Rotary Evaporator Replacement Glassware

Transcription

1 Rotary Evaporator Replacement Glassware from Ace Glass Ace Glass, founded in 1936, continues our long tradition of manufacturing high quality specialty glassware. We would like to introduce a new, comprehensive line of glassware to fit today s popular rotary evaporators. This brochure outlines the more widely used glassware sets and component parts to replace your existing glass. Ace also offers both custom glass and glass repair services for rotary evaporators. Ace Glass rotary evaporator replacement glass, all manufactured in the USA to exacting specifications and standards.

2 2 Rotary Evaporator Replacement Glassware Condenser C Assembly for Buchi Rotary Evaporators (Poly Coated) (Non-Coated) Fits Buchi Models 200/205 and Series Glassware can be ordered either clear poly coated or standard non-coated. The C Assembly contains the main glass outer trap body with a 35/20 inner ball joint bottom connection that attaches to the receiver flasks (which are sold separately). Features standard top and side flange that connects directly to the Buchi rotary evaporator. Assembly C also includes the glass cold trap inner body, Buchi Part #00672, PTFE sealing ring with Viton O-rings, PTFE lid or cap, PTFE hose barbs and GL threaded caps (Poly Coated) (Non-Coated) (Poly Coated) (Non-Coated) C Assembly Poly Coated Description Buchi Part # Order Code Each Complete C Assembly , Complete C Assembly. Also includes 1 x 1000mL receiving flask, stainless , steel clamp Poly Coated Components Outer trap body only C Assembly Non-Coated Complete C Assembly Complete C Assembly. Also includes 1 x 1000mL receiving flask, stainless , steel clamp Individual Components Non-Coated Outer trap body only Cold trap inner body PTFE Lid PTFE seal ring with Viton O-ring Stopcock/Bottom Stopcock/Top /32 joint adapter (without clip) Stainless steel clamp Glass steam tube (part of Buchi #40016) See page six for individual flask listings Ordering & Product Information: Subject to Ace Discount Net

3 Rotary Evaporator Replacement Glassware (Poly Coated) (Non-Coated) Condenser CR Assembly for Buchi Rotary Evaporators Fits Buchi Models 200/205 and Series Assembly is very similar to C Assembly except that the bottom joint is 45/40 inner to fit into separate distribution head. Complete CR Assembly includes main glass cold trap outer body, glass cold trap inner body, PTFE cap, PTFE seal ring with Viton O-rings, GL thread caps and hose barbs (Poly Coated) (Non-Coated) (Poly Coated) (Non-Coated) CR Assembly Poly Coated Description Buchi Part # Order Code Each Complete CR Assembly , Complete CR Assembly. Also includes 1 x 1000mL receiving flask, stainless , steel clamp Poly Coated Components Cold trap condenser body only Lower distribution head with shut-off valve CR Assembly Non-Coated Complete CR Assembly , Complete CR Assembly. Also includes 1 x 1000mL receiving flask, stainless , steel clamp Individual Components Non-Coated Cold trap condenser body only Lower distribution head with shut-off valve Cold trap inner body PTFE Lid PTFE seal ring with Viton O-ring Stopcock/Distribution Head Stopcock/Top /32 joint adapter (without clip) Stainless steel clamp Glass steam tube (part of Buchi #40016) See page six for individual flask listings (Poly Coated) (Non-Coated) For Engineering Support, visit

4 4 Rotary Evaporator Replacement Glassware Condenser A Assembly for Buchi Rotary Evaporators (Poly Coated) (Non-Coated) Fits Buchi Models 200/205 and Series Complete A Assembly includes main glass condenser body with inner coil for angled installation, O-ring, GL thread caps and hose barbs. Bottom joint is 35/ (Poly Coated) (Non-Coated) A Assembly Poly Coated Description Buchi Part # Order Code Each Complete A Assembly 40633/ Complete A Assembly. Also includes 1 x 1000mL receiving flask, stainless steel clamp A Assembly Non-Coated Complete A Assembly Complete A Assembly. Also includes 1 x 1000mL receiving flask, stainless steel clamp Individual Components Non-Coated 29/32 joint adapter (without clip) Stopcock/Top Stainless steel clamp Glass steam tube (glass part of Buchi #40016) See page six for individual flask listings Custom work or repairs needed? Call Ace Glass at Ordering & Product Information: Subject to Ace Discount Net

5 Rotary Evaporator Replacement Glassware (Poly Coated) (Non-Coated) Condenser V Assembly for Buchi Rotary Evaporators Fits Buchi Models 200/205 and Series Complete V Assembly includes main glass vertical condenser body with inner coil, O-ring, GL thread caps and hose barbs. Bottom joint is 35/ (Poly Coated) (Non-Coated) V Assembly Poly Coated Description Buchi Part # Order Code Each Complete V Assembly 40603/ Complete V Assembly. Also includes 1 x 1000mL receiving flask, stainless steel clamp V Assembly Non-Coated Complete V Assembly Complete V Assembly. Also includes 1 x 1000mL receiving flask, stainless steel clamp Individual Components Non-Coated 29/32 joint adapter (without clip) Stopcock/Bottom Stainless steel clamp Glass steam tube (glass part of Buchi #40016) See page six for individual flask listings See the Ace Glass Catalog for a complete listing of rotary evaporators and glassware. For Engineering Support, visit

6 6 Rotary Evaporator Replacement Glassware Buchi Replacement Glass Components 3954 A A 3990/ Long Short Vapor Duct Tubes (without combi clip) Joint Fits Buchi Models Length, mm (A) For Assy. Buchi Part # Order Code Each 29/ A * / A * / V * / V * /32 R114-R A ** /40 R114-R A ** /42 R114-R A ** /32 R114-R V ** /40 R114-R V ** /42 R114-R V ** *Same as Buchi part numbers 48160, 48161, and 48164, except the above are without clip. **Same as Buchi part numbers 32340, 32342, 32344, 32339, 32341, 32343, except the above are without clip Joint Flask Adapters (without combi clip) Joint Fits Buchi Models Buchi Part # Order Code Each 29/ / / / Stopcocks Description Buchi Part # Order Code Each Stopcock/Bottom 40627/ Stopcock/Top 40628/ /6892 Evaporating Flasks Pear shaped with Joints Poly Coated, HEAVY WALL Joint Size, ml Buchi Part # Order Code Each 29/32 500mL / mL / mL /42 500mL / mL / mL /40 500mL / mL / mL Non-Coated, HEAVY WALL Joint Size, ml Buchi Part # Order Code Each 29/32 500mL / mL / mL /42 500mL / mL / mL /40 500mL / mL / mL Ordering & Product Information: Subject to Ace Discount Net

7 Rotary Evaporator Replacement Glassware Drying Flasks Pear shaped with side indents, neck joint Poly Coated, HEAVY WALL Joint Size, ml Buchi Part # Order Code Each 29/32 500mL / mL / mL /40 500mL / mL / mL Non-Coated, HEAVY WALL Joint Size, ml Buchi Part # Order Code Each 29/32 500mL / mL / mL /40 500mL / mL / mL , 6902 Receiving Flasks Single neck, round bottom Poly Coated, HEAVY WALL Joint Size, ml Buchi Part # Order Code Each 35/ mL 40775/ / mL 40776/ / mL 40777/ Non-Coated, HEAVY WALL Joint Size, ml Buchi Part # Order Code Each 35/ mL / mL / mL /6902 Buchi Replacement Glass Components If you don t see your part or component listed here, or if you need a custom component, call or Ace Glass and we ll be glad to make it for you. For Engineering Support, visit

8 8 Rotary Evaporator Replacement Glassware Rotary Evaporator Replacement Glass Components Large Evaporator Flasks Used with Heidolph 20 Liter Rotary Evaporators. These large flasks are fabricated from blanks selected for balance and quality. Necks are carefully welded to prevent rotational whip. Flasks can be plastic coated upon request. Cap., Overall Height, A Flange B C Liters mm O.D., mm I.D., mm mm Order Code Each Large Receiver Flasks Used with Heidolph 20 Liter Rotary Evaporators. This receiver flask is fabricated from blanks selected for balance and quality. Center neck is a polished 40/25 joint, side neck is a GL-18 thread, supplied with solid cap. At bottom is a 0-10mm easy action stopcock with a GL-18 side arm, supplied with a 3 / 8" hose connection tube. Flasks can be plastic coated upon request. Cap., Liters Overall Hght., mm Center Neck Side Neck Bottom Outlet Order Code Each /25 GL mm/GL Vapor Tubes for Heidolph 4000 Series Used as replacements with Heidolph 4000 Series Rotary Evaporators. Tube is secured in rotary drive with low-stress plastic clip that seats into groove behind joint. Available plain or with Firestone Splash Guard to protect against splash-up. Code -30 is supplied with evaporator. Type Joint Order Code Each Plain 24/ Plain 24/ Plain 29/ Plain 45/ w/splash Guard 24/ w/splash Guard 29/ Ordering & Product Information: Subject to Ace Discount Net

9 Rotary Evaporator Replacement Glassware 9 Large Evaporator Flasks For Buchi Rotavapor System Easy replacement select the size and capacity you need 6702 Large Evaporator Flasks These large flasks are fabricated from blanks selected for balance and quality. Necks are carefully welded to prevent rotational whip. Flasks can be plastic coated* upon request. Easy Order Instructions 1. Determine flange size (A) O.D., (B) I.D., (C) thickness (see diagram). 2. Match flask capacity with overall height and flange size. EVAPORATOR FLASK OVERALL HEIGHT C A B 1. Select Flange Size. A O.D., mm (Inches) B I.D., mm (Inches) C Thickness (mm) Flange Size Designation S (Small) 90 (3.5) 67 (2.7) 18 M (Medium) 100 (3.9) 72 (2.8) 19 L (Large) 110 (4.3) 83 (3.3) 23 EL (Extra Large) (5.9) (4.7) Select Flask Capacity and match with Flange Size. * Plastic coated flasks are transparent, and will withstand temperatures up to 100 C. The coating is resistant to the occasional laboratory solvent or acid splash, but should not be soaked in them. Avoid prolonged contact. Capacity, Liters Overall Height, mm Flange Size Order Code Each S M M L L EL S M M L EL M M L EL Special sizes can be made to order. Call or ACE GLASS for more information. For Engineering Support, visit

10 10 Rotary Evaporator Replacement Glassware Rotary Evaporator Replacement Glass Components Stopcocks with Inlet Feed Tube Used in Heidolph 4000 Series Rotary Evaporator condensers and other popular brand rotary evaporator condensers as inlet feed tube to allow continuous feed of volumes exceeding capacity of evaporating flask. Size is 19/38 with 6mm O.D. feed tube. Order Code Each Traps Rotary Evaporator, Boulanger, Self Washing Self-washing rotary evaporator trap designed by William A. Boulanger. Unique design incorporates an inverted, straight, heavy-walled expansion chamber that allows for flow-back of bumped materials. Condensation of evaporated solvent on walls of trap continuously rinses trap during operation. Vacuum stem has two opposing holes, flush with bottom of stem, to allow solvent vapor to rapidly flow out, while allowing condensed solvent to return to flask. This feature means the evaporator shaft is also continuously rinsed and the material returned to the flask. To prevent pooling of the condensate in the shaft trap, the end of the trap has a center hole for complete drainage. When solids are bumped onto the sides of the trap toward the end of solvent evaporation, introduction of a small amount of solvent at top of trap with a swirling motion effectively rinses the material back into the flask. Capacity, Top Outer Bottom Inner ml Joint Joint Order Code Each /40 14/ /40 24/ /40 14/ /40 24/ /42 29/ Ordering & Product Information: Subject to Ace Discount Net

11 Rotary Evaporator Replacement Glassware Traps Rotary Evaporator, Anti-Splash Greatly reduces carry-over from foaming or bumping. Capacity, Top Outer Bottom Inner Approx. Overall ml Joint Joint Height, mm Order Code Each /40 14/ /40 24/ /42 14/ /20 14/ /40 24/ /42 29/ /40 24/ Traps Rotary Evaporator, Anti-Splash, Improved Greatly reduces carry-over from foaming or bumping. Two drain holes, close to base of the inner tube, allow solvent to drain back into evaporator flask. Capacity, Top Outer Bottom Inner Approx. Overall ml Joint Joint Height, mm Order Code Each /40 14/ /40 24/ /20 14/ /40 24/ /42 29/ /40 24/ Traps Rotary Evaporator, Anti-Climb Upper tubulation prevents migration of film and foam directly into the condenser. Capacity, Top Outer Bottom Inner Approx. Overall ml Joint Joint Height, mm Order Code Each /40 14/ /40 24/ /40 14/ /40 24/ /42 29/ Rotary Evaporator Replacement Glass Components For Engineering Support, visit

12 12 Rotary Evaporator Replacement Glassware Rotary Evaporator Replacement Glass Components Adapters Vial or Bottle, PTFE Used to connect a vial or a bottle to the vapor tube of a rotary evaporator. Fabricated from PTFE, one side is an outer joint with rib for using clamp such as 7598, other end is a outer vial or bottle thread. Joint Thread Size Order Code Each 24/ / / / Adapters Splash Guard, with Fritted Disc, Firestone* medium length joints, top and bottom, that will accept full length joints, plus a coarse porosity A ( µ) fritted disc that assures no carry-over in the event of pot splash-up. Overall length is kept to a minimum to effect best distillation. Top Outer Joint Bottom Inner Joint Order Code Each 24/25 24/ /25 29/ /25 45/ *Designed by Dr. Raymond Firestone (U.S. Patent No. 4,267,150) 5258 Adapters Splash Guard, Firestone* medium length joints, top and bottom, that will accept full length joints. When inserted into flask, splash guard combines with flask neck to give best protection against pot splash up. Overall height is kept to a minimum to effect best distillation. Top Outer Joint Bottom Inner Joint Order Code Each 14/20 14/ /25 24/ *Designed by Dr. Raymond Firestone (U.S. Patent No. 4,267,150) Ordering & Product Information: Subject to Ace Discount Net

13 Rotary Evaporator Replacement Glassware Rotary Evaporator Firestone* Ingenious rotary evaporator constructed of glass or stainless steel, PTFE and glass-filled PTFE that operates without the devices normally associated with this type of equipment. Use with any lab stirring motor. Hollow glass or Stainless Steel (for larger capacity flasks) 10mm O.D. tube, with 14/20 or 24/40 at one end for flask and holes drilled near center for vacuum, attaches to laboratory stirring motor. Tube turns inside PTFE bearing held in #15 Ace-Threds by glass-filled PTFE bushing, compression saddle with O-ring and lock nut. 2mm straight bore stopcock attaches to drying tube and/or McLeod gauge. One arm of 4mm bore double oblique stopcock attaches to dry ice trap and vacuum line; other arm is for easy vacuum release and can be connected to a trap. Complete item supplied with joint clamp; does NOT include stirring motor, chuck, flask or splash guard. Instead of connecting motor directly, use ACE Flexible Shaft, to get heavy motor out of the way. Optional. For Flask Glass Shaft Stainless Steel Shaft Joint Order Code Complete Order Code Complete 14/ / *Designed by Dr. Raymond Firestone (U.S. Patent #4,569,724). A stainless steel shaft is available for heavier flasks Replacement Parts Order Code Each Glass Body, only Glass/PTFE Bushing, with O-ring, only (2) Glass/PTFE Lock Nut, only (2) Compression Saddle with O-ring, only (2) PTFE Bearing, only (2) Hollow Glass Tube, 14/ Hollow Glass Tube, 24/ Hollow S-S Tube, 14/ Hollow S-S Tube, 24/ Splash Guard, 14/ Splash Guard, 24/ Flexible Shaft, 91.4cm, Complete For a full selection of Rotary Evaporators from IKA and Heidolph, visit the Ace website at or see our GeneralCatalog Rotary Evaporator Replacement Glass Components For Engineering Support, visit

14 14 Rotary Evaporator Replacement Glassware Rotary Evaporator Replacement Glass Components New! 6893 Receiving Bottles/Flasks Graduated, round bottom receiving flasks for use as replacement receivers on all glassware sets. 250 ml size graduated in 10 ml increments; 1000 ml and 2000 ml in 100 ml increments. Joint is 35/20. Cap., ml Joint O.D., mm Lgth. below joint, mm Order Code Each / / / / Receiving Tubes/Cylinders New! Graduated, tapered bottom receiving tube for use as replacement receivers on all glassware sets. 100 ml size graduated in 0.5 ml increments from 0-10 ml; 5 ml increments from ml. Joint is 35/20. Cap., O.D., Lgth. below Order ml Joint mm joint, mm Code Each / Special Note: 35/20 and 35/25 spherical joint components are interchangeable. See the Ace Glass Catalog for a complete listing of rotary evaporators and glassware. Ordering & Product Information: Subject to Ace Discount Net

15 Rotary Evaporator Replacement Glassware Adapters Conversion Glass conversion adapter with 24/40 or 29/42 joint to #15 or #25. #15 is used with through -22 or through -134; #25 is used with or connecting adapter to connect vials or flasks to rotary evaporator. Suitable for vacuum work. Order each item separately. Joint Ace-Thred Order Code Each 24/40 # /40 # /42 # /42 # Adapters Connecting, PTFE PTFE connecting adapter with #15 or #25 Ace-Thred and GPI thread to connect , -37, -44 or -47 conversion adapter to matching vial for use in rotary evaporator. Suitable for vacuum work. Order each item separately. Note! FETFE not suitable for use with methylene chloride or acetone. Use Chemraz instead. With FETFE O-ring With Chemraz O-ring GPI Ace- Order Order Thread Thred Code Each Code Each # # # # # # # # Multipack Connecting Adapter Kit Convenience kit with several PTFE Ace-Thred to GPI thread adapters to fit various vial sizes version includes the -11 through -24 PTFE adapters listed above version includes the -121 through -134 PTFE adapters listed above. The kit also includes one #15 glass conversion adapter. Order Code Per Kit ACE Scientific Glass Repair Service ACE Custom Glass Design Service Rotary Evaporator Replacement Glass Components For Engineering Support, visit

16 0608 Prices and specifications are subject to change without notice P.O. Box 688 Vineland, NJ Fax: TOLL-FREE: FAX: