Wet Frac Sand Processing

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Wet Frac Sand Processing Meeting the Demands of a Growing Market Oilfield Minerals Outlook, June 21, 2012 CHRISTOPHER KELLEY Sales Manager

Objectives of Wet Frac Sand Processing - Liberate Individual Silica Particles - Remove Non Silica Contaminants - Liberate and Remove Clay Impurities - Remove Non Frac Sand Size Fractions (Depends of Processors Requirements) - Break Up Clusters 2

Basically Take Raw Sand and Prepare it for Feed To Dryer and Dry Screening Plant 3

Frac Sand 4

Preparation for Wet Processing Plant Mining Methods: Dredging Harvest w/ Earthmoving Equipment (Liberated Sands) Blasting and Harvest w/ Earthmoving Equipment (Not Liberated Sands) 5

Preparation of Non Liberated Sands Over 6 to 8 Primary Crushing and Tertiary Impactors for materials over 6 to 8 size Use of Jaw Crusher followed by Either Horizontal Shaft Impactors (HSI) or Vertical Shaft Impactors (VSI) It is important to only liberate and not crush the individual silica particles during liberation Can be operated in closed circuit with Primary screen with circulating load returning to tertiary impactors 6

Non Liberated Sands Over 6-8 (Primary Jaw) 7

Non Liberated Sands Over 6-8 (Tertiary Impactor) 8

Preparation of Non Liberated Sands (less than 6-8 ) Single Stage Crushing for materials typically 6 to 8 size or less Use Either Horizontal Shaft Impactors (HSI) or Vertical Shaft Impactors (VSI) It is important to only liberate and not crush the individual silica particles during liberation 9

Vertical Shaft Impactors (VSI) 10

Primary Screen w/ Sluice Box & Sprays 11

Primary Screen w/ Sluice Box & Sprays 12

Single Stage Frac Sand Plant (No Clays) 13

Cyclone (Principles of Operation) 14

Single Stage Frac Sand Plant (No Clays) 15

Hydrosizer (Principles of Operation) A square or round hydraulic chamber that makes separations via an upward streaming column of water (tweeter water) that separates particles based on their hindered settling rate differential. Separation efficiencies are same as high efficiency wet screening machines (90%) however footprint is smaller and capital costs are lower. To change cut point (separation) simply calculate water quantity required and change teeter water flow rate. Pump that supplies Teeter water is designated for that duty only. 16

Recessed Plate & Frame Press (Pros & Cons) Feed enters the top of the unit via a central feed well. Water Is Injected through a series of pipes to cause an upward rising current. A zone of suspended or teetered solids is established. Fines flow over a weir at the top of the unit. The slurry density of the teetered bed is monitored by a pressure transmitter A PID controller maintains the teetered bed density by adjusting the underflow valve, which releases coarse material. 17

Hydrosizer (How they Work) 18

Hydrosizer (Teeter Water Feed System) 19

Hydrosizer (Two Cell Installation) 20

Hydrosizer (Installation) 21

Flat Bottom Classifier Style Hydrosizer 22

Flat Bottom Classifier Style Hydrosizer (Installation) 23

Single Stage Frac Sand Plant (No Clays) 24

Dewatering Screen (Linear Motion) Dewatering Screen Installation typical discharge of Frac Sand; 8 mesh (2.36mm) by 70 mesh (212 micron) is between 10 & 15% moisture) 25

Dewatering Screen (Linear Motion) 26

Horizontal Belt Filter (Compositech) Typical discharge of Frac Sand; 8 mesh (2.36mm) by 70 mesh (212 micron) is between 4 & 5 % moisture) 27

Horizontal Belt Filter 28

Dewatering Screen (Discharge to Stockpile) 29

Single Stage Frac Sand Plant (W/ Clays & Attritioning) 30

Attrition Cells Used to liberate clays from silica particles Rotating shaft with paddles causes particle on particle scouring Feed should be about 68 to 78% solids Too dilute and the particles glide past one another Too dense and the pulp won t flow through system 31

Standard Components Gearbox Shell Baffles Paddles Motor Outlet Shaft Hubs Inlet Drain

Attrition Cells Paddle Arrangement Paddles pump up or down Alternating arrangement Four paddles per blade arrangement Five (5) sets of blade arrangements 60 HP motor No Belts or Sheaves All surfaces rubber lined down down down up up

Attrition Cell Installation

Single Stage Frac Sand Plant (W/ Clays & Attritioning) 35

Separator TM Feed Box Feed Inlet Feed Box Extension Vortex Finder Cone Section(s) Siphon Control Valve & Gauge Spigot Underflow Regulator Overflow Pipe Overflow Siphon Boot 36

Separator TM (Installation) 37

TREATMENT of NON FRAC SAND MATERIAL After recovering the Frac sand material producers are typically left with the minus 70 mesh (212µ) or minus 50 mesh (300µ) material along with the majority of process water The solids are basically fine sands, silts and clays It is desirable to minimize the amount of solids reporting to settling ponds in order to minimize pond size and cleaning costs. Producers should find marketable uses for these discarded solids such as: Foundry sands Flowable fills Industrial Fillers Landfill cover Soil Augmentation Remote locations of plants makes finding economically feasible uses for byproducts difficult 38

Single Stage Frac Sand Plant W/ UFR (Ultra Fines Recovery) 39

Single Stage Frac Sand Plant W/ UFR (Ultra Fines Recovery) 40

Two Frac Sand Fractions 41

Two Frac Sand Fractions W/ Attritioning 42

Frac Sand & Foundry Sand Fractions w/ UFR 43

Thickener/Clarifier Reduce Settling Pond Size Reduce Energy Requirements for Pumping of Tailing to Settling Ponds Allow Immediate Reuse of Water in Process Allow for Use of Other Technologies to totally Eliminate Settling Ponds 44

Thickener/Clarifier 45

THICKENER/CLARIFIER 46

THICKENER/CLARIFIER 47

POLYMER ADDITION SYSTEM (Dry to Liquid) 48

Thickener Discharge 49

SETTLING POND ELIMINATION Environmentally responsible while also allowing easy reclamation of the process site after reserves are depleted 50

SETTLING POND ELIMINATION Reasons for Settling Pond Elimination Government restrictions on ponds No space available for ponds Immediate reuse of water in process Ponds would be on sand reserves Eliminate costs of maintaining ponds Potential for monetary value via recovery of clays in a consistent form (very rare) 51

OPTIONS (Settling Pond Elimination) Centrifuges Belt Filter Press Recessed Plate & Frame Press Others being developed 52

Pretreatment for Total Pond Elimination 53

DECANTER CENTRIFUGE (SWECO) 54

DECANTER CENTRIFUGE (Principle of Operation) 55

DECANTER CENTRIFUGE (Crosssection view) 56

CENTRIFUGE (Pros & Cons) Advantages Compact Able to adjust discharge moisture Quick set up time Very mobile Easy to clean Disadvantages Requires full time skilled attendant High capital cost Requires polymer addition Requires mechanics who can maintain and fix equipment with extremely tight tolerances When things go wrong repairs can be extremely expensive 57

BELT FILTER PRESS 58

BELT FILTER PRESS (Principles of Operation) 59

Belt Filter Press (Cross section) 60

Belt Filter Press (Pros & Cons) Advantages Inexpensive Disadvantages Requires full time skilled attendant Requires a large quantity of polymer (cationic) addition Inconsistent product discharge Hard to adjust discharge moisture Extremely messy Ask someone who has had one in their facility 61

Recessed Plate & Frame Press 62

Recessed Plate & Frame Presses 63

Composition of Recessed Chamber Filter Plates

Filtrate Discharge from Filter Plate

Cake Discharge (Recessed Plate & Frame) 66

Recessed Plate & Frame Press (Pros & Cons) Advantages No attendant required No additional polymer required Can adjust cake dryness (cycle length) Clean site around press Few moving parts easy to maintain Easy to clean Disadvantages Large not mobile Higher capital cost 67

Misinformed Public 68

Frac Sand Stockpile Damp Frac Sand Stockpile Ready for Dryer and Final Sizing 69