s Overview and Maintenance Guide Revision B Copyright Waters Corporation 2010 2011 All rights reserved Copyright notice 2010 2011 WATERS CORPORATION. PRINTED IN THE UNITED
More informationAgilent 1290 Infinity II Vialsampler Data Sheet
Agilent 1290 Infinity II Vialsampler Data Sheet Agilent 1290 Infinity II Vialsampler Data Sheet Product Description The Agilent 1290 Infinity II Vialsampler is designed for UHPLC applications up to 1300
More informationModel K 5800 G Part No
K5800G Manual 11/30/01 5:02 PM Page 1 Model K 5800 G Part No. 1.194-103.0 High Pressure Washer Operator Manual Overview..................................1 Precautions...............................1-2
More informationThis document is a preview generated by EVS
TECHNICAL REPORT RAPPORT TECHNIQUE TECHNISCHER BERICHT CEN/TR 16468 March 2013 ICS 65.100.01; 67.050 English Version Food analysis - Determination of pesticide residues by GC-MS - Retention times, mass
More informationH-10PM. Refrigerant Leak Detector
H-10PM Refrigerant Leak Detector Congratulations! You have just purchased the most versatile, high performance service leak detector available in the industry today. It will detect refrigerants with a
More informationMass Spectrometry. Fundamental LC-MS. Vacuum Systems
Mass Spectrometry Fundamental LC-MS Vacuum Systems i Wherever you see this symbol, it is important to access the on-line course as there is interactive material that cannot be fully shown in this reference
More informationANNEX I. Technical specifications for: Supply of various Trace Explosive Detection Systems
EUROPEAN COMMISSION JOINT RESEARCH CENTRE Institute for Reference Materials and Measurements (Geel) ANNEX I Technical specifications for: Supply of various Trace Explosive Detection Systems TABLE OF CONTENTS
More informationRapidTrace + Automated SPE Workstation. Instruments. Accessories Racks Vial Adapters Test Tubes O-Rings Miscellaneous
RapidTrace + Automated SPE Workstation Instruments RapidTrace + Accessories Racks Vial Adapters Test Tubes O-Rings Miscellaneous Automate Your Extractions Increase your throughput and productivity The
More informationUNITY 2 TM. Air Server Series 2 Installation Manual. Version September 2012
UNITY 2 TM Air Server Series 2 Installation Manual Version 1.12 September 2012 1. Installation...2 1.1. Tools required...2 1.2. Procedure...2 1.3. Requirement for a sample pump (U-ASPMP1 / U-ASPMP2)...8
More informationPerkin Elmer Clarus 500 Gas Chromatograph
IET International Equipment Trading, Ltd. www.ietltd.com Proudly serving laboratories worldwide since 1979 CALL +847.913.0777 for Refurbished & Certified Lab Equipment Perkin Elmer Clarus 500 Gas Chromatograph
More informationINSTALLATION. and INSTRUCTION MANUAL. for QUALITY AIR BREATHING SYSTEMS. Model ABM - 715
INSTALLATION and INSTRUCTION MANUAL for QUALITY AIR BREATHING SYSTEMS Model ABM - 715 M A R T E C H S E R V I C E S C O M P A N Y P.O. Box 7079 OFFICE: 800-831-1525 Mazeppa, MN 55956 Fax : (507)843-4953
More informationWater Distiller Service Manual
Water Distiller Service Manual Water Distiller Service Manual L70478WT 2008 Regal Ware, Inc. Table of Contents RECOMMENDED TOOLS... 2 GENERAL INSPECTION...3 BOILING CHAMBER TROUBLESHOOTING & REPAIRS Description...
More informationFundamentals of Solid-Phase Extraction (SPE): Principles and Practical Tips for Developing Sample Preparation Methods
Thank you for joining us! The Webinar will begin shortly. Fundamentals of Solid-Phase Extraction (SPE): Principles and Practical Tips for Developing Sample Preparation Methods 2013 Waters Corporation 1
More informationK 3.97 M. Specifications or visit our website: In USA call: Part No
K 3.97 M High Pressure Washer Operator Manual Overview... 2 Precautions... 2-4 Assembly Instructions... 4-5 Operating Instructions... 5-6 GFCI Instructions... 6 Using the Accessories... 6 Working with
More informationCentrifugal Vacuum Concentrators and Cold Traps
Centrifugal Vacuum Concentrators and Cold Traps 2 Ce n t r iva p Va c u um Co n c e n t r ato r s & Co l d Tr a p s Page An Overview 2 CentriVap micro IR Vacuum Concentrators 4 CentriVap Benchtop Vacuum
More informationQAQC LABS ANALYTICAL DRYING
WHAT IS FLUID BED? By forcing enough air through a bed of particles, the particle bed may assume a fluid-like state (resembling a boiling liquid). Heating the incoming air and managing air flow rate through
More informationCALIDUS tm the Modular micro Gas Chromatograph
CALIDUS tm the Modular micro Gas Chromatograph Sample Processing Unit Plug & Play Programmed Temperature Column Modules Plug & Play Detector Modules Flame Ionization Thermal Conductivity A CALIDUS micro
More informationModel K 520 M Part No
Model K 520 M Part No. 1.069-680.0 High Pressure Washer Operator Manual Overview... 2 Precautions... 2-4 Assembly Instructions... 4 Operating Instructions... 5 Using the Accessories... 6 Working with Detergents...
More informationArtisan Technology Group is your source for quality new and certified-used/pre-owned equipment
Artisan Technology Group is your source for quality new and certified-used/pre-owned equipment FAST SHIPPING AND DELIVERY TENS OF THOUSANDS OF IN-STOCK ITEMS EQUIPMENT DEMOS HUNDREDS OF MANUFACTURERS SUPPORTED
More informationProduct Guide for Ludger Clean Post-endoglycosidase and Post-exoglycosidase Clean-up Plate
Product Guide for Ludger Clean Post-endoglycosidase and Post-exoglycosidase Clean-up Plate Part of the Ludger-Velocity Fast Glycan Analysis Range. (Ludger Product Guide: LC-PBM-96) Ludger Document # LC-PBM-96-Guide-v2.0
More informationFREESTYLE SPE UNIQUE POSSIBILITIES FOR SOLID PHASE EXTRACTION
FREESTYLE SPE UNIQUE POSSIBILITIES FOR SOLID PHASE EXTRACTION ONE DEVICE MANY OPTIONS Modular and amazingly independent. The FREESTYLE system is a fully automated sample preparation system for the unsupervised
More informationDacor Technical Service
Attention: This manual is just a section from the complete Wall Oven Service Manual. If you find that you require the complete service manual, which includes exploded views and parts, use and care information
More informationAgilent 1290 Infinity II Online SPE Solution
Agilent 1290 Infinity II Online SPE Solution Instruction Agilent Online-SPE-Solution - Instruction Technical Information about the Agilent Online-SPE-Solution (optional setups with: G4242A Online-SPE Starter
More informationRev B, 9/2/2009. Kodiak Chiller Overview
930-0001 Rev B, 9/2/2009 Kodiak Chiller Overview Presentation Outline Phone: 781-933-7300 Lytron Technical Support Contact Information 3 Introduction 4 Part I: Unpacking 5 Part II: Installation 7 Part
More informationOWNER S MANUAL FOR AIR ADMIRAL VACUUM/PRESSURE STATION MODELS:
OWNER S MANUAL FOR AIR ADMIRAL VACUUM/PRESSURE STATION MODELS: 79202-00 79202-05 79202-30 79202-35 Approval Agency s Model 79202-00 & 79202-05 Model 79202-30 & 79202-35 Not recommended for pumping acid,
More informationAP Air Ion Counter Instructions
AP Air Ion Counter Instructions Standard 2 million ions/cm 3 version- The 6 m long ground cord should be used to connect the meter to earth ground for most types of measurements - - especially if you are
More informationElectric Pressure Washer
Electric Pressure Washer English..... 4 Español... 20 Français... 38 K1700 CUBE 1.106-113.0 K1710 CUBE 1.106-116.0 8.638-793.0-A 12/16 Machine Parts List 1. Water Inlet 2. High Pressure Outlet 3. Hose
More informationANALOX 5001 Carbon Dioxide Monitor. User Manual ANALOX Analox 5001 Carbon Dioxide Monitor User Manual
ANALOX 5001 ANALOX 5001 Carbon Dioxide Monitor User Manual Analox Sensor Technology Ltd 15 Ellerbeck Court, Stokesley Business Park North Yorkshire, TS9 5PT T: +44 (0)1642 711400 F: +44 (0)1642 713900
More informationK Specifications. Max. Water Volume
K 2.75 High Pressure Washer Operator Manual Overview... 2 Precautions... 2-4 Assembly Instructions... 4 Operating Instructions... 5 Using the Accessories... 6 Working with Detergents... 7 Shut Down and
More informationBARRINGTON PRESSURE LITE VITREOUS CHINA SIPHON JET TOILET K-4327
BARRINGTON PRESSURE LITE VITREOUS CHINA SIPHON JET TOILET K-4327 BEFORE YOU BEGIN INSTALLER HAZARD NOTIFICATION WARNING: Risk of injury or water damage. Contents of vessel under pressure can cause severe
More informationNEW Restek Electronic Leak Detector
RESTEK INNOVATION NEW Restek Electronic Leak Detector Why allow a tiny leak become a GIANT problem? Chromatography Products www.restek.com NEW Restek Electronic Leak Detector Ever have a small leak turn
More informationStandard Operating Procedure Gas Chromatograph Mass Spectrometry (GC/MS) - Agilent 7890B GC & 240 Ion Trap MS
Standard Operating Procedure Gas Chromatograph Mass Spectrometry (GC/MS) - Agilent 7890B GC & 240 Ion Trap MS The Agilent 7890B is a state-of-art gas chromatograph (GC) that provides superior performance
More informationModel K 240 plus Part No
Model K 240 plus Part No. 1.223 585.0 High Pressure Washer Operator Manual Overview... 2 Precautions... 2-4 Assembly Instructions... 4 Operating Instructions... 5 GFCI Instructions... 6 Using the Accessories...
More informationSimplicity. Reliability. Performance. Stratum. Automated VOC Sample Prep System
Simplicity Reliability Performance Stratum Automated VOC Sample Prep System The Stratum Purge and Trap Concentrator (PTC) is a sample preparation instrument used to remove Volatile Organic Compounds (VOCs)
More informationUSER S INFORMATION MANUAL
USER S INFORMATION MANUAL HOT WATER HEATING BOILERS DOMESTIC WATER HEATERS 150,000-300,000 Btu/hr MODELS EB-EWU-02 IMPORTANT INSTALLER - AFFIX INSTALLATION MANUAL ADJACENT TO THE BOILER CONSUMER - RETAIN
More informationGAS CHROMATOGRAPHY PURDUE UNIVERSITY INSTRUMENT VAN PROJECT. DEMYSTIFICATION ACTIVITY FOR THE GAS CHROMATOGRAPH (Revised: ) INTRODUCTION
INTRODUCTION DEMYSTIFICATION ACTIVITY FOR THE GAS CHROMATOGRAPH (Revised: 1-24-93) Gas chromatography (GC) is a very powerful tool for separating components of a mixture. The GC utilizes the physical and
More informationModel gffoz Process Ozone Sensor (In-Line)
Date ECO# Rev Description Originator 9/15/97 1.0 First Publication DB 10/8/97 2.0 Miscelaneous corrections DB 10/28/97 3.0 Minor changes BM 5/1/98 3.1 Added CE compliance BM TM IN USA, INCORPORATED 87
More information22 The Flame Ionization Detector
22 General Information FID pneumatics Special considerations Conditions that prevent the detector from operating Detector shutdown Jets Automatic reignition Lit offset Procedure: Changing the auto-reignite
More information451 Black Forest Road Hull, IA Ph: (712) Fax: (712) TS g/hr Turnkey Ozone Generation System
451 Black Forest Road Hull, IA 51239 Ph: (712) 439-6880 Fax: (712) 439-6733 TS-40 40 g/hr Turnkey Ozone Generation System Installation and Operation Manual TS-40 Manual Cautions, Warnings and Hazards
More informationTG-10 Wall Mount Installation and Operation Manual. High Output Ozone Generator
TG-10 Wall Mount Installation and Operation Manual High Output Ozone Generator Ozone Solutions 451 Black Forest Road Hull, IA 51239 Phone: (712) 439-6889 Fax: (712) 439-6733 2 Table of Contents Safety
More informationThe Complete and Easy Guide to Configuring Your Specific Thermo NanoLC for Mass Spec Analysis
The Complete and Easy Guide to Configuring Your Specific Thermo NanoLC for Mass Spec Analysis September 2013, Version 2 The world leader in serving science Content Selection Tree EASY-nLC 1000 Slide 3
More informationK 2.97 M. Specifications Operating pressure, max PSI Water volume GPM Voltage V Amp draw AMPS
K 2.97 M High Pressure Washer Operator Manual Overview... 2 Important Precautions... 3-4 Assembly Instructions... 4 Operating Instructions... 5 GFCI Instructions... 6 Using the Accessories... 6 Working
More informationVariable Temperature Microprobe Systems
Variable Temperature Microprobe Systems the world s resource for variable temperature solid state characterization 2 The Variable Temperature Microprobe System The variable temperature microprobe system
More informationAIR CONDITIONING. Carrier Corporation 2002 Cat. No
AIR CONDITIONING Carrier Corporation 2002 Cat. No. 020-016 1. This refresher course covers topics contained in the AIR CONDITIONING specialty section of the North American Technician Excellence (NATE)
More informationcussons Refrigeration Assembly Range TECHNOLOGY REFRIGERATION AND AIR CONDITIONING CUSSONS TECHNOLOGY LABORATORY RECOMMENDATION
REFRIGERATION AND AIR CONDITIONING CUSSONS LABORATORY RECOMMENDATION Cussons Refrigeration laboratories are offered to provide teaching to a range of different skill levels. In all the laboratories teaching
More informationModel K 330 M Part No
Model K 330 M Part No. 1.994-916.0 High Pressure Washer Operator Manual Overview..................................1 Precautions...............................1-3 Assembly Instructions.........................3
More information1 L Rotary Vacuum Evaporator Instruction Manual
1 L Rotary Vacuum Evaporator Instruction Manual Important This manual is designed for safe and optimal performance of this unit Please read manual carefully before operating this unit Keep this manual
More informationReacti-Therm I and III Heating Modules
INSTRUCTIONS Reacti-Therm I and III Heating Modules TS-18822 TS-18824 Number TS-18822 TS-18824 Description Reacti-Therm I Heating Module (single block) Reacti-Therm III Heating Module (triple block) 2101.1
More informationLIQUIDATOR Electronic Ionization System
LIQUIDATOR Electronic Ionization System Operation and Installation Manual LIQUITECH LIQUIDATOR Series Electronic Controller Unit LIQUITECH Model QLTF Flow Cell LiquiTech, Inc. 421 Eisenhower Lane South
More informationService Manual Model 3163
Service Manual Model 3163 Contents Important Safety Information.......... 1 Specifications.................. 2 General Information.............. 2 Direct Vent Requirements........... 2 Propane System................
More informationDissolved Oxygen Sensors
Instruction Sheet PN 51A-HxDO/rev.E July 2005 Models Hx438 and Gx448 Dissolved Oxygen Sensors For additional information, please refer to the Instruction Manuals CD shipped with this product, or visit
More informationTraining Fees 4,000 US$ per participant for Public Training includes Materials/Handouts, tea/coffee breaks, refreshments & Buffet Lunch.
Training Title ADVANCED GC PROCESS Training Duration 5 days Training Venue and Dates Advanced GC Process 5 17 21 February, 2019 $4,000 Dubai, UAE Trainings will be conducted in any of the 5 star hotels.
More informationThermo-Finnigan LCQ Interface Manual
Thermo-Finnigan LCQ Interface Manual For Thermo Finnigan LCQ XP, Deca, Advantage, Duo, and Classic Models Version 20101129 IonSense Inc. 999 Broadway Suite 404 Saugus, MA 01906 Copyright 2005-2010 by IonSense
More informationGetz Equipment Innovators 450 lb Dual Portable Dry Chemical Fill System
Getz Equipment Innovators 450 lb Dual Portable Dry Chemical Fill System 1 Revised 11/18/10 2320 Lakecrest Drive, Pekin IL 61554 PH. (888) 747-4389 Fax (309) 495-0625 Website: www.getzequipment.com LIMITED
More informationACQUITY UPLC H-Class Column Compartments Operator s Overview and Maintenance Information
ACQUITY UPLC H-Class Column Compartments Operator s Overview and Maintenance Information Revision B Copyright Waters Corporation 2010 All rights reserved Copyright notice 2010 WATERS CORPORATION. PRINTED
More informationWaters Xevo G2-S QTof Operator s Overview and Maintenance Guide
Waters Xevo G2-S QTof Operator s Overview and Maintenance Guide 715003596 Revision B Copyright Waters Corporation 2013 All rights reserved Copyright notice 2011 2013 WATERS CORPORATION. PRINTED IN THE
More informationK Specifications. Max. Water Volume
K 2.35 High Pressure Washer Operator Manual Overview... 2 Precautions... 2-4 Assembly Instructions... 4 Operating Instructions... 5 Using the Accessories... 6 Working with Detergents... 7 Shut Down and
More informationInjection/Trapping. Analysis
High flow pump, two split system 2 waste position 9 0-0 µl/min 4 7 - µl/min 6 Injection/Trapping.-2.kV 8 detector position 200-00 µl/min Analysis 200-00 nl/min.-2.kv 2/20/20 University of Washington Proteomics
More information150 & 200 RT MG-SERIES GAS FIRED DOUBLE-EFFECT EFFECT ABSORPTION CHILLER-HEATER
GUIDE SPECIFICATIONS 150 & 200 RT MG-SERIES GAS FIRED DOUBLE-EFFECT EFFECT ABSORPTION CHILLER-HEATER HEATER 1. General Description The Contractor shall furnish and install (Qty) Yazaki model CH- Gas Fired,
More informationInstruction Manual for FORMALDEHYDE GAS DETECTOR MODEL FP-30/FP-40
Instruction Manual for FORMALDEHYDE GAS DETECTOR MODEL FP-30/FP-40 This instrument is sold and serviced by RKI Instruments, Union City, CA For questions, parts, or service please contact RKI at (800) 754-5165.
More informationINSTALLATION. and INSTRUCTION MANUAL. for QUALITY AIR BREATHING SYSTEMS. Model ABM - 700
INSTALLATION and INSTRUCTION MANUAL for QUALITY AIR BREATHING SYSTEMS Model ABM - 700 M A R T E C H S E R V I C E S C O M P A N Y P.O. Box 7079 OFFICE: 800-831-1525 Mazeppa, MN 55956 Fax : (507)843-4953
More informationPOWDER GUIDE. Trouble shooting tips to maximise the benefits of Apcoshield Powder Coatings
POWDER GUIDE From ASIAN PAINTS (I) LTD Trouble shooting tips to maximise the benefits of Apcoshield Powder Coatings Section A : Powder Application Problems Trouble Possible Causes Solutions 1. Poor charging
More informationFigure 1-1 Furnace Front Elevation
FURNACE EQUIPMENT 1.1 Furnace Description The LA-306 is a compact, near-infrared, conveyor belt furnace for laboratory and general purpose thermal processing in the range of 100-980 ⁰C in a controlled
More informationFisher Scientific Model 281A Vacuum Oven. Installation and Operating Manual Rev. 0
Fisher Scientific Model 281A Vacuum Oven Installation and Operating Manual 30979 Rev. 0 Preface Models covered in this manual: Catalog numbers Models numbers Voltage 13-262-50 6288 120V 13-262-51 6289
More informationUndercounter Refrigerator Operation Manual i.series and Horizon Series
Undercounter Refrigerator Operation Manual i.series and Horizon Series Blood Bank Models i.series: ib105 (Version B) Horizon Series: HB105 (Version B) Laboratory/Pharmacy Models i.series: ilr105 (Version
More informationπ H-6369, H-6370 DEHUMIDIFIER GENERAL INFORMATION uline.com WATER IN THE BUCKET RECOMMENDED HUMIDITY LEVELS WARM AIR EXHAUST IS NORMAL
π H-6369, H-6370 DEHUMIDIFIER 1-800-295-5510 uline.com GENERAL INFORMATION RECOMMENDED HUMIDITY LEVELS Spring/Summer: 35% - 50% Fall/Winter: 35% - 40% WARM AIR EXHAUST IS NORMAL During operation your dehumidifier
More information