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Contact person Alen Rakovic 2015-08-28 5P05551 1 (19) Fire Research +46 10 516 51 37 Alen.Rakovic@sp.se PcP. Durk Sverige AB Ruskvädersgatan 3B 418 34 Göteborg Fire Testing of fire protection gratings Type LHD (Appendicies 1) Postal address Office location Phone / Fax / E-mail This document may not be reproduced other than in full, except with the SP Västeråsen +46 10 516 50 00 prior written approval of SP. Box 857 Brinellgatan 4 +46 33 13 55 02 SE-501 15 BORÅS SE-504 62 BORÅS info@sp.se Sweden

2015-08-28 5P05551 2 (19) Table of Content 1 Introduction... 3 2 Fire test... 3 2.1 Experimental setup... 3 2.1.1 Fire protection gratings... 7 2.2 Experimental protocol... 9 3 Result and discussion... 12 3.1 Visual observations... 12 3.2 Gas temperatures... 14 3.3 O 2 concentration... 17 4 Conclusion... 18 References... 19

2015-08-28 5P05551 3 (19) 1 Introduction A review of national and international standards and guidelines shows that several documents address the problem of a fire in leaking transformer oil to various degrees but with no specific performance requirement [1] [2] [3] [4]. A traditional method for improving fire safety at transformer stations is to fill the transformer pit with gravel. In the Swedish standard SS 421 01 01 [5] it is written (translated to English below): Preferably arrangements that contribute to extinguish the fire in the leaked liquid shall be used, for example the use of a layer of stones (approximately 300 mm deep and with a grain size of about 40/60 mm) that extinguishes the burning liquid that enters the layer. There is a lack of a technology neutral requirements concerning the performance of the arrangement described above that should contribute to extinguish the fire of leaking flammable fluid. Fire protection gratings is one technology that has been developed for these purpose. This report presents quantitative tests of a specific scenario, simulating a transformer rupture where the burning transformer oil is rapidly flowing into the transformer pit. The tests are performed in order to investigate how well PcP.s fire protection grating Type LHD is able to extinguish the fire under these specific conditions. The test scenario was developed and tested 2013 by SP as described in SP report 2013:09 [6]. 2 Fire test The scenario modeled correlates to a sudden accidental release and ignition of large oil quantities from a transformer. The maximum stipulated temperature increase inside the transformer under normal conditions is 60 C [6]. The oil temperature is not expected to exceed 90 C, thus the oil temperature was increased to 90 C in this test before ignition. The amount of oil corresponds to a depth of 3 cm in the pit. The fire test was performed two times - both times under same conditions. The test should not be regarded as representative for all possible failure scenarios. 2.1 Experimental setup The transformer pit was 3.75 meters by 3.2 meters and 1 meter deep. The pit is built in concrete at PcPs facilities in Vildbjerg (Denmark). During tests the oil was stored in a tippable cart with a total volume of 600 liters. Transformer oil used in the tests was the Nynas Transformer Oil Nytro 10XN. Technical data sheet for the oil is attached in Appendix 1. Sketches and photo of transformer pit and placement of measuring instruments are presented in Figure 1 to 3. The temperature measurement was conducted with five thermocouple piles. The thermocouple piles are named A-E and their location are shown in Figure 1. Each pile contained six thermocouples at 1, 20, 50, 75, 90 and 130 cm above the ground level. Fire protection gratings ware installed at 0.80 m from the ground, i.e. the thermocouples at 90 cm and 130 cm were located above the fire protection gratings. Gas sampling for O 2 analysis was conducted at two positions, at the center of the pit and at 1 m from the back end of the pit, as shown in Figures 1 and 2. The inlet of the gas sampling pipe was located 10 cm below the fire protection gratings. The symbols in the figures represents: - O are the thermocouple trees, placed at the positions A-E. - X are the locations of the gas sampling pipes, placed 10 cm below the fire protection gratings.

2015-08-28 5P05551 4 (19) Figure 1. Top view of the experimental setup. Figure 2. Side view of the experimental setup.

2015-08-28 5P05551 5 (19) Figure 3. Photo of the test setup. The fire protection gratings were placed resting 80 cm from the ground level between angle bars installed on the pit inner frame and I-beam (HEB 140) placed in the middle of the longitudinal direction of the longest side of the pit as shown in Figure 4 and Figure 5. Figure 4. Fire protection gratings resting on angle bars.

2015-08-28 5P05551 6 (19) Figure 5. Fire protection gratings resting on I-beam (HEB 140) placed in the middle of the longitudinal direction of the longest side of the pit. A shield made of metal sheet was placed on the opposite side of the tipping cart to avoid oil spillage outside the pit due to the wave caused by the rapid release of oil into the transformer pit, Figure 6.

2015-08-28 5P05551 7 (19) Figure 6. Shield placed on the opposite side of the tipping trailer to avoid spillage of the burning oil due to the wave front. 2.1.1 Fire protection gratings Figure 7 shows a photo of a single grating board. It is manufactured from hot-galvanised sheet-metal. Four individual 3 mm thick sheet steel panels are welded together to form a grating board. The board has perforated surface structure. According to the manufacturer, the perforation ratio is about 4.1 % of the total surface. Each panel consists of six rows of holes, shown in Figure 7. Four of the rows are punched in the way that they form a shape of upward cone and remaining two rows are punched in the way that they form a shape of downward cone, shown in Figure 8. The holes have a diameter of 8 mm and are distributed on a centered rectangular lattice with nearest neighbor distance 25.5 mm and next nearest neighbor distance 36 mm, seen in Figure 9.

2015-08-28 5P05551 8 (19) Figure 7. PcP. fire protection grating board. Figure 8. Four of the rows are punched upwards and two rows are punched downwards.

2015-08-28 5P05551 9 (19) Figure 9. Perforation spacing is 25.5 mm between nearest neighbors and 36 mm between next nearest neighbors. 2.2 Experimental protocol The test was performed two times - both times under same conditions. Each test started with filling the tippable trailer with 370 liter transformer oil, the amount that corresponds to depth of 3 cm for the pit used in the test. The oil was then heated with an electric heater combined with external gas burners. When the temperature of 90 C was reached, the oil was ignited with a gas burner as shown in Figure 11. After 1:30 (min:sec) pre-burn time the oil was tipped into the transformer pit. Figure 11 shows the burning oil before tipping the oil into the pit. Figure 12 shows the sequence when the oil is tipped into the transformer pit. Important experimental parameters are listed below: - 370 liter of oil - Heated to 90 C before ignition - 0:00 (min:sec) - Start of measurement - 2:00 (min:sec) - Ignition of oil - 3:30 (min:sec) - Tipping of the burning oil into the pit

2015-08-28 5P05551 10 (19) Figure 10. Ignition of the oil. Figure 11. Burning oil before tipping.

2015-08-28 5P05551 11 (19) Figure 12. Tipping the burning oil into the pit.

2015-08-28 5P05551 12 (19) 3 Result and discussion 3.1 Visual observations A sequence of photographs taken during the test is shown in Figures 13, 14 and 15. Figure 13 shows the high intensity of the flames when the oil was poured into the transformer pit. The intensity of the flames decreased significantly as soon as all of the oil penetrated the cavities of the fire protection gratings, as seen in Figure 14. Complete flameout, shown in Figure 15, occurred approximately 6 seconds after the start of tipping the oil into the pit. Similar visual observations were made in both tests. Figure 13. High intensity of the flames after tipping the burning oil into the pit.

2015-08-28 5P05551 13 (19) Figure 14. Flames were visibly smaller within a few seconds after tipping the burning oil into the pit. Figure 15. All visible flames disappeared approximately 6 seconds after tipping the burning oil into the pit.

Temperature [ C] REPORT 2015-08-28 5P05551 14 (19) 3.2 Gas temperatures The temperature and oxygen concentration measurements from both tests correspond well. The results from second test are presented in this report. The results for the gas temperature measured by all thermocouple piles (A-E), positioned according to Figure 1, are shown in Figures 16, 17, 18, 19 and 20. For all graphs the time-axis has been shifted so that t = 0 corresponds to the moment when the oil was started to be poured into the pit. The thermocouples installed at 1 cm height from the ground are became covered by the oil layer at the bottom of the pit, meaning that these thermocouples measure the liquid temperature of the oil. The instant temperature increase after tipping the burning oil into the pit is followed by a rapid drop in temperature. Within 60 seconds the temperatures at all positions have stabilized at approximately 100 C or lower. The temperatures below the protection gratings decay more slowly and fluctuate more than the temperatures above the protection gratings. This is due to the close proximity to the heated oil. 500 400 300 200 100 Thermocouple pile A 0-10 0 10 20 30 40 50 60 70 80 90 100 Time [s] 1 cm from the ground 20 cm from the ground 50 cm from the ground 75 cm from the ground 5 cm above the Profile Plank 50 cm above the Profile Plank Figure 16. Gas temperature measured in the thermocouple pile A.

Temperature [ C] Temperature [ C] REPORT 2015-08-28 5P05551 15 (19) 250 200 150 100 50 Thermocouple pile B 0-10 0 10 20 30 40 50 60 70 80 90 100 Time [s] 1 cm from the ground 20 cm from the ground 50 cm from the ground 75 cm from the ground 5 cm above the Profile Plank 50 cm above the Profile Plank Figure 17. Gas temperature measured in the thermocouple pile B. Thermocouple pile C 400 350 300 250 200 150 100 50 0-10 0 10 20 30 40 50 60 70 80 90 100 Time [s] 50 cm above the Profile Plank 20 cm from the ground 50 cm from the ground 75 cm from the ground 5 cm above the Profile Plank 50 cm above the Profile Plank Figure 18. Gas temperature measured in the thermocouple pile C.

Temperature [ C] Temperature [ C] REPORT 2015-08-28 5P05551 16 (19) Thermocouple pile D 700 600 500 400 300 200 100 0-10 0 10 20 30 40 50 60 70 80 90 100 Time [s] 1 cm from the ground 20 cm from the ground 50 cm from the ground 75 cm from the ground 5 cm above the Profile Plank 50 cm above the Profile Plank Figure 19. Gas temperature measured in the thermocouple pile D. 500 400 300 200 100 Thermocouple pile E 0-10 0 10 20 30 40 50 60 70 80 90 100 Time [s] 1 cm from the ground 20 cm from the ground 50 cm from the ground 75 cm from the ground 5 cm above the Profile Plank 50 cm above the Profile Plank Figure 20. Gas temperature measured in the thermocouple pile E.

Concentration [vol %] REPORT 2015-08-28 5P05551 17 (19) 3.3 O 2 concentration Gas concentrations at two positions during the test, at the center of the pit and 1 from the back end of the pit, are shown in Figure 21. O 2 concentrations 24 22 20 18 16 14 12 10 8 6 4 2 0-10 0 10 20 30 40 50 60 70 80 90 100 Time [s] Center 1 m from the back end Figure 21. O 2 concentrations measured at center of the pit and 1 m from the back end of the pit.

2015-08-28 5P05551 18 (19) 4 Conclusion The tests were performed in order to investigate how well the PcP.s fire protection grating Type LHD is able to extinguish an oil fire under a specific fire scenario. The scenario modeled correlates to a sudden accidental release and ignition of large oil quantities from a transformer. The fire protection gratings Type LHD managed to successfully extinguish the fire during the performed tests. Complete flameout above the fire protection gratings occurred within 6 seconds under the conditions tested. Shortly after, the temperature and oxygen concentration measurements indicate that the fire was extinguished in the entire pit, also under the fire protection gratings. The rapid quenching of the fire is partly due to the reduced oxygen concentration and it is therefore important that the fire grid protection is covering the complete pit and is fastened tight to the concrete wall to minimize leakage of air around the edge of the construction.

2015-08-28 5P05551 19 (19) References [1] 980-1994 R2001 - IEEE Guide for Containment and Control of Spills in Substations, 2001. [2] NFPA 850: Recommended practice for fire protection for electric generating plants and high voltage direct current converter stations, 2010. [3] NFPA 70: National Electric Code, 2011. [4] FM Global Property Loss Prevention Data Sheets 5-4 TRANSFORMERS, 2012. [5] SEK Svenska Elektriska Kommissionen, SS 421 01 01 Starkströmanläggningar med nominell spänning överstigande 1 kv AC., 2004. [6] J. Lindström och M. Försth, Fire test Profile Plank for transformer pit fire protection, SP Fire Research, Borås, 2013. [7] IEC 60076-2 Power Transformers - Part 2: Temperature rise, 1993. Fire Research - Fire Dynamics Performed by Examined by Signature_1 Alen Rakovic Signature_2 Maria Hjohlman

PRODUCT DATA SHEET Nytro 10XN PROPERTY UNIT TEST METHOD GUARANTEED DATA TYPICAL DATA Physical ASTM MIN MAX Appearance D 1524 Clear and bright complies Density, 15 C kg/dm 3 D 1298 0.910 0.880 Viscosity, 40 C mm 2 /s D 445 12.0 7.6 Viscosity, 100 C mm 2 /s D 445 3.0 2.1 Viscosity, 0 C mm 2 /s D 445 76 48 Flash Point, COC C D 92 145 150 Pour Point C D 97-40 -63 Aniline Point C D 611 63 77 Colour D 1500 0.5 <0.5 Interfacial tension at 25 C mn /m D 971 40 50 Chemical Total acid No. mg KOH/g D 974 0.03 <0.01 Corrosive sulphur D 1275 B non-corrosive non-corrosive Antioxidant, phenols Wt % D 2668 0.3 <0.3 Water content ppm D 1533 35 <20 PCB Content ppm D 4059 not detectable not detectable Electrical Dielectric dissipation factor at 100 C % D 924 0.3 <0.1 Breakdown voltage - As received kv D877 30 55 - As received kv D 1816 (0.08''gap) 35 50 - As processed kv D 1816 (0.08''gap) 56 >70 - Impulse breakdown kv D 3300 145 >300 Gassing tendency µl /min D 2300B +35 Oxidation Stability After 72 h D 2440 - Sludge Wt % 0.1 <0.01 - Neutralization No. mg KOH/g 0.3 <0.01 After 164 h - Sludge 0.2 <0.01 - Neutralization No. 0.4 <0.01 Rotating Bomb test minutes D 2112 195 370 Sludge-free life h DOBLE 80 >88 Nytro 10XN is an inhibited insulating oil meeting ASTM D3487 type II, excluding gassing tendency, and IEC 60296 Ed.4 (2012) special applications. Severely Hydrotreated Insulating Oil Issuing date: 2012-04-01