OMNIS Sample Robot Pick&Place

OMNIS Sample Robot Pick&Place 2.101X.1010 Product manual 8.1012.8001EN / 2018-08-17

Metrohm AG Ionenstrasse CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com OMNIS Sample Robot Pick&Place 2.101X.1010 Product manual 8.1012.8001EN / 2018-08-17

Technical Communication Metrohm AG CH-9100 Herisau techcom@metrohm.com This documentation is protected by copyright. All rights reserved. This documentation has been prepared with great care. However, errors can never be entirely ruled out. Please send comments regarding possible errors to the address above.

Table of contents Table of contents 1 Overview 1 1.1 OMNIS Sample Robot Pick&Place Product description... 1 1.2 OMNIS Sample Robot Pick&Place Product versions... 1 1.3 Main module Pick&Place Product versions... 2 1.4 Pick&Place module Product versions... 3 1.5 Peristaltic pump module Product versions... 3 1.6 OMNIS Sample Robot Pick&Place License versions... 4 1.7 About the documentation... 5 1.8 Additional information... 5 1.8.1 Accessories... 5 2 Safety 7 2.1 Product safety... 7 2.2 Hazard levels... 7 2.3 Warning symbols... 8 2.4 Intended use... 9 2.5 Residual risks... 9 2.5.1 General dangers at the workplace... 9 2.5.2 Danger from electrical potential... 10 2.5.3 Danger from machine movements... 11 2.5.4 Danger from biological substances... 11 2.5.5 Danger from highly flammable substances... 12 2.5.6 Danger from careless transport... 12 2.5.7 Danger from leakage... 12 2.5.8 Danger from high temperatures... 13 2.6 Responsibility of the operator... 13 2.7 Personnel requirement... 13 3 Functional description 14 3.1 System overview... 14 3.1.1 System Signals... 14 3.1.2 System Interfaces... 15 3.2 Overview OMNIS Sample Robot Pick&Place S... 16 3.3 Overview OMNIS Sample Robot Pick&Place M... 17 3.4 Overview OMNIS Sample Robot Pick&Place L... 18 3.4.1 Main module Pick&Place Overview... 19 III OMNIS Sample Robot Pick&Place

Table of contents 3.4.2 Pick&Place module Overview... 21 3.4.3 Peristaltic pump module Overview... 24 3.4.4 Rack base Overview... 28 3.5 Sample Robot Pick&Place Functional description... 29 3.5.1 Main module Pick&Place Functional description... 30 3.5.2 Pick&Place module Functional description... 30 3.5.3 OMNIS peristaltic pump module Functional description... 30 3.5.4 Rack base Functional description... 31 3.6 OMNIS Sample Robot Indicators and controls... 32 3.7 Main module Connectors... 33 4 Transport and storage 34 4.1 Checking the delivery... 34 4.2 Storing the packaging... 34 4.3 Lifting the sample robot... 34 5 Installation 35 5.1 Installation by Metrohm... 35 5.2 Sample robot setting up... 35 5.3 Replacing the seal of the sample beaker lid... 36 5.4 Inserting and equipping the titration head... 38 5.5 Optional: Equipping the KF titration head with a homogenizer or rod stirrer... 44 5.6 Mounting the safety shield... 46 5.7 Connecting the tubing to the distributor of the Pick&Place module... 49 5.8 Connecting the drainage tubing... 51 5.9 Connecting the inlet and outlet tubing... 52 5.10 Connecting/Disconnecting the power cord... 53 6 Initial start-up 55 6.1 Initial start-up by Metrohm... 55 7 Operation and control 56 7.1 Operation... 56 7.2 Switching the OMNIS sample robot on and off... 56 7.3 Opening the gripper manually... 57 7.4 Attaching and removing the sample rack... 58 IV OMNIS Sample Robot Pick&Place

Table of contents 8 Maintenance 61 8.1 General maintenance... 61 8.2 Maintenance agreement... 62 8.3 Cleaning the product... 63 8.3.1 Cleaning the Pick&Place module... 64 8.4 Checking and replacing product parts... 71 8.4.1 Replacing the finger tip and PTFE sleeve... 72 8.4.2 Replacing the beaker adapter... 74 8.4.3 Replacing the titration head... 77 8.4.4 Checking the pump tubing... 80 8.4.5 Replacing the pump tubing... 82 9 Malfunctions and troubleshooting 87 9.1 Troubleshooting... 87 10 Disposal 88 11 Technical specifications 89 11.1 Ambient conditions... 89 11.2 Main module Energy supply... 89 11.3 Pick&Place module Energy supply... 89 11.4 Peristaltic pump module Energy supply... 90 11.5 OMNIS sample rack Energy supply... 90 11.6 OMNIS Sample Robot Pick&Place Dimensions... 90 11.7 Main module Pick&Place Dimensions... 91 11.8 Pick&Place module Dimensions... 92 11.9 Peristaltic pump module Dimensions... 92 11.10 OMNIS rack base / OMNIS module base Dimensions.. 93 11.11 OMNIS sample rack Dimensions... 93 11.12 Main module Pick&Place Housing... 94 11.13 Pick&Place module Housing... 94 11.14 Peristaltic pump module Housing... 95 11.15 OMNIS Sample Robot Pick&Place Housing... 95 11.16 OMNIS module base Housing... 95 11.17 OMNIS sample rack Housing... 96 11.18 Main modules Connectors specifications... 96 11.19 OMNIS Sample Robot module Connectors specifications... 97 V OMNIS Sample Robot Pick&Place

Table of contents 11.20 OMNIS rack base Connectors specifications... 97 11.21 OMNIS sample rack Connectors specifications... 97 11.22 OMNIS Sample Robot Pick&Place Display specifications... 97 11.23 Peristaltic pump module Liquid Handling specifications... 97 11.24 Magnetic stirrer Stirrer specifications... 98 11.25 OMNIS Sample Robot Pick&Place Sample handling specifications... 98 11.26 Pick&Place module Sample handling specifications... 99 11.27 OMNIS sample rack Sample handling specifications... 99 VI OMNIS Sample Robot Pick&Place

Overview 1 Overview 1.1 OMNIS Sample Robot Pick&Place Product description The OMNIS Sample Robot Pick&Place system is suitable for use with titrations involving automatic sample changes. The modular construction makes it possible to configure the system in accordance with the area of application. The OMNIS Software is used to control the system. The system is connected to the Ethernet network for that purpose. 1.2 OMNIS Sample Robot Pick&Place Product versions The OMNIS Sample Robot can be configured individually. The OMNIS Sample Robot Pick&Place is available in the following versions as framework for the configuration: Table 1 Product versions Art. no. Designation Version feature 2.1010.1010 OMNIS Sample Robot S Pick&Place S version 2.1011.1010 OMNIS Sample Robot M Pick&Place M version 2.1012.1010 OMNIS Sample Robot L Pick&Place L version The required numbers for the customer service can be found on the type plate (see example): 1 (01) = external article number 2 (21) = Serial number 3 (240) = Metrohm article number 1

Main module Pick&Place Product versions Information on the accessories for the respective product version can be obtained either on the Internet at http://www.metrohm.com or via your regional Metrohm representative. 1.3 Main module Pick&Place Product versions The product is available in the following versions: Table 2 Product versions Art. no. Designation Version feature 2.1010.0010 Main module Pick&Place S Main module Pick&Place, S version 2.1011.0010 Main module Pick&Place M Main module Pick&Place, M version 2.1012.0010 Main module Pick&Place L Main module Pick&Place, L version The required numbers for the customer service can be found on the type plate (see example): 1 (01) = External article number 2 (21) = Serial number 3 (240) = Metrohm article number Information on the accessories for the respective product version can be obtained either on the Internet at http://www.metrohm.com or via your regional Metrohm representative. 2

Overview 1.4 Pick&Place module Product versions The product is available in the following versions: Table 3 Product versions Art. no. Designation Version feature 2.1014.0010 Pick&Place module Without magnetic stirrer 2.1014.0110 Pick&Place module With integrated magnetic stirrer The required numbers for the customer service can be found on the type plate (see example): 1 (01) = External article number 2 (21) = Serial number 3 (240) = Metrohm article number Information on the accessories for the respective product version can be obtained either on the Internet at http://www.metrohm.com or via your regional Metrohm representative. 1.5 Peristaltic pump module Product versions The product is available in the following versions: Table 4 Product versions Art. no. Designation Version feature 2.1016.0010 Peristaltic pump module (2-channel) 2 installed peristaltic pumps 2.1016.0110 Peristaltic pump module (4-channel) 4 installed peristaltic pumps The required numbers for the customer service can be found on the type plate (see example): 3

OMNIS Sample Robot Pick&Place License versions 1 (01) = External article number 2 (21) = Serial number 3 (240) = Metrohm article number Information on the accessories for the respective product version can be obtained either on the Internet at http://www.metrohm.com or via your regional Metrohm representative. 1.6 OMNIS Sample Robot Pick&Place License versions The licenses are available in the following versions: Table 5 License versions Art. no. Designation Version feature 6.06005.010 Function license S Included in the scope of delivery of the main module Pick&Place 6.06005.020 Function license M Included in the scope of delivery of the main module Pick&Place 6.06005.030 Function license L Included in the scope of delivery of the main module Pick&Place 6.06005.910 Function license update S M Update 6.06005.920 Function license update S L Update 6.06005.930 Function license update M L Update Further information on the respective license version can be obtained either on the Internet at http://www.metrohm.com or via your regional Metrohm representative. 4

Overview 1.7 About the documentation Please read through this documentation carefully before putting the product into operation. The documentation contains important information and warnings which you must follow in order to ensure safe operation of the product. Symbols and conventions The following icons and formatting may appear in this documentation: Method File New Work area / Properties [Next] Cross-reference to figure legend The first number refers to the figure number, the second to the product part in the figure. Instruction step Carry out these steps in the sequence shown. Designations for names of parameters, menu items, tabs and dialog windows in the software. Menu or menu item Menu paths in order to arrive at a particular position in the software. Button or key 1.8 Additional information 1.8.1 Accessories Additional information concerning the topic can be found: in the software help in the Metrohm information portal on the Internet https:// guide.metrohm.com Up-to-date information on the scope of delivery and optional accessories for your product can be found on the Internet. You can download this information using the article number as follows: 5

Additional information Downloading the accessories list 1 2 3 4 Enter https://www.metrohm.com/ into your Internet browser. Enter the article number of the product (e.g. 2.1001.0010) into the search field. The search result is displayed. Click on the product. Detailed information regarding the product is shown on various tabs. On the Included parts tab, click Download the PDF. The PDF file with the accessories data is created. When you receive your new product, we recommend downloading the accessories list from the Internet, printing it out and keeping it for reference purposes. 6

Safety 2 Safety 2.1 Product safety 2.2 Hazard levels This product exhibited no flaws in terms of technical safety at the time it left the factory. To preserve this status and ensure non-hazardous operation of the product, the following instructions must be observed carefully. The following warning messages indicate the severity of the danger and its possible effects. DANGER Immediate danger of life Irreversible injuries that will result in death. Warns of dangerous situations or unsafe actions that will most certainly cause severe injuries or death. Lists measures to avoid hazard. WARNING Severe health hazards Serious injuries that could result in death. Warns of dangerous situations or unsafe actions that could result in serious injuries or death. Lists measures to avoid hazard. 7

Warning symbols CAUTION Health hazards or severe property damage Warns of dangerous situations or unsafe actions that could result in moderate injuries or considerable property damage. Lists measures to avoid hazard. 2.3 Warning symbols Make sure that any additional hazard symbols are marked on the product for your operation of the product. The following warning symbols in the documentation and at hazard areas of the product point out hazard potentials: Warning of a hazard area Warning symbol on the product If this warning symbol is on the product, read the respective documentation prior to installation and initial start-up. Warning of electric shock from electrical potential Warning of danger of fire and explosion from highly flammable substances and gases Warning of danger of poisoning and chemical burns from chemical hazardous substances Warning of danger of infection and poisoning from biological hazardous substances Warning of risk of injury from high temperatures 8

Safety edges Warning of cut injuries from pieces of broken glass and/or sharp Warning of risk of injury by laser radiation 2.4 Intended use 2.5 Residual risks Warning of dangerous optical radiation Metrohm products are used for the analysis and handling of chemicals. Usage therefore requires the user to have basic knowledge and experience in handling chemicals. Knowledge regarding the application of fire prevention measures prescribed for laboratories is also mandatory. Adherence to this technical documentation and compliance with the maintenance specifications make up an important part of intended use. Any utilization in excess of or deviating from the intended use is regarded as misuse. Specifications regarding the operating values and limit values of individual products are contained in the "Technical specifications" section, if relevant. Exceeding and/or not observing the mentioned limit values during operation puts people and components at risk. The manufacturer assumes no liability for damage due to non-observance of these limit values. The EU declaration of conformity loses its validity if modifications are carried out on the products and/or the components. 2.5.1 General dangers at the workplace Generally, the regulations and provisions of the regulatory institutions and authorities in the field of work apply. The instructions regarding the following areas have to be followed when using the products: Work safety Handling mechanical installations Handling electricity Handling hazardous and environmentally damaging substances Handling hazardous and environmentally damaging liquids Disposing hazardous and environmentally damaging substances If they are not followed, this may result in: 9

Residual risks Disturbing, injuring and/or killing of people Malfunction and/or damage to instruments and infrastructure Damage and/or contamination of the environment WARNING General dangers at workplace If the safety measures are not followed, working in a laboratory bears a high risk of injury, which can endanger your life and health. 2.5.2 Danger from electrical potential Only professionally trained and qualified specialist personnel may operate the products. Follow the applicable provisions concerning work safety and all regulations on wearing protective clothing. Use suitable tools to perform your work. Check the fill level of waste bottles or waste canisters and analysis vessels, and make sure they do not overflow. Use protective grounding when working with highly flammable substances and gases. WARNING Electric shock from electrical potential Risk of injury by touching live components or through moisture on live parts. Never open the housing of the instrument. Protect live parts (e.g. power supply unit, power cord, connection sockets) against moisture. If you suspect that moisture has gotten into the instrument, disconnect the instrument from the energy supply. Then notify Metrohm Service. Only personnel who have been issued Metrohm qualification may perform service and repair work on electrical and electronic components. 10

Safety 2.5.3 Danger from machine movements WARNING Risk of squashing and pinching from machine movements Injuries from movable instrument parts. 2.5.4 Danger from biological substances Do not reach into the working area of the instruments during the work process. Install and use the protective devices enclosed with the product during the work process. Do not bypass the installed protective devices. If the product is used for biological hazardous substances, it must be marked in accordance with regulations. In case of a return shipment to Metrohm or a Metrohm Service partner, the product or product component has to be decontaminated and the hazard symbol for biological hazardous substances must be removed. A declaration of decontamination must be enclosed. WARNING Danger of infection and poisoning from biological hazardous substances Poisoning from toxins and/or infections from samples contaminated with microorganisms. Clean and disinfect contaminated surfaces. Wear protective equipment. Use exhaust equipment when working with vaporizing hazardous substances. Dispose of biologically contaminated substances properly. 11

Residual risks 2.5.5 Danger from highly flammable substances WARNING Danger of fire and explosion from highly flammable substances and gases Burns from fire and/or injuries from explosions. Avoid ignition sources. Use protective grounding. Use exhaust equipment. 2.5.6 Danger from careless transport WARNING 2.5.7 Danger from leakage Risk of injury from careless transport Injuries from spilled chemical and/or biological substances, falling parts and pieces of broken glass. Remove loose parts (e.g. sample racks, sample beaker, bottles) before transport. Remove liquids. Lift and transport the instrument with both hands on the base plate. Lift and transport heavy instruments only according to instructions. WARNING Risk of injury by leakage A risk of injury exists in connection with escaping liquids of leaking parts and/or connection elements. Replace leaking parts and connection elements without delay. Tighten loose connecting elements. Use environmentally-friendly methods to dispose of escaping liquids. 12

Safety 2.5.8 Danger from high temperatures WARNING Risk of injury from high temperatures Burns from hot surfaces and/or hot liquids. Install and use the protective devices enclosed with the product. Wear protective gloves while working in hot areas. Clean up spilled liquids and solids immediately. 2.6 Responsibility of the operator Eliminate defects or damage which impair operating safety without delay. Eliminate malfunctions which could impair safety without delay. The rules, regulations and instructions listed in the present document are not the only valid ones. Comply with the applicable statutory rules, government agency directives and regulations. Unauthorized modification of the products excludes any and all liability on the part of the manufacturer for any damage resulting from this as well as for any consequential damage. No modifications, attachments or conversions which could impair safety may be carried out on the products without the approval of the manufacturer. Spare parts must meet the technical requirements established by the manufacturer. Original spare parts always meet these requirements. Personnel must be familiar with this safety-relevant information and it must be available for consultation at all times. 2.7 Personnel requirement Only qualified personnel may operate the present product. Qualified personnel are people authorized by the safety responsible to carry out the necessary operations. They are capable of recognizing and avoiding possible dangers. These people are qualified due to their professional training, experience and/or instruction. They know the relevant standards, laws, provisions, accident prevention regulations and the company conditions. 13

System overview 3 Functional description 3.1 System overview 3.1.1 System Signals Visual signals All products and components of the system that are equipped with multicolor status displays indicate their respective status using colors and flashing patterns. The meaning of the colors and flashing patterns is explained in the following table. Use of the flashing patterns Not all products and components use all of the flashing patterns illustrated below. However, the meaning of the flashing patterns is the same for all products and components. Signal Meaning LED lights up yellow LED flashes yellow (slowly) LED flashes yellow (fast) LED lights up green LED flashes green (slowly) LED flashes red (fast) System start or initialization Ready for connection setup or locking Connection setup started or locking underway Ready for operation In operation Malfunction or error 14

Functional description 3.1.2 System Interfaces The system provides the following interfaces: Designation Abbreviation Symbol Use Metrohm Device Link MDL For connecting additional modules or products to a basic product. Human Interactive Device HID For connecting an external control product. Metrohm Solution Identification MSI For connecting the OMNIS Liquid Adapter. Local Area Network LAN For connecting the product to a local network. USB connector USB For connecting USB devices. 15

Overview OMNIS Sample Robot Pick&Place S 3.2 Overview OMNIS Sample Robot Pick&Place S Figure 1 OMNIS Sample Robot Pick&Place S 1 Main module 2 Pump module 3 Pick&Place module 4 Rack base 16

Functional description 3.3 Overview OMNIS Sample Robot Pick&Place M Figure 2 OMNIS Sample Robot Pick&Place M 1 Main module 2 Pump module 3 Pick&Place module 4 Rack base 17

Overview OMNIS Sample Robot Pick&Place L 3.4 Overview OMNIS Sample Robot Pick&Place L Figure 3 OMNIS Sample Robot Pick&Place L 1 Main module 2 Pump module 3 Pick&Place module 4 Rack base 18

Functional description 3.4.1 Main module Pick&Place Overview Figure 4 Main module Pick&Place General overview 1 Main lift 2 Arm holder 3 Lift arm 4 Arm joint 5 Gripper arm 3-5 Robot arm 6 Gripper 7 Gripper fingers The main lift (4-1) is located on the main module Pick&Place. The arm holder (4-2) connects the lift arm (4-3), the arm joint (4-4) and the gripper arm (4-5) with the main lift. The gripper fingers (4-7) are mounted on the gripper (4-6). 19

Overview OMNIS Sample Robot Pick&Place L 3.4.1.1 Main lift Overview Figure 5 Main lift Movement capacity 1 Main lift 2 Arm holder 3 Lift arm The lift arm (5-3) can be moved up and down along the main lift (5-1) with the help of the arm holder (5-2). The main lift (5-1) can be rotated to the left and right. 3.4.1.2 Gripper arm Overview Figure 6 Gripper arm Movement capacity 1 Arm joint 2 Gripper arm 3 Gripper 4 Gripper fingers 20

Functional description The gripper arm as a whole is moved up and down by the main lift. With the arm joint (6-1), the gripper arm (6-2) can be turned to the left and to the right. The gripper (6-3) can open and close the gripper fingers (6-4), in order to pick up and hold beakers. 3.4.2 Pick&Place module Overview Extension versions Up to 4 Pick&Place modules can be installed per OMNIS Sample Robot. In addition, if required, 1 holder for homogenizers (Polytron PT 1300 D) can be mounted on the front of the Pick&Place module. Front Figure 7 Front Pick&Place module 1 Guide chain 2 Lift tower 3 Safety shield 4 Collection tray 5 Slide 6 Titration head holder On each Pick&Place module there is a slide (7-5) for positioning the sample beakers under the titration head. 21

Overview OMNIS Sample Robot Pick&Place L At both slide positions (7-5) (front and rear), the titration head holder (7-6) can be moved downwards via the lift tower (7-2) so that the safety shield (7-3) encases the sample beaker. A titration head that fits the sample beaker to be used can be utilized in the titration head holder (7-6). The titration head contains sensors, dosing tips, cleaning accessories (and occasionally a rod stirrer or homogenizer) that are required for the measurement. Rear Figure 8 Rear Pick&Place module 1 Drain nozzle 2 Distributor At the rear of the Pick&Place module there is a drain nozzle (8-1) to which a tubing is connected via a tubing adapter. Any liquid that may escape will be routed through this tubing into the waste canister. In case of an error, this protects the Pick&Place module from damage. The distributor (8-2) that is used for connecting the rinsing tubing and aspiration tubing is fitted on the back panel of the Pick&Place module. Option for working with a homogenizer (Polytron PT 1300 D) A homogenizer (Polytron PT 1300 D) (9-1) can be inserted in the titration head (9-3) for applications which require homogenization of the sample. A holder for homogenizers has to be mounted for guiding the homogenizer (9-2). For further information, see Inserting and equipping the titration head. 22

Functional description Figure 9 Front Pick&Place module with holder for homogenizer (Polytron PT 1300 D) 1 Holder for homogenizer (Polytron PT 1300 D) 2 Polytron PT 1300 D 3 Titration head 23

Overview OMNIS Sample Robot Pick&Place L 3.4.3 Peristaltic pump module Overview Extension versions 2 or 4 pumps can be mounted per pump module. In the case of the two-way variant, the pumps are mounted on the front only and numbered 1 and 2. In the case of the four-way variant, 2 additional pumps are mounted on the rear and numbered 3 and 4. Arrows indicating inlet and outlet are also to be found above each peristaltic pump next to the numbering. Optionally, 2 additional lid trays can be installed, e.g., for applications with covered sample beakers such as volumetric Karl Fischer titration. Front Figure 10 Front Peristaltic pump module 1 Tubing organizer 2 Housing 3 Peristaltic pumps 24

Functional description Rear Figure 11 Rear Peristaltic pump module 1 Tubing organizer 2 Peristaltic pumps 3 Drain nozzle 2 or 4 peristaltic pumps (11-2) can be fitted on each peristaltic pump module. 2 peristaltic pumps each can be used to rinse and clean the sensors in a Pick&Place module. A tubing organizer (10-1) is located on the top side of the peristaltic pump module to ensure orderly placement and secure fastening of the connected tubing. A drain nozzle (11-3) to which a tubing is connected via a tubing adapter can be found at the rear of the peristaltic pump module. Any liquid that may escape will be routed through this tubing into the waste canister. In case of an error, this protects the pump module against damage. Option for working with covered sample beakers For applications where the sample needs to be protected from environmental influences for example, the sample beakers can be closed with Dis- Cover lids. To store these Dis-Cover lids during analysis, different lid trays can be installed that offer space for 2 to 4 Dis-Cover lids (depending on the product version of the OMNIS Sample Robot Pick&Place). 25

Overview OMNIS Sample Robot Pick&Place L Figure 12 Front Peristaltic pump module with lid tray for OMNIS Sample Robot S 1 Lid tray For Dis-Cover lid Figure 13 Front Peristaltic pump module with lid tray for OMNIS Sample Robot M / L 1 Top lid tray For Dis-Cover lid 2 Bottom lid tray For Dis-Cover lid 26

Functional description 3.4.3.1 Overview Peristaltic pump Figure 14 Peristaltic pump 1 Press clamp 2 Outlet 3 Inlet 4 LED Supply and drainage tubing is connected at the inlet (14-3) and outlet (14-2) of the peristaltic pump. A pump tubing is located in the interior of the peristaltic pump between the inlet and the outlet that is pinched off by four rollers. The conveyance medium is pumped through the system by this volume displacement. The press clamp (14-1) protects the pump tubing against external influences. The press clamp can be dismantled to check the pump tubing and to replace it if necessary. The LED (14-4) displays the status of the peristaltic pump. 27

Overview OMNIS Sample Robot Pick&Place L 3.4.4 Rack base Overview Figure 15 Rack base of an OMNIS sample robot 1 Rack base 2 Rack holder 3.4.4.1 Sample rack Overview On each rack base (15-1), up to 2 sample racks can be inserted on the rack holders (15-2). The system uses the sensors in the rack holder to detect which sample rack type (if any) is present. Figure 16 Sample rack 1 Sample beaker 2 Sample position 3 Transport handles 4 Spout hole 28

Functional description The sample beakers (16-1) are stored in the sample positions (16-2) in the sample rack. The transport handles (16-3) allow for the sample rack to be transported by hand so that it can be set down on and removed from the rack holder of the rack base. Several empty sample racks can be stacked on top of one another on the transport handles. The sample rack contains rinsing holes for emptying liquids in case of overflows and for cleaning. Cleaning The sample rack is not dishwasher-safe. Table 6 Sample rack versions Art. no. Beaker volume Number of beakers 6.02041.010 250 ml 9 6.02041.020 200 ml 9 6.02041.030 120 ml 16 6.02041.040 75 ml 25 3.5 Sample Robot Pick&Place Functional description The Sample Robot Pick&Place is comprised of the following components: Main module Pick&Place Pick&Place module Peristaltic pump module Rack base Module base The OMNIS Sample Robot System is used for the automatic measurement of different organic and inorganic samples. The samples are stored, transported and processed through the components individually integrated in the system. 29

Sample Robot Pick&Place Functional description 3.5.1 Main module Pick&Place Functional description All of the attached modules in the OMNIS Sample Robot System are supplied with electricity through the main module Pick&Place. The main lift with gripper and gripper arm is fastened to the main module Pick&Place. The gripper is used for transporting the sample beakers out of the sample racks and into the processing stations intended for this purpose. Once the processing of the samples has been completed, the gripper removes the sample beakers out of the processing stations once again and transports them back into the previously removed sample rack. The control hardware is integrated in the interior of the main module Pick&Place. 3.5.2 Pick&Place module Functional description The samples in the OMNIS sample robot system are analyzed on the Pick&Place module. The sample beakers are transported by the sample robot into the front sample position of the Pick&Place module. After the sample beaker has been put into place, the slide with the sample beaker moves under the titration head and the lift moves downward. The sensors installed in the titration head analyze the sample. After completion of the measurement, the sensors are cleaned with one of the pumps that are integrated in the pump module. The solution that is generated during this process is aspirated by an additional pump of the pump module and the lift with the sensors rises. Afterwards the slide moves back out again and the sample beaker is removed by the sample robot. 3.5.3 OMNIS peristaltic pump module Functional description 2 or 4 peristaltic pumps are integrated on the peristaltic pump module. 2 peristaltic pumps are assigned to each workstation in the OMNIS sample robot system. The upper peristaltic pump (numbered with 1 or 3) rinses off the sensors in the Pick&Place modules with solvent after the analysis of a sample. For this purpose, the solvent is aspirated from the rinsing canister through the peristaltic pump. If required, these pumps can also be used to dilute a sample with solvent or to bring it into solution prior to an analysis. The lower peristaltic pump (numbered with 2 or 4) aspirates the remaining solution out of the sample beaker during and after the rinsing procedure and routes it to the waste canister. 30

Functional description Optionally, up to 2 lid trays can be installed on the pump module. The Dis- Cover lid that was removed from the sample beaker is parked on the lid tray until it is needed again to seal the sample beaker. If malfunctions occur at the peristaltic pump, this will be displayed via LED at the peristaltic pump. 3.5.3.1 Functional description Peristaltic pump The peristaltic pump operates in accordance with the volume displacement principle. The pump tubing in the interior connects the inlet and the outlet of the peristaltic pump. This pump tubing is pinched off by four internal rollers. Media are aspirated in and out by this squeezing of the pump tubing and the volume displacement that results from it. 3.5.4 Rack base Functional description The rack base is the skeletal structure for the sample robot. The sample racks in which the sample beakers are located are stored on the rack holders of the rack base. The rack holders contain sensors that automatically detect which sample rack type is currently located on the individual rack base. The OMNIS sample robot system uses the sample rack type to detect which type of sample beakers are located in the sample rack. This information is passed along to the control which sets the gripper to the respective size of the sample beakers. If a sample rack that is still to be approached by the sample robot is removed, this is detected by the rack holders and passed along to the OMNIS sample robot system. This sample rack will no longer be approached by the sample robot and the absence of the sample rack will be displayed in the control. 31

OMNIS Sample Robot Indicators and controls 3.6 OMNIS Sample Robot Indicators and controls Figure 17 OMNIS Sample Robot Indicators and controls 1 On/off switch 2 Status display Multi-colored Indicators The status of the instrument is displayed with the status display (17-2) using different colors System Signals (see chapter 3.1.1, page 14). Controls The on/off switch (17-1) is used for the hardware-side operation of the OMNIS Sample Robot. Table 7 Behavior of the on/off switch Pressure duration Acoustic signal Functions on the sample robot Short pressing (1 to 5 s) Beep after 1 s Switching on the instrument Shutting down the instrument Long pressing (approx. 5 s) Double-beep Gripper opens (if available) 32

Functional description 3.7 Main module Connectors Symbol labeling Observe the connector symbols when connecting the instruments. Figure 18 Connectors Main module Pick&Place 1 Human Interactive Device (HID) 2 Local Area Network (LAN) 3 Metrohm Device Link (MDL) 4 Power socket 33

Checking the delivery 4 Transport and storage 4.1 Checking the delivery 4.2 Storing the packaging Immediately upon arrival of the merchandise, check the shipment against the delivery note to ensure completeness and absence of damage. The product is supplied in extremely protective packaging together with the separately packed accessories. Keep this packaging, as only this ensures safe transportation of the product. 4.3 Lifting the sample robot Avoid lifting the sample robot after the initial installation whenever possible. The bigger M and L versions in particular need to be adjusted again after transportation. If it is necessary to lift the sample robot, try to avoid a sag by lifting the system on all four sides. Take the total weight of the system into account. Check the positioning accuracy of the sample robot after placing the sample robot down. If inaccuracies occur, Metrohm support will assist you. 34

Installation 5 Installation 5.1 Installation by Metrohm Installation of the products As a basic rule, the installation of the system and of the new products and modules is handled by trained and instructed specialists from the Metrohm Company and/or its representative. 5.2 Sample robot setting up The product has been developed for operation indoors and may not be used in explosive environments. Place the instrument in a location of the laboratory which is suitable for operation and provides protection against corrosive atmosphere and contamination by chemicals. The sample robot needs a horizontal and plane table that is stable and free of vibrations for a precise mode of operation. The work surface may not bend under a load of 60 kg. Observe the dimensions and weights of the individual products and modules that are part of the complete system. You will find this information in the "Technical specifications" section. Protect the product against excessive temperature fluctuations and direct sunlight. The power cord has to be accessible while operating and must not be replaced by an impermissible cable. 35

Replacing the seal of the sample beaker lid 5.3 Replacing the seal of the sample beaker lid The appropriate seals must be placed on sample beaker lids for KF titration (KF Dis-Cover lids) to tightly seal sample beakers. These seals must not be damaged. We recommend replacing the seal of the sample beaker lid approx. every 6 months. The standard seals were designed for aqueous applications and Karl Fischer titrations. If more aggressive solvents such as chlorobenzene or glacial acetic acid are used, we recommend using the sample beaker lids (Dis-Cover lids) without seals. Table 8 List of sample beakers with sample beaker lids Art. no. Designation Beaker size 6.02710.000 KF Dis-Cover lid for sample beaker 75 ml (P&P) with seals 6.02710.010 KF Dis-Cover lid for sample beaker 120 ml (P&P) with seals 6.02710.030 Dis-Cover lid for sample beaker 75 ml (P&P) 6.02710.040 Dis-Cover lid for sample beaker 120 ml (P&P) 6.02710.050 Dis-Cover lid for sample beaker 250 ml (P&P) 75 ml 120 ml 75 ml 120 ml 250 ml The accessories for the respective product version can be obtained either on the Internet at http://www.metrohm.com or from your regional Metrohm representative. 36

Installation Figure 19 Sample beaker lid: Dis-Cover lid (1) and KF Dis-Cover lid (2) with seal for sample beaker lid (complete) Placing the seal onto the sample beaker lid 1 Placing and fitting the lid seal Figure 20 Placing the rubber seal onto the lid Slide the rubber seal from below over the lid bottom (1) so that it sits neatly in the prefabricated groove (2). Make sure that the rubber seal fits the groove perfectly. You might need to stretch the rubber seal and press it into the groove. 37

Inserting and equipping the titration head Removing the seal of the sample beaker lid 1 Pull the lid seal down over the lid bottom and remove it. 5.4 Inserting and equipping the titration head The titration head has the designations "LOCK" for closed and "UNLOCK" for open, see also Replacing the titration head (see chapter 8.4.3, page 77). Figure 21 Inserting the titration head (general) 1 Titration head 2 Titration head holder 3 Markings "LOCK" and "UNLOCK" Inserting the titration head Prerequisites: The sample robot is switched off. All of the sensors in the titration head are dismounted. 38

Installation The safety shield is dismounted. 1 Inserting the titration head Insert the titration head (21-1) from below into the titration head holder (21-2). In case a rod stirrer is used: The marked opening (triangle or arrow) for inserting the rod stirrer on the titration head should be located as close as possible to the tower of the Pick&Place module. This ensures that the rod stirrer is in a central position and takes up only a small amount of space. 2 Fastening the titration head Figure 22 Fastening the titration head Rotate the titration head by hand until the marking points to "LOCK". 39

Inserting and equipping the titration head Equipping the titration head for titration Figure 23 Positions of the components in the titration head (titration with rod stirrer) 1 Position for the spray nozzles or rinsing nozzles 2 Position for the electrode 3 Position for the aspiration tip 4 Position for the preinstalled dosing tips for connecting dosing tubing 5 Position for the rod stirrer Equipping the titration head for titration Prerequisites: The sample robot is switched off. The required titration head is mounted. 1 Mounting the rinsing tubing Insert the spray nozzles from above into the positions intended for this purpose and mount the rinsing tubing. During insertion, take care to ensure that the spray nozzles do not touch the rod stirrer because otherwise this could lead to jamming of the stirrer. 40

Installation 2 Inserting the electrode Insert the electrode from above into the position intended for this purpose. 3 Mounting the aspiration tubing Insert the aspiration tip from above into the position intended for this purpose and mount the aspiration tubing. If necessary, shorten the aspiration tip to the desired length afterwards. 4 Mounting the dosing tubing Mount the dosing tubing onto the preinstalled dosing tips. 5 Inserting the rod stirrer Insert the rod stirrer from above into the position intended for this purpose, place the corresponding stirring propeller from below onto the rod stirrer coupling and connect the cable of the rod stirrer to the MDL socket of the main module. This step is not necessary if the Pick&Place module involved is the version with the built-in magnetic stirrer (2.1014.0110). 41

Inserting and equipping the titration head Equipping the titration head for Karl Fischer titration Figure 24 Positions of the components in the KF titration head 1 Buret tip for titrant Preinstalled dosing tip with antidiffusion valve 2 Dosing tip for reagent (Solvent) Preinstalled dosing tip with antidiffusion valve 3 Stopper or aspiration tip 4 Double Pt wire electrode Double Pt wire electrode, for KF sample changers incl. electrode cable (6.0340.000) 5 Screw nipples (4 pieces) Screw nipple (6.2730.030) 6 Titration head for KF titration (6.01403.020) Equipping the titration head for KF titration Prerequisites: The sample robot is switched off. The required titration head is mounted. 1 Inserting the stopper or aspiration tip Insert the stopper (24-3) into the screw nipple at the back (close to the Pick&Place module tower). 42

Installation Depending on the application, the stopper can also be replaced by an aspiration tip to aspirate the solution after the titration. The aspiration tip might need to be shortened to the desired length and an aspiration tubing must be mounted. 2 Inserting the buret tip for the titrant Insert the buret tip into the screw nipple on the left, mount the titration tubing and screw it tight. The titration tip should be located just above the stirring bar, but should not impede it. 3 Inserting the dosing tip for the reagent (Solvent) Insert the dosing tip (24-2) into the screw nipple on the right, mount the dosing tubing and screw it tight. The dosing tip should be located just above the stirring bar, but should not impede it. 4 Inserting the electrode Insert the double Pt wire electrode (24-4) with the electrode cable into the screw nipple at the front and screw it tight. Optional: Equipping the titration head for KF titration with a homogenizer or rod stirrer For applications with a titration head for KF titration with a homogenizer (Polytron PT 1300 D) or rod stirrer, see Optional: Equipping the KF titration head with a homogenizer or rod stirrer (see chapter 5.5, page 44). 43

Optional: Equipping the KF titration head with a homogenizer or rod stirrer 5.5 Optional: Equipping the KF titration head with a homogenizer or rod stirrer This KF titration head can be used for either homogenizers or rod stirrers. The guide sleeve for use with homogenizer (Polytron PT 1300 D) is included in the standard delivery of the KF titration head. If a rod stirrer is to be used, this guide sleeve (see (25-3)) needs to be replaced. Figure 25 Positions of the components in the titration head (KF titration with Polytron or rod stirrer) 1 Buret tip of the titrant Preinstalled dosing tip with antidiffusion valve 3 Guide sleeve for the homogenizer Guide sleeve for Polytron PT 1300 D, preinstalled or guide sleeve for the rod stirrer (6.01201.000) 2 Dosing tip of the solvent Preinstalled dosing tip with antidiffusion valve 4 Double Pt wire electrode Double Pt wire electrode for KF sample changers, incl. electrode cable (6.0340.000) 5 Stopper or aspiration tip 6 Titration head for KF titration with homogenizer or rod stirrer (6.01403.050) 44

Installation Equipping the titration head for KF titration with a homogenizer (Polytron PT 1300 D) or rod stirrer Prerequisites: The sample robot is switched off. The required titration head (25-6) is mounted, see Inserting and equipping the titration head (see chapter 5.4, page 38). 1 Stopper or aspiration tip The stopper (25-5) is mounted in the screw nipple at the back (close to the Pick&Place module tower). Depending on the application, the stopper can also be replaced by an aspiration tip to aspirate the solution after the titration. The aspiration tip might need to be shortened to the desired length and an aspiration tubing must be mounted. 2 Mounting the titration tubing for the titrant Insert an M6 tubing in the M6 connector of the preinstalled dosing tip for titrant and screw it tight. 3 Mounting the dosing tubing for the solvent Insert an M6 tubing in the M6 connector of the preinstalled dosing tip for solvent and screw it tight. 4 Inserting the electrode Insert the double Pt wire electrode (25-4) with the electrode cable into the screw nipple at the front and screw it tight. 5 Inserting the homogenizer (Polytron PT 1300 D) Insert the Polytron PT 1300 D with mounted dispersion aggregate into the preinstalled homogenizer guide sleeve (25-3). Tighten the guide sleeve firmly. 45

Mounting the safety shield This step is not necessary if a rod stirrer is used. 6 Using a rod stirrer Instead of the guide sleeve for homogenizers (25-3), insert the guide sleeve for rod stirrers and tighten it lightly. Insert the rod stirrer through the guide sleeve into the titration head and mount the stirring propeller from below to the rod stirrer. Tighten the guide sleeve firmly. This step is not necessary if a homogenizer is used. 5.6 Mounting the safety shield WARNING Working without a safety shield A risk of injury exists when working without a safety shield mounted. Never operate the sample robot without a safety shield. Before beginning work, make sure that all of the protective devices are mounted on the sample robot and operational. Always wear personal protective equipment when working with the sample robot. The safety shield has the designations "LOCK" for closed and "UNLOCK" for open. 46

Installation Figure 26 Inserting the safety shield 1 Safety shield 2 Titration head holder 3 Markings "LOCK" and "UNLOCK" Mounting the safety shield Prerequisites: The sample robot is switched off 1 Inserting the safety shield Insert the safety shield (26-1) from the bottom into the titration head holder (26-2). 47

Mounting the safety shield 2 Fastening the safety shield Figure 27 Fastening the safety shield Rotate the safety shield clockwise until the marking points to "LOCK". 48

Installation 5.7 Connecting the tubing to the distributor of the Pick&Place module Figure 28 Connecting the tubing to the distributor 1 Rinsing tubing 2 Aspiration tubing 3 Distributor 4 Rinsing tubing 5 Outlet tubing Connecting the tubing to the distributor Prerequisites: The sample robot is switched off 1 Connecting the rinsing tubing Manually tighten or plug in the three rinsing tubings (28-1) in the M3 bore holes of the distributor (28-3). The rinsing tubings lead to the spray nozzles of a titration head in the Pick&Place module. 49

Connecting the tubing to the distributor of the Pick&Place module 2 Connecting the aspiration tubing Manually tighten the aspiration tubing (28-2) in the M3 bore hole of the distributor. 3 Connecting the rinsing tubing Remove the union nut. Pull the end of the tubing over the connection nipple of the distributor and fasten in place with the union nut. The rinsing tubing (28-4) leads to the rinsing pump (Pump 1 or Pump 3) and can be cut to the correct length. 4 Connecting the outlet tubing Remove the union nut. Pull the end of the tubing over the connection nipple of the distributor and fasten in place with the union nut. The outlet tubing (28-5) leads to the aspiration pump (Pump 2 or Pump 4) and can be cut to the correct length. 50

Installation 5.8 Connecting the drainage tubing Connecting and placing the drainage tubing 1 Push the tubing adapter (1) in an angle of 30 degrees (see illustration) onto the drain nozzle. 2 3 51

Connecting the inlet and outlet tubing Plug the drainage tubing (2) in the tubing adapter and guide it through the tubing duct (3) to the waste canister (red line). Take care that the tubings are not bent upwards to prevent liquids from backing up. 5.9 Connecting the inlet and outlet tubing Figure 29 Connecting the inlet and outlet tubing 1 Outlet tubing 2 Inlet tubing 3 Connecting element 4 Peristaltic pump Connecting the inlet and outlet tubing of the peristaltic pump Prerequisites: The sample robot is switched off 1 Plug the inlet tubing (29-2) into the connecting element (29-3) of the peristaltic pump (29-4) by hand and rotate clockwise until it fits closely. 52

Installation The tubing connections at the inlet and outlet of the peristaltic pump correspond to the "Luer lock system". The peristaltic pump rotates clockwise. 2 3 Connect the outlet tubing (29-1) following the same procedure. Place the tubing without squeezing it onto the top side by using the tubing organizer. Make sure that the tubing is positioned as close as possible to the housing. The pump operates the aspiration tubing and the three rinsing tubings 5.10 Connecting/Disconnecting the power cord WARNING Electric shock from electrical potential Risk of injury by touching live components or through moisture on live parts. Never open the housing of the product. Protect live parts (e.g. power supply unit, power cord, connection sockets) against moisture. If you suspect that moisture has gotten into the product, disconnect the product from the energy supply. Then notify Metrohm Service. Only personnel who have been issued Metrohm qualification may perform service and repair work on electrical and electronic components. Connecting the power cord Accessories Use power cord according to specifications under "Technical specifications". 53

Connecting/Disconnecting the power cord Power cord with a maximum length of 2 m, three-core with IEC 60320 instrument plug type C13. Conductor cross-section 3x 0.75 mm 2 / 18 AWG. Power plug according to customer requirements (6.2122.XX0), designed for a minimum of 10 A. 1 Plugging in the power cord Plug the power cord into the product's power socket. Connect the power cord to the energy supply. To switch off the product, you must unplug the power cord from the energy supply. 54

Initial start-up 6 Initial start-up 6.1 Initial start-up by Metrohm Initial start-up of the product As a basic rule, the initial start-up of the system and of the new products and modules is handled by trained and instructed specialists from the Metrohm Company and/or its representative. 55

Operation 7 Operation and control 7.1 Operation Operating via the control software The product can be operated using the commands of the control software. Additional information can be found in the software help. 7.2 Switching the OMNIS sample robot on and off Switching the OMNIS sample robot on and off The on/off switch robot. is located on the main module of the sample 1 Switching the OMNIS sample robot on Press the on/off switch signal is heard. for one second until the single acoustic The status display (see "Indicators", page 32) is lit up yellow until it is paired with the OMNIS Software. As soon as the sample robot is paired with the OMNIS Software, the color of the status display switches to green and the sample robot is ready for operation. 2 Switching the OMNIS sample robot off Press the on/off switch for one second until the single acoustic signal is heard. The status display goes out and the sample robot is switched off. 56

Operation and control Additional information on the controls, see OMNIS Sample Robot Indicators and controls (see chapter 3.6, page 32). 7.3 Opening the gripper manually CAUTION Unsecured sample beakers If the gripper is opened, then unsecured sample beakers can cause injuries and property damage to the instrument. Wear personal protective equipment. Always hold the sample beaker in one hand when the gripper is being opened manually. Figure 30 Main module Pick&Place, front 1 On/off switch 2 LED Opening the gripper manually Prerequisites: The sample robot stands still. 1 Hold the sample beaker in one hand. 57

Attaching and removing the sample rack 2 Hold the on/off switch (30-1) pressed down for five seconds until a dual beep is heard. The gripper opens and the sample beaker can be removed. 7.4 Attaching and removing the sample rack CAUTION Utilization of non-authorized sample beakers The use of non-authorized sample beakers in the OMNIS Sample Robot System can lead to injuries and considerable property damage. Use only sample beakers that are authorized by Metrohm. Because of the shape of the rack holder and the counterpart on the sample rack, only one position exists at which the sample rack can be properly placed on the rack base. 58

Operation and control Figure 31 Overview image Attaching and removing the sample rack 1 Rack base 2 Rack holder 3 Sample rack 4 Transport handles Attaching a sample rack 1 Attaching a sample rack Figure 32 Attaching a sample rack Grip the sample rack (31-3) on the transport handles (31-4) with both hands and set it down on the rack base (31-1). 59

Attaching and removing the sample rack 2 Pushing in the sample rack Figure 33 Pushing in the sample rack Push the sample rack towards the front until it is firmly seated on the rack holder (31-2). A brief acoustic signal will sound as soon as the sample rack is seated correctly on the rack base and the rack holder. Removing the sample rack 1 Grip the sample rack on the transport handles with both hands and remove it towards the top. A brief acoustic signal will sound as soon as the sample rack has been removed from the rack base and the rack holder. 60

Maintenance 8 Maintenance 8.1 General maintenance The products require appropriate care. Excess contamination of the products may result in functional disruptions and a reduction in the service life of the mechanics and electronics. Only perform maintenance work that is described in this instruction. Contact the Metrohm service for further maintenance and repairing works. Disconnect the product from the power grid prior to any maintenance and cleaning. Remove spilled chemicals and solvents immediately. Protect the plug connections in particular against contamination. The product is protected by design measures from being penetrated by liquids. CAUTION Instrument damage due to removed covers Damage of the instrument or malfunction by removing the housing covers. Never open the housing of the instrument when the power cord is connected. There are no parts inside the housing which may be serviced or replaced by the user, unless this is explicitly described. Only personnel who have been issued Metrohm qualification may perform service and repair work on electric and electronic parts. 61

Maintenance agreement WARNING Electric shock from electrical potential Risk of injury by touching live components or through moisture on live parts. Never open the housing of the product. Protect live parts (e.g. power supply unit, power cord, connection sockets) against moisture. If you suspect that moisture has gotten into the product, disconnect the product from the energy supply. Then notify Metrohm Service. Only personnel who have been issued Metrohm qualification may perform service and repair work on electrical and electronic components. WARNING Risk of injury due to lack of safety shield Risk of injury when working without mounted safety shields. Never operate instruments without safety shields. Before beginning work, make sure that all the safety shields are mounted correctly and are operational. 8.2 Maintenance agreement Maintenance of the product is best carried out as part of an annual service performed by specialist personnel from Metrohm. Shorter maintenance intervals may be necessary if you frequently work with caustic and corrosive chemicals. Metrohm Service offers every form of technical advice for maintenance and service of all Metrohm products. 62

Maintenance 8.3 Cleaning the product WARNING Danger of poisoning and chemical burns from chemical hazardous substances Poisoning and/or chemical burns by contact with aggressive chemical substances. Use only detergents that do not cause any unwanted side reactions with the materials to be cleaned. Clean contaminated surfaces. Wear protective equipment. Use exhaust equipment when working with vaporizing hazardous substances. Dispose of chemically contaminated materials (e.g. cleaning material) properly. WARNING Electric shock from electrical potential Risk of injury by touching live components or through moisture on live parts. Never open the housing of the product. Protect live parts (e.g. power supply unit, power cord, connection sockets) against moisture. If you suspect that moisture has gotten into the product, disconnect the product from the energy supply. Then notify Metrohm Service. Only personnel who have been issued Metrohm qualification may perform service and repair work on electrical and electronic components. Cleaning the surfaces of the product Prerequisites The product is disconnected from the power grid. 1 Clean the surfaces with a damp cloth. 63

Cleaning the product If the suspicion arises that liquids have found their way into the product, disconnect the product from the power grid and contact your Metrohm Service. Water or ethanol can be used as a cleaning medium. The connectors at the rear of the product must only be cleaned with a dry cloth. 8.3.1 Cleaning the Pick&Place module WARNING Danger of poisoning and chemical burns from chemical hazardous substances Poisoning and/or chemical burns by contact with aggressive chemical substances. Use only detergents that do not cause any unwanted side reactions with the materials to be cleaned. Clean contaminated surfaces. Wear protective equipment. Use exhaust equipment when working with vaporizing hazardous substances. Dispose of chemically contaminated materials (e.g. cleaning material) properly. Cleaning the surfaces of the Pick&Place module Prerequisites 64

Maintenance The instrument is disconnected from the power grid. 1 Remove dust and dirt from the Pick&Place module surface with a damp cloth. The safety shield has the designations "LOCK" for closed and "UNLOCK" for open. Figure 34 Cleaning the safety shield 1 Safety shield 2 Titration head holder 3 Markings "LOCK" and "UNLOCK" Cleaning the safety shield Prerequisites 65

Cleaning the product The instrument is disconnected from the power grid. 1 Dismantling the safety shield Figure 35 Dismantling the safety shield Grip the safety shield (34-1) with one hand and rotate it counterclockwise until the marking points to "UNLOCK" (34-3). Remove the safety shield downwards out of the titration head holder (34-2). 2 Cleaning the safety shield Remove dust and dirt from the safety shield with a damp cloth. 66

Maintenance 3 Inserting the safety shield Figure 36 Inserting the safety shield Insert the safety shield from the bottom into the titration head holder. 4 Fastening the safety shield Figure 37 Fastening the safety shield Rotate the safety shield clockwise until the marking points to "LOCK". 67

Cleaning the product Figure 38 Cleaning the slide and collection tray 1 Slide 2 Collection tray Cleaning the slide and collection tray Prerequisites The instrument is disconnected from the power grid. 68

Maintenance CAUTION Material damage caused by liquids on the slide Material damage can be caused by liquids on the slide if the slide is tilted or removed while it carries a liquid. Remove liquids before the slide is taken out of the collection tray. 1 Removing the slide Figure 39 Removing the slide Remove the slide (38-1) by hand upwards out of the collection tray (38-2). The slide is fastened to the guide rails of the Pick&Place module with 4 magnets. 2 Cleaning the slide Clean carefully as the electronic board is open. Make sure that no liquid can drip from the slide or onto the electronic board. Remove dust and dirt from the slide with a damp cloth. 69

Cleaning the product 3 Cleaning the base plate Remove dust and dirt from the base plate with a damp cloth. If a magnetic stirrer is integrated in the Pick&Place module, skip it during cleaning. 4 Attaching the slide Figure 40 Attaching the slide Attach the slide from above onto the collection tray. Water or ethanol can be used as a cleaning medium. 70

Maintenance 8.4 Checking and replacing product parts To guarantee the flawless functioning and operation of the products as well as of their functional units, all parts must be regularly checked and replaced if needed. The following points must always be observed: The product is switched off. The product is disconnected from the power grid. In the following paragraphs you will find an explanation of how the product parts can be checked individually and what has to be taken into account. The procedure for replacing the parts is then described step-bystep where necessary. WARNING Electric shock from electrical potential Risk of injury by touching live components or through moisture on live parts. Never open the housing of the product. Protect live parts (e.g. power supply unit, power cord, connection sockets) against moisture. If you suspect that moisture has gotten into the product, disconnect the product from the energy supply. Then notify Metrohm Service. Only personnel who have been issued Metrohm qualification may perform service and repair work on electrical and electronic components. 71

Checking and replacing product parts 8.4.1 Replacing the finger tip and PTFE sleeve Figure 41 Replacing the finger tip and PTFE sleeve 1 Gripper 2 Gripper finger 3 PTFE sleeve 4 Finger tip 5 Retainer Dismantling the finger tip and PTFE sleeve Prerequisites The sample robot is switched off. There is no beaker in the gripper. If you are using a gripper with retainer (41-5), lift the retainer off the gripper beforehand. 1 2 3 Clasp the gripper (41-1) from above with one hand and hold it firmly. Use the other hand to pull the finger tip (41-4) downwards and off the gripper finger (41-2) by applying gentle rotating movements. Stretch the PTFE sleeve (41-3) and pull it off downwards. 72

Maintenance A slot to facilitate assembly and disassembly is located in the PTFE sleeve. The PTFE sleeve can be stretched over this slot, e.g., with a small screwdriver or fingernail, and then subsequently removed via the lower section on the gripper finger. Mounting the finger tip and PTFE sleeve Prerequisites The sample robot is switched off. The PTFE sleeve and the finger tip are dismounted. 1 2 Clasp the gripper from above with one hand and hold it firmly. Stretch the PTFE sleeve and slide it onto the gripper finger from below. A slot to facilitate assembly and disassembly is located in the PTFE sleeve. The PTFE sleeve can be stretched over this slot, e.g., with a small screwdriver or fingernail, and then subsequently pushed over the lower section on the gripper finger. 3 4 5 Using gentle rotating movements, slide the finger tip onto the PTFE sleeve from below. Make sure that the finger tip is firmly seated on the gripper finger and that it can still be rotated. Place the retainer (41-5), if applicable, back onto the gripper with retainer. CAUTION The gripper with retainer must always me operated with the retainer! This ensures that the beakers are always gripped correctly. 73

Checking and replacing product parts 8.4.2 Replacing the beaker adapter Figure 42 Replacing the beaker adapter 1 Slide 2 Ring 3 Beaker adapter Table 9 Beaker volume Available beaker adapters and settings Beaker diameter Beaker height Article number 75 ml 35.5 mm 113 mm 6.01404.040 120 ml 47.3 mm 113 mm 6.01404.030 200 ml 70 mm 100 mm 6.01404.020 250 ml 64.7 mm 113 mm no adapter required Replacing the beaker adapter Prerequisites: The sample robot is switched off 74

Maintenance The slide is extended 1 Removing the ring Figure 43 Removing the ring Rotate the ring (42-2) counterclockwise by hand and remove towards the top from the slide (42-1). 2 Removing the beaker adapter Figure 44 Removing the beaker adapter Remove the beaker adapter (42-3) out of the slide by hand from above. 75

Checking and replacing product parts 3 Inserting the beaker adapter Figure 45 Inserting the beaker adapter Make sure that the correct values for the beaker diameter and beaker height (see "Available beaker adapters and settings" table) are entered for the respective Pick&Place module in the OMNIS Software. The value can be modified in the Instruments area under Properties / Specific data. If you switch to another beaker size, make sure to also take the titration head into account. Insert the beaker adapter from above into the slide. Rotate the beaker adapter so that its 4 lugs slide into the grooves of the slide. 76

Maintenance 4 Fastening the ring Figure 46 Fastening the ring Attach the ring by hand to the slide and tighten clockwise. 8.4.3 Replacing the titration head Figure 47 Replacing the titration head 1 Titration head 2 Titration head holder 3 Markings "LOCK" and "UNLOCK" Table 10 Available titration heads 77

Checking and replacing product parts Beaker volume 75 ml 75 ml 75 ml Stirring propeller 6.01900.020 Openings / designations 4xM10 4xM10 for KFT 2xSGJ14, 1xM10 Article number 6.01403.010 6.01403.020 6.01403.040 120 ml 6.01900.030 3xSGJ14, 4x6.4mm 6.01403.030 200 ml 6.01900.030 3xSGJ14, 4x6.4mm 6.01403.060 250 ml 6.01900.010 6xSGJ14, 3xSGJ9 6.01403.000 Replacing the titration head Prerequisites: The sample robot is switched off All of the sensors in the titration head are dismounted The safety shield is dismounted 1 Removing the titration head Figure 48 Removing the titration head Grip the titration head (47-1) with one hand and rotate it counterclockwise until the marking points to "UNLOCK" (47-3). Remove the titration head towards the bottom out of the titration head holder (47-2). 78

Maintenance 2 Inserting the titration head Figure 49 Inserting the titration head Insert the titration head from the bottom into the titration head holder. 3 Fastening the titration head Figure 50 Fastening the titration head Rotate the titration head by hand until the marking points to "LOCK". 79

Checking and replacing product parts 8.4.4 Checking the pump tubing Interval The pump tubing must be checked each time before starting work. Figure 51 Removing the press clamp 1 Press clamp Removing the press clamp Prerequisites: The sample robot is disconnected from the power grid. 1 Pull the press clamp (51-1) on one side outwards by hand. Pull off the other side. Remove the press clamp. Do not fasten or loosen the hex screws of the press clamps. Checking the pump tubing Prerequisites: The sample robot is disconnected from the power grid. 80

Maintenance Daily/continuous checking The pump tubing is comprised of wear parts and is susceptible to leaks and damage. Check the pump tubing daily and/or continuously. Replace worn and/or damaged pump tubing. 1 Perform a visual inspection of the pump tubing. Note any cracking or leaking liquid while doing so. If the pump tubing should exhibit damage, replace it without delay. Replacing the pump tubing (see chapter 8.4.5, page 82) Mounting the press clamp Prerequisites: The sample robot is disconnected from the power grid. 1 Figure 52 Mounting the press clamp Insert one side of the press clamp with the lug into the guide rail provided for this purpose and push it in. Plug the other side in as well with the lug in the guide rail and push it in. 81

Checking and replacing product parts Make sure that the press clamp is placed so that it is flush and positioned cleanly. 8.4.5 Replacing the pump tubing Use the following pump tubing: Light-colored tubing from Pharm-A-line (6.01801.020) with white press clamp (6.02703.000). Only pump tubing that has been authorized by Metrohm may be used. Dismantling the pump tubing Prerequisites: The sample robot is disconnected from the power grid. 1 Removing the peristaltic pump tubing Figure 53 Removing the inlet and outlet tubing Rotate the tubing counterclockwise and remove it upwards out of the peristaltic pump. 82

Maintenance 2 Removing the press clamp Figure 54 Removing the press clamp Pull one side of the press clamp (1) outwards by hand. Pull off the other side. Remove the press clamp. 3 Removing the pump tubing Figure 55 Removing the pump tubing Pull one of the connecting elements of the pump tubing outwards by hand. Afterwards, remove the other side. 83

Checking and replacing product parts The pump tubing is positioned close to the inner rollers for optimum conveyance of the media. It is for that reason that a certain amount of force must be applied for disassembling the first connecting element. The pump tubing and its connecting elements are designed for this application of force. Installing the pump tubing Prerequisites: The sample robot is disconnected from the power grid. The pump tubing is dismounted. 1 Inserting the pump tubing Figure 56 Inserting the pump tubing Slide one connecting element on one side into the guide rail and up until it stops. 84

Maintenance Figure 57 Placing the pump tubing around rollers Place the pump tubing around the rollers and slide the second connecting element up on the other side until it stops in the guide rail as well. The position of the pump tubing must be close and snug to the rollers for optimum conveyance of the media. It is for that reason that a certain amount of force must be applied for assembling the second connecting element. The pump tubing and its connecting elements are designed for this application of force. 85

Checking and replacing product parts 2 Mounting the press clamp Figure 58 Mounting the press clamp Do not fasten or loosen the hex screws of the press clamps. Insert one side of the press clamp with the lug into the groove provided for this purpose and push it in. Plug the other side in as well with the lug in the groove and push it in. Make sure that the press clamp is placed so that it is flush and positioned cleanly. 3 Connecting the tubing with the peristaltic pump See Connecting the inlet and outlet tubing (see chapter 5.9, page 52). 86