About Us. Technoforce has the best in the industry Pilot Plant test facilities in India and Europe.

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2 About Us Technoforce was started in 1990 to manufacture process equipment based on thin-film technology. Extractors and Crystallizers were added to the product range subsequently. The manufacturing facilities meet ASME U stamp,european PED CE- mark and China Special Equipment License requirements. We have satisfied customers in Europe, North America, Middle East, Africa, South East Asia and India. Technoforce has the best in the industry Pilot Plant test facilities in India and Europe.

3 Our Capabilities A broad range of technologies like Thin Film Evaporation, Drying, Short Path Distillation, Continuous Extraction, Centrifugal Stripping and Crystallization are available from a single source. Turnkey solutions in the form of modular skids can save months from your project schedules. We work very closely with customers at every stage. Our online customer service tools simplify communications during pilot plant trials and project execution. LAB STUDY Preliminary investigation for a sound trial plan PILOT PLANT TRIALS Optimizing process parameters PROCESS AND MECHANICAL DESIGN EQUIPMENT MANUFACTURING Thin film machines up to 50 sq. m PROJECT EXECUTION SKID MOUNTED SYSTEMS Structural frames, piping, pumps, vacuum systems, instrumentation, PLC + SCADA ERECTION AND COMMISSIONING AFTER SALES SERVICE

4 Pilot Test Centre We have well equipped Test Centers in India and The Netherlands, where pilot trials are conducted. The performance guarantee is backed by the trial results. We would typically request for 0.5 to 1 kg of feed material for preliminary investigation. Tests on Pilot Plant may require 50kg to 1000kg of material, depending on the application. Technical or commercial information received from our customers is controlled. Confidentiality agreements are executed whenever requested PILOT PLANT SETUP Agitated Thin Film Evaporator Short Path Distillation Unit Falling Film Evaporator Rising Film Evaporator Suppressed Boiling Evaporator Agitated Thin Film Dryer Liquid- Liquid Extraction Column Annular Centrifugal Extractor * Plug Flow Crystallizer* Multi-stage Centrifugal Stripper* UTILITIES AVALIABLE Thermic fluid: up to 300 C Steam: up to 10 bar Hot water: up to 90 C Cooling water Chilled water Brine: -10 C Vacuum: 70 mbar, 0.001mbar CONTRACT PROCESSING* A few hundred kg to several tones of material can be processed using our Short Path Distillation Setup on rent. Initially, trials are conducted in the Pilot Test Centre to optimize the operating conditions. This data also helps us to do costing and quote the charges for contract processing. The analytical backup involving wet chemistry, GC and HPLC is available to monitor the product quality. * Available only in the India pilot plant Test facility at Nashik, India Test facility at Chemelot, the Netherlands

5 Manufacturing Facility Technoforce has a square meter fully integrated manufacturing facility in Nashik, Maharashtra, India. Stainless Steels, Hastalloys, Alloy 20, Duplex Steel, Titanium can be the materials of construction. Rotary Equipment like Thin Film Evaporators can be made up to 50 square meters in size. The shops are audited under ASME U stamp, European PED CE- mark and China Special Equipment Manufacturing License HIGHLIGHTS Robotic Welding CNC Cutting and Machining Large Capacity Lathes Metal Testing, Metrological & Calibration facilities for quality control LARGE CAPACITY LATHES ROBOTIC WELDING 3D MODELLING SKIDS FABRICATION CNC MACHINING ORBITAL WELDING

6 Agitated Thin Film Evaporator An Agitated Thin Film Evaporator (ATFE), also known as Wiped Film Evaporator (WFE), consists of a jacketed shell precision machined from inside and a rotor having blades that maintain a close clearance from the shell. A feed distributor at entry point distributes the liquid in a thin film on the heated wall. The high speed rotor further spreads and intensely agitates the film as it flows down. The generated vapors flow countercurrently and get cleaned by an integrally mounted entrainment separator. The processing is completed in a few seconds. Our high viscosity units can handle products with viscosities of several million centipoise! Residence time of a few seconds with a narrow spread, an important feature for heat sensitive products Required evaporation is achieved in a single pass, avoiding product recirculation and possible degradation Scale formation on the heat transfer surface is avoided due to the intense agitation of the liquid film Excellent turn down capability Low product holdup, ideal for hazardous applications Operating pressure as low as 1 mbar and operating temperature up to 400 C Special designs for clean room applications Vacuum distillation of bulk drugs, intermediates, fine chemicals, glycols, used lubricating oils, fatty acids and their derivatives, rubber chemicals, amines and esters Concentration of bulk drugs Processing of oleoresins, enzymes, plant extracts, milk products, juices and sugars Stripping of silicone oils, pesticides, plasticizers and monomers Recovery of contaminated solvents and products from residues Paraformaldehyde and high viscosity applications like stripping of polymer melts Purification of biodiesel and recovery of glycerin Each component is subjected to detailed mechanical investigation

7 Short Path Distillation Unit A Short Path Distillation Unit (SPDU) is also called as Molecular Distillation Unit. It provides minimum pressure drop, permitting high vacuum operation up to mbar. It is distinguished from a standard Agitated Thin Film Evaporator by an internally mounted condenser. The vapor generated on the heated surface travels a very short distance to reach the condenser surface, thus eliminating pressure drop. The condensed distillate and concentrate are collected separately in the bottom section before they are taken out. Operating vacuum as low as mbar helps in distilling high boiling and heat sensitive products Residence time of a few seconds Required distillation achieved in a single pass Enhanced vacuum can lower boiling point by 100 to 150 C, as compared to ATFE Excellent for gently processing heat sensitive, high boiling products Low product holdup Excellent turndown capability Low power requirement Operating temperatures up to 400 C High vacuum distillation of Pharmaceuticals, bulk drugs, natural or synthetic vitamins, esters Epoxy resins, plasticizers, and stabilizers Fish oil, omega-3 fatty acids, fatty acid derivatives, glycerides, tocopherol and tocotrienols Fine Chemicals, silicone oils, and higher alcohols Re-refining of spent lube oil Purification of natural and synthetic waxes Product recovery from distillation column residues Impure Feed, Distilled Product and Residue

8 Agitated Thin Film Dryer An Agitated Thin Film Dryer (ATFD) has a centrally located rotor having closely fitting blades. It rotates in a precision-machined jacketed shell. The feed is converted into a thin film, which is intensely agitated due to action of the high-speed rotor. The feed material goes through phases of slurry, paste and wet powder, before coming out as a dry powder. We offer vertical, horizontal or combination dryers to take feed in solution, slurry, paste or wet powder form. The most energy efficient dryer in the market. Thermal efficiency exceeds 90% Indirect heating and drying in absence of air, particularly effective for oxygen sensitive products Full recovery of organic solvents Residence time of a few seconds, well suited for heat sensitive products Dust free powder of relatively higher bulk density Processing without dilution of feed Powder of uniform consistency, eliminating pulverizer from downstream step Operating pressure as low as 1mbar and temperature up to 400 C Continuous discharge system for free flowing powders from vacuum Drying Pharmaceuticals, bulk drugs and intermediates Dyes, pigments and intermediates Organic and inorganic salts Clean room applications Possibility of amorphous powders Recoveries Solvents and products from residue DMSO from salts Glycerin from salts and residue Organic solvents or products from salt bearing waste streams Slurry, Cake, Distillate and Powder

9 Rising Film Evaporator A Rising Film Evaporator (RFE) is a vertical shell and tube heat exchanger with a vapor liquid separator mounted at the top. The liquid to be concentrated is fed at the bottom of the heated tube bundle. As it receives the heat, the vapors generated lift the liquid upwards and push it on the wall as a film. The velocities generated by the vapor lift are quite high, giving good thermal performance. The balance liquid and vapor are separated in the vapor- liquid separator. Simple solution for concentration of liquids that are moderately heat sensitive Thermosiphon action due to boiling in vertical tubes eliminates the need for circulation pump Multiple effect arrangement provides better steam economy Trace quantities of suspended particles in the feed are tolerated Concentration of dilute solutions containing water and organic solvents in applications such as: Plant extracts in water or organic solvents As a reboiler to distillation column Economical alternative to falling film evaporator for moderate vacuum and moderately heat sensitive products

10 Falling Film Evaporator A Falling Film Evaporator (FFE) is a vertical shell and tube heat exchanger with a vapor- liquid separator mounted at the bottom. The liquid to be concentrated is fed at the top of the heated tubes and distributed in such a way that it flows down on the inside surface of the tubes as a thin film. As the film gets heated, the vapors generated flow co-currently. The drag of vapors increases the turbulence and improves heat transfer performance. The balance liquid and vapor are separated in the vapor- liquid separator. Small holdup ensures quick response to changes in operating conditions, quick start-up and an easy switchover Suitable for heat sensitive products Multiple effect arrangement for better steam economy Gentle evaporation, mostly under vacuum, with a short residence time in the evaporator Concentration of dilute solutions of heat sensitive products containing water or solvents in applications such as: Plant extracts in water or organic solvents As a reboilier to a distillation column Recovery of solvents from contaminants Purification of biodiesel Reduced size of Agitated Thin Film Evaporator with volume reduction by tubular evaporation.

11 Plug Flow Crystallizer Inside a Plug Flow Crystallizer (PFC), a shaft with uniquely arranged blades rotates within a shell. The product flows through in a nearly plug flow manner under uniform and gentle agitation. Multiple heating /cooling sections provide controlled temperature gradients and good control on primary nucleation. Gentle agitation minimizes secondary nucleation. Plug flow conditions provide uniform residence time, promoting narrow Crystal Size Distribution (CSD), which is important for improved purity and flowability. The most scientifically designed continuous crystallizer Runs continuously Can be used with high percentage of solids in slurries Easy conversion from batch operation to continuous operation Can also be used as a Scraped Surface Heat Exchanger for highly viscous products Heating and cooling of heat sensitive, viscous products and particulate laden products Continuous crystallization by cooling or evaporation Dewaxing Separation of isomers Purification of organic intermediates Narrow Crystal Size Distribution

12 Liquid- liquid Extraction Column A Liquid- liquid Extraction Column (LLEC) is used as a continuous option to batch extraction in kettles. A liquid feed is contacted with an immiscible solvent that exhibits preferential affinity towards desired components. At the outlet, we get an extract enriched with the desired component and the raffinate, the spent feed, containing very little of the desired component. A continuous LLEC has a series of mixers and settlers that offer 4 to 6 equivalent stages of separation. Up to 50% reduction in solvent usage and 70% reduction in power usage are possible Improved and consistent results Significant reduction in power, space and solvent loss Continuous operation, no supervision required Optimum design arrived at after simulation by Computational Fluid Dynamics (CFD) studies Separation of close boiling components, which are otherwise difficult to separate by distillation Breaking of azeotropes COD, BOD reduction in wastewater Purification of fine chemicals and pharmaceuticals Change in ph by washing Reactive extraction CFD simulation for optimum results

13 Annular Centrifugal Extractor An Annular Centrifugal Extractor (ACE) has a rotor basket spinning at a high speed. This promotes intensive mixing in the outside annular space where the two immiscible phases quickly reach an equilibrium. The mixture enters the inner volume of the rotating basket where high centrifugal force quickly separates the two phases. The extract and raffinate are discharged through separate outlets. Small holdup makes it suitable for quick switchover with batch integrity Liquids with low-density difference and emulsifying tendencies are successfully processed Continuous operation, no supervision required Quick switchover due to small holdup. Ideal for pharma application Up to 50 70% reduction in solvent and power use Requires less space Consistent results Very small holdup makes it ideal for hazardous applications Extraction of bulk drugs having small batch production cycle Separation of close boiling components, which are otherwise difficult to separate by distillation Breaking of azeotropes COD, BOD reduction in wastewater Purification of fine chemicals and pharmaceuticals Change in ph by washing Reactive extraction Extraction of fermentation products Extraction of hazardous products Extract Raffinate Solvent Feed Centrifugal Extractor - Sectional Drawing

14 Suppressed Boiling Evaporator A Suppressed Boiling Evaporator(SBE), also called as Forced Circulation Evaporator (FCE), has a vertical shell and tube heat exchanger as the calandria, a separator and a circulation pump for circulation of slurry though the tubes. Good velocity in the tubes and adequate hydrostatic head suppresses boiling inside the tubes. Therefore, scaling on the tube surface is minimized. Thanks to our axial flow pump, Technoforce evaporators out-perform the competition when it comes to reduced scaling Axial flow pump ensures high tube velocities with minimum power consumption Carefully balanced flow and hydrostatic head truly suppress boiling and scaling in the tubes Generously sized flash separator minimizes entrainment, resulting in a clear distillate Preconcentration of scale prone liquids before drying Multiple effect arrangement for reduction in the steam requirement Wastewater concentration for volume reduction Concentration of solution having organic and inorganic salts Evaporative crystallization Axial Flow Pump These pumps are designed for high flow against low head. They are used with a great advantage in closed loop circulation where the pump casing becomes merely an elbow in the circulation line. Axial flow pumps deliver 5 times more flow as compared to centrifugal pumps using the same horsepower The high efficiency impellers are developed using Computational Fluid Dynamics (CFD) simulation techniques and machined on a CNC machining center. The pump performance is validated on a test rig. State of the art impleller perfected with CFD simulations

15 Zero Discharge Systems Multiple Effect Evaporator Technoforce offers Multiple Effect Evaporator (MEE) systems with a stripper, thermo compressor, axial flow pump and sludge dryer. Our objective is to save your operating and disposal costs, and minimize scaling in evaporators. Multiple effects and thermocompressor reduce steam consumption Minimum power requirement due to the use of our state-of the-art axial flow pumps Stripper isolates volatile organics and reduces COD Sludge dryer converts TDS to dry powder Modular skid mounted systems reduce the site activity to a few weeks Effluent wastewater concentration Concentration of organic and inorganic solutions bearing salts Evaporative crystallization Sludge Dryers Technoforce Sludge Dryers convert effluent slurries into a dry powder mass in a single step Indirectly heated. No air required No dusting, smell and air pollution issues which are typically associated with spray or flash dryers Thermal efficiency of over 90% Continuous discharge of free flowing solids Total recovery of water Less space required Our sludge dryers are in operation for the last 20 years. Powder from Sludge Dryer Multiple Effect Evaporator skid

16 Works Technoforce Solutions (I) Pvt Ltd D 33, MIDC Industrial Area, Ambad Nashik , India T +91 (0) / Sales Office Technoforce Solutions (I) Pvt Ltd 1107, Universal Majestic, PL Lokhande Marg Ghatkopar Mankhurd Link Road, Govandi, Mumbai , India T +91 (0) / 117 sales@technoforce.net` EU Pilot Plant Technoforce Solutions BV Chemelot Campus (Gate 2), Urmonderbaan 22, 6167 RD, Geleen, The Netherlands T +31 (0) ppeu@technoforce.net