The Use of Aqueous Ozone in the Beer and Wine Industry

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The Use of Aqueous Ozone in the Beer and Wine Industry Presented by Cameron Tapp ClearWater Tech, LLC Ozone Generators for Water & Air Purification

Cold Ozone-Enriched Water O 3 Ozone is not stored - It s generated on-site as needed Ozone is powerful - Microorganisms can t build up an ozone tolerance Ozone is environmentally friendly - Used properly cannot endanger the environment Ozone is safe - Reverts to oxygen before entering sensitive settling ponds Ozone is clean - Leaves no chemical by-products or residual to spoil product quality

Chemical Sanitation Hazardous Material - Special handling & storage requirements Variable Effectiveness - Organisms can become tolerant and less effective Environmentally unfriendly - Ground water contamination, chemical off-gas Collateral Damage - Beneficial bacteria in leech fields or settling ponds can be killed

Hot Water Rinse Cost: Time To produce heat Wear and tear on equipment To produce heat To reduce heat Safety: Dangerous for workers

Cold Water Advantages Saves heating costs Instant ON saves time No cool down - saves time Gentle on equipment surfaces

THE PRODUCT - BEER 9th largest brewery in U.S. Largest Craft Beer producer in USA Employs 150 people at its plant in Chico, CA

THE CHALLENGE Achieve 3 log reduction in mold, yeast (saccharamyces) and enterobacteria counts in rinse water Reduce wear on fermentation tanks caused by chemicals Improve safety reduce cost of chemical handling Save money over time by minimizing manpower and chemical costs

Previous technologies caused problems or had proven ineffective Chlorine Dioxide- - Pitted the stainless steel fermentation tanks - Can impart a change in product flavor - even at low levels in rinse water - Safety issues associated with Chemical handling, levels in rinse water Paracetic Acid: - Inconsistent sanitation results Caused by off-gasing of H2O2 in paracetic acid compound when the lines are depressurized. - The H2O2 in paracetic acid compound reduced shelf life of product significantly Iodophore - An iodine compound used for sanitizing : - Iodine can pit fermentation tanks and degrade soft rubber materials in combination with other cleaning agents - Risk to product flavor

THE OZONE SOLUTION Ozone system installed to serve the brewery s plant-wide sanitary rinse water system 1. Bottle rinser/pre-filler 2. Plant wash down 3. Rinsing fermentation tanks - Pre-rinse with municipal water - Final rinse with ozonted water

System Parameters Incoming municipal water has ph of 7.6 and a chlorine residual of 0.08 to 0.1 ppm Applied ozone dosage rate of approx. 3.3 ppm in the sidestream Target ozone residual level in the storage tank is 1.0 ppm

From UV treated city supply 40gpm 60gpm Pl Off-gas Recirculation Injector Reaction vessel Pl Ozone Generator ORP Probe O 3 Probe 60 gpm 2 inlet The Application 10,000 gallon storage tank 3 outlet

The Results... Seven years and Counting Maintaining 3 log reduction in mold, yeast and bacteria counts Maintaining consistent 1.0 ppm dissolved ozone in storage tank Eliminated wear on fermentation tanks and other stainless steel parts Reduced chemical handling No risk to product flavor Sierra Nevada finds ozone system reliable and easy to maintain

THE PRODUCT - WINE Tobin James Winery - Paso Robles, CA Barrel Washing

THE CHALLENGE microorganisms of concern Acetobacter spp. (bacteria): - Converts ethyl alcohol into acetic acid (volatile acidity) - Strong off-odor (ethyl acetate) found on grapes, in cellars, on equipment, in wood of used wine barrels Brettanomyces spp. (wild yeast) - Found on grapes and in wine, Mousy and metallic off-flavor - Difficult to eliminate once embedded in cooperage - Contamination concern during bottling of low alcohol, slightly sweet wines (risk of secondary fermentation)

The Ozone Solution Ozone is a biocide effective against: Fungi (yeast, mold and their spores) Protozoa (including cysts) Bio-Film Bacteria Virus

Locations to Use Ozone Ozone can be utilized throughout wineries and breweries using a stationary Clean In Place (CIP) system or a Mobile Wash Cart. Rinsing fermentation tanks Cruncher / Auger Transfer lines Bottle rinse Barrels Equipment pads / floor drains Plastic totes

$32,500 in annual savings by reducing hot water use 50%. Calculations: (Assuming a 260 days of operation per year) Gallons x 8.33 x Temp Rise (ºF)( = BTU BTU/100,000 = 1 Therm 1 Therm = 29.3 kwh The Savings Example of ROI 25,000 x 8.33 x 120 / 100,000 x 1.0 = $250/Day

Conclusion Ozone is a logical choice for sanitation in breweries and wineries es due to: No risk to product taste Ozone is generated on-site / - no transportation or handling issues Cost Savings - lower chemical costs,, less wear on stainless equipment Proven track record - ozone has been successful in these applications for over 20 years A natural sanitizer for a natural product No modern beer or wine producer would be without an ozone system. Jeff Poe, Wine Maker Tobin James

Thank You Cheers!