InTrac 797-M InTrac 797-P Instruction manual

Similar documents
For very low to medium/high conductivity: Where optimal performance is essential. INGOLD Leading Process Analytics

Dissolved Oxygen Sensors

Transmitters ph2050 e, O e and Cond7050 e The right measure of performance and price

Manual / Handbuch Spare parts list / Ersatzteilliste

ph Measuring System Start-up and maintenance manual e Contents

Quick Start Guide LIQ-QSG-Hx438, Rev A June Rosemount Hx438. Amperometric Steam Sterilizable Dissolved Oxygen Sensors

PRO 2000i LOW LEVEL DEPOSITOR

Model: 1413 Model: 1418 Float-Controlled Condensate Trap, PN 100

Turbidity Systems. Inline Turbidity Measurements For More Visibility Into Your Process. INGOLD Leading Process Analytics

Multi-Mode Electrode pro

HEAT ONLY & COMBI BOILER

Mechanical seals external, single or double, to DIN EN 12756

VMS-3. Part Number: Ultraviolet Systems VMS-3. Installation, Operation & Maintenance

Glass and Dishwashers AMX / AUX Series

SLT-Series Installation and maintenance instructions

Tough as They Come. Ceramat. Retractable fittings for extreme conditions. With ceramic sealing to the process.

GESTRA Steam Systems DK 45. English. Installation Instructions Steam Trap DK 45

EasyClean200 EasyClean300

Models TX-KE and TX-KP Toxic Gas Transmitters

Glass and Dishwashers AMX / AUX Series

Transmitter Trb 8300 & InPro 8000 Sensor Series Full range turbidity measurements

INSTALLATION & MAINTENANCE

MODEL A-316 CARBON MONOXIDE (CO) MONITOR AND ALARM FOR COMPRESSED AIR TESTING

NEOTeCHA Reactor Sampling Type PV

Rinse connection adapter CPR 40

Installation Instructions

Operating Manual. Model: 1400 Model: 1400-N RIFOmat Float-Controlled Condensate Traps, PN Safety instructions. 2 General description and use

Model gffoz Process Ozone Sensor (In-Line)

PT15 MATERIAL : DIMENSIONS - Nominal in inches. AVAILABLE SPARES: Disc (Packet of 5) ORDERING INFORMATION: Refer to "HOW TO ORDER" page.

HERZ-DR-T-90. Radiator Control Valves with Pre-Setting Function by Means of Double Cone, Suitable for Conversion to Thermostatic Operation. H max.

Condensate Monitor CGKW. Operator s Manual 42/23-36 EN Rev. 2

Technical Specifications: Your product has a high quality finish and should be treated with care to preserve the visible surfaces.

EFX 600. aquamanta. Instruction Manual. 4year guarantee. the experts in aquatic technology. >600 Litres

Gas Instantaneous Water Heater

Instructions for CO 2 Cold Trap System. Part No

Quick Start Guide LIQ-QSG-Hx338, Rev M July Rosemount Hx338. Steam Sterilizable and Autoclavable ph Sensor

Part 2: Installation Instructions cl

Level Electrode NRG NRG Original Installation Instructions English

Steam Trap BK 45 BK 45-U BK 45-LT BK 46

A measured step forward

Laboport Chemically-resistant Laboratory Pumps and Systems

HX Field Replacement Kit

Granule Gastro/Combi

SERVICE MANUAL WASHING. Washer-dryers HEC-RIM HEC-ARCHED. Structural characteristics, electrical components, accessibility

Vacuum Pump Kit User Manual

CORREX MP Anode with external voltage source. Installation & Operation Manual

LABOPORT. Chemically-resistant Laboratory Pumps with Modular Accessories. Operating Instructions for Laboratory Pumps. and for LABOPORT Systems

Industrial Filters Replacement Procedure

UV I UNIT030W / UV I UNIT055W

Installation & Operating Instructions

COOLARC 46 OPERATOR S MANUAL IM /2016 REV03 ENGLISH

SR-60 SR-80 SR-120. Owner s Manual 1

Illustration shows item no Z Original operating manual. Operating manual. BlueMobil eco. Item no: Z-3278

Instruction manual. Submersible sump pump. Safety instructions Application Electrical connection Installation Maintenance Technical data

SPARE PARTS EXPLODED VIEW GAS WALL BOILERS Model MICROGENUS PLUS. R EN - Edition 02-01/04/2007

LP30 High Integrity Low Level Alarm Probe Installation and Maintenance Instructions

CRISTAL Built-in Dish Sterilizer Instruction Manual

SimplyClear Pressurized Filter Product Manual

Retractable ph/orp Sensor

Operating and installation instructions

MC1000 / MC1001 MANUAL. Operating and Calibration Instructions

CLS-1450 Series Spinner Flask Instruction Manual

Service package PDAD- -SP (en) Assembly instructions d [ ]

These Appliances must be installed and serviced by a competent person as stipulated by the Gas Safety (Installation & Use) Regulations.

ferroli Boiler Replacement Maxima 35C- Modena HE

Instruction Manual - Anti-Siphon Ejector Chlorine & Sulfur Dioxide 500 PPD (10 kg/h) Maximum Capacity

Installation Instructions

Operating Instructions

Salt Spray Cabinet. Manual. Model Ref.: VF7705 (500 liter) VF7710 (1000 liter)

Atlas Lightweight Evacuable Pellet Dies User Manual

Bravo Display Warning Messages

Glass and Dishwashers. BarAid 500/800. Installation and. Starting from Serial No.:

Product overview Suction Guns, suction machines, Vac-Blast Cleaners

Reliability in Laboratory Centrifuges Since Operator s Manual. Models 614B, 614L, 614U/UL and 614V/VL Laboratory Centrifuge. Rev. 5.

PROPANE GAS HEATER MODEL NO: DEVIL 4000 OPERATION & MAINTENANCE INSTRUCTIONS PART NO: ORIGINAL INSTRUCTIONS GC ISS 4

INSTALLATION AND MAINTENANCE INSTRUCTIONS. IM US March RediHeat. Table Of Contents. I. Installation RediHeat Start-Up Procedure 4

Heated Gas Sampling Probe PSG Basic

OPERATION and MAINTENANCE INSTRUCTION MANUAL. ADU-12 Task Force Pneumatic Portable Dental System

Operator s Manual CAYENNE HEAT N SERVE 4/3 RECTANGULAR RETHERMALIZER ENGLISH

RENZ FOR QUALITY PRODUCT CATALOGUE.

Tank, Heater, and Control Operation Manual REV. E DATE: 04May2015

Operator s Manual. 6 Gallon Model No. VQ607SFD FOR YOUR SAFETY. Read and understand this manual before use Keep this manual for future reference

INSTRUCTION MANUAL FOR OIL BURNER MODELS

Adsorption dryer PDAD. (en) Operating instructions g [ ]

Getz Equipment Innovators 450 lb Dual Portable Dry Chemical Fill System

INSTRUCTION MANUAL FOR OIL BURNER MODELS

Operation and Maintenance Manual Sondex All-Welded Heat Exchangers (SAW)

MK 45-1 MK 45-2 MK 45 A-1 MK 45 A-2

OPERATIONAL & MAINTENANCE MANUAL For SEM Model 0101 HD Crusher Serial Numbers: 1010 thru 1057

Alpha CombiMax 350 and 600

Lo-Carbon T-series Window & Roof Models

Model: 1100 Float-Controlled Condensate Trap, PN 25

Chemical resistant Vacuum Pumps

Mitocell: Instructions for Use

Part No KEMPER Filter-Master XL

Vacuum Switch, Differential Pressure Adapter, Switching Amplifier

SCC 61 E Valid as of E61SE0404 up to E61SE... SCC 61 E

HX-30/40 and HX-30/40 S Glass and Dishwashers

UL U TR LTRASONIC S ONIC SCALE ALER PIEZO MINI

Zip Econoboil. On wall boiling water. Installation instructions & user manual. Model number: ,

Transcription:

InTrac 797-M InTrac 797-P Instruction manual 797-M/-P-01-CH 20 606 1183

ø50 ø50 ø50 R 1 1/4" ø25 InTrac 797-M/-P 3 InTrac 797-M InTrac 797-P Instruction manual 43 H = 75 a = 325 OUT position ca. 465 IN position ca. 417 ca. 485 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

4 InTrac 797-M/-P Contents 1. Introduction...5 2. General remarks...5 2.1 Please note...5 2.2 Safety precautions...5 3. Description...6 3.1 Uses and features...6 3.2 Function of twin-chamber lock...6 3.3 Operation of manual retractable housing...7 (InTrac 797-M) 3.4 Operation of pneumatic retractable housing...9 (InTrac 797-P) 4. Setup...10 4.1 Mounting the retractable housing...10 4.2 Calibrating the sensor or ph electrode...10 4.3 Inserting the electrode in the housing...10 4.4 Removing the electrode from the housing...11 4.5 Inserting the retractable housing...12 4.6 Removing the retractable housing...12 4.7 Connecting the sterilizing and flushing lines...13 4.8 Connecting the air supply for actuating the...13 pneumatic housing InTrac 797-P 4.9 Temperature sensor...13 5. Operation...14 5.1 Sterilizing the electrode...14 5.1.1 General...14 5.1.2 Sterilizing the electrode in the reactor...14 5.1.3 Sterilizing the electrode in the twin-chamber lock...15 5.1.4 Piping and valving for demanding applications...16 5.2 Removing the electrode without stopping process...17 5.3 Inserting the electrode without stopping process...17 6. Maintenance...18 6.1 Calibration intervals for ph electrodes...18 6.2 Cleaning the electrode...18 6.3 Storing the electrode...18 6.4 Replacing the O-rings...18 7. Specifications...19 7.1 Technical data...19 7.2 Ordering information...19 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 5 1. Introduction When used correctly the InTrac 797 retractable housing is safe to operate and does not present any danger. Before starting to use the housing carefully read this Instruction Manual, and observe the safety precautions and warnings contained in it. The housing has been tested by us and dispatched ready for installation. The retractable housing is delivered without fittings for connecting steam lines. Sets of steam-line fittings in various types are obtainable as accessories (see 7.2) and can easily be attached to the housing (the illustrations in this manual show the InTrac 797 housing fitted with Serto unions). 2. General remarks 2.1 Please note On receipt immediately check that the housing is undamaged and the accessories are complete. For further information, to order spare parts or for repairs, please contact your supplier. 2.2 Safety precautions 1. Do not attempt any work on the head part of the housing or the fitted electrode when the housing is installed and in the inserted position, i.e. in the process medium. Such operation should only be carried out when the retractable member is in the retracted position, i.e. the electrode tip must be in the lower rinsing chamber (see Fig. 1.2). 2. The retractable member must always be in one of two defined positions: IN : measuring or operating or inserted position OUT : maintenance or retracted or withdrawn position If the member stops between the defined positions IN and OUT, the process medium can escape through the lower rinsing chamber and rinsing lines (see section 3.2 Safety precautions ). 3. The retractable member must not be inserted without the electrode in place (see Fig. 1.1). 4. Warning! When the electrode retracts, small amounts of process medium cling to the electrode and find their way into the housing. If the substances are toxic, environmentally harmful or pathogenic, they must be properly disposed of. 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

6 InTrac 797-M/-P 3. Description 3.1 Uses and features InTrac 797 is a sterilizable, retractable housing designed to contain ph, redox electrodes, or 12 mm O2 sensors for use in bioreactors. It can also contain FSC 402 turbidity sensors. It enables the electrode to be withdrawn for maintenance purposes under sterile conditions while the process is running. After servicing, the electrode can be sterilized in the twin-chamber lock and inserted again without impairing the reactor s sterile contents. Combination ph and redox electrodes are filled with a gelled reference electrolyte which needs no topping-up and requires no pressuration. InTrac 797 is mounted on the side of the bioreactor with the aid of a weld-in socket (25 mm dia.). 3.2 Function of twin-chamber lock In the twin-chamber lock (see Fig. 1.2), the measuring tip of the withdrawn electrode can be cleaned, serviced if necessary and then sterilized with steam. In contrast to single-chamber designs, the twin-chamber arrangement ensures that after sterilization the lower rinsing chamber adjacent to the process medium remains sterile when the electrode is inserted. This is because the portion of the retractable member arriving in the lower rinsing chamber as the electrode is being inserted, has first been sterilized in the upper rinsing chamber. Lower rinsing chamber Upper rinsing chamber Figure 1.1 IN Position Figure 1.2 OUT Position 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 7 Safety precautions All valves (see Fig. 2) must be closed while the moving part of the housing is travelling forwards or backwards, otherwise the reactor contents can escape through the lower rinsing chamber. Valves 1, 2, 3: closed Figure 2 Installation of valves 3.3 Operation of manual retractable housing (InTrac 797-M) With manual operation, the retractable member is brought to the required position by actuating the locking pin and moving it by hand. Only when the locking pin has latched in place is the member in one of the two defined positions: IN : measuring or operating or inserted position OUT : maintenance or retracted or withdrawn position Safety precautions If the retractable member is left between the defined positions IN and OUT, the process medium can escape through the lower rinsing chamber and rinsing lines (see section 3.2 Safety precautions ). 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

8 InTrac 797-M/-P To withdraw the retractable member Pull out lower locking pin (1) and withdraw the moving part by hand until pin (1) latches in place. Turning the retractable member slightly clockwise will release any ring seals that may have become stuck. 1 2 OUT Figure 3 Retractable member I To insert the retractable member Pull out the upper locking pin (2) and insert the retractable member by hand until pin (2) latches in place.turning the retractable member slightly clockwise will release any ring seals that may have become stuck. 1 2 IN Figure 4 Retractable member II The force required to insert and withdraw the retractable member increases with the pressure in the reactor. We recommend a practicable limit of 4 bar vessel pressure for manual operation. Above this pressure, use pneumatic operation. 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 9 3.4 Operation of pneumatic retractable housing (InTrac 797-P) The InTrac 797-P housing is delivered without compressed air connections. These are part of the pneumatic Festo set, which is obtainable as an accessory (see 7.2). When operated pneumatically, the retractable member is moved to the required position by means of compressed air at 3-8 bar. Movement is controlled by a 5/2-way valve with toggle switch, and two one-way restrictor valves. The desired position ( IN or OUT ) is determined by the setting of the 5/2-way valve. Air connections (for 6/4 mm plastic tube) A R B S P A: Compressed air connection B: Compressed air connection P: Control air 3 to 8 bar R: Venting connection A S: Venting connection B Figure 5 Compressed air connections Figure 6 Conversion of manual to pneumatic version Safety precautions If the control air loses pressure or is contaminated with dust, the retractable member might jam at some position between IN and OUT. If this happens, the process medium can escape through the rinsing chamber and flushing lines (see also 3.2). The retractable member must never be inserted without the electrode in place. Consideration should be given to the installation of an alarm to signal drop in, or loss of, air pressure. A suitable, checkvalve protected, pneumatic reservoir may also be considered. These items are not of our supply. 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

10 InTrac 797-M/-P 4. Setup 4.1 Mounting the retractable housing The housing is mounted on the side of the bioreactor using a weld-in socket (25 mm dia. 40 mm long) inclined at 15. If a new socket has to be welded on, make sure the angle is 15. After careful welding, the bore must be reamed out to 25 mm H7 (Consult Instructions for weld-in sockets ES-O2-CH ). G 1 1/4" 15 ø25-h7 ø42 ±0.1 Figure 7 Weld-in socket 4.2 Calibrating the sensor or ph electrode See instructions for electrode, sensor and transmitter. 4.3 Inserting the electrode in the housing 1. Move the retractable member to the OUT position. 2. Unscrew protective sleeve (A) from adapter (B) (see Fig. 8). 3. First place the white slip-ring (002011055) on the electrode, then the O-ring (203021000). 4. Push the electrode or sensor fully into the housing, and screw in fingertight only. 5. Pass the plug of the electrode cable through the protective sleeve (A), and screw to the receptacle of the electrode (see Fig. 8). 6. Screw the protective sleeve (A) fingertight to adapter (B). 7. Draw cable grommet (C) over cable and press it into protective sleeve (A). 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 11 C Cable grommet A Protective sleeve B Adapter Figure 8 Inserting the electrode 4.4 Removing the electrode from the housing 1. Move the retractable member to the OUT position. 2. Detach cable grommet (C) from protective sleeve (A) (see Fig. 8). 3. Unscrew protective sleeve (A) from adapter (B). 4. Unplug electrode cable from electrode. 5. Unscrew the electrode using the hexagon head and withdraw the electrode from the housing in a straight line. Safety precautions Never remove the electrode while at the IN (measuring) position, otherwise the reactor s contents will run out through the housing. 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

12 InTrac 797-M/-P 4.5 Inserting the retractable housing 1. Insert the housing, containing the calibrated sensor or ph electrode, into the welded socket, and tighten the cap nut on the welded socket by hand. Do not over-tighten or use tools, hand tight is sufficient. 2. Connect steam lines to fittings (see section 4.7). Safety precautions The retractable member of the electrode assembly must never be inserted without the electrode in place. Initially the retractable member must be in the OUT position. 4.6 Removing the retractable housing Safety precautions Before attempting to remove the housing ensure the vessel (or pipe-line) is empty and clean if necessary. 1. Close all valves. 2. Move the retractable member to the OUT position. 3. Flush the twin-chamber lock with steam or condensate for a few seconds. Valve settings as in Table 1-C. 4. Remove cable grommet (C) from protective sleeve (A) (see Fig. 8). 5. Unscrew protective sleeve (A) from adapter (B). 6. Disconnect electrode cable from electrode. 7. Carefully disconnect steam lines from the fittings. 8. Undo cap nut from the welded socket and withdraw housing complete with electrode out of the welded socket. 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 13 4.7 Connecting the sterilizing and flushing lines (see Fig. 2) The housing is supplied with blind plugs in the ports of the rinsing chambers. Important: It is essential that the two closely adjacent fittings point vertically downwards (see Fig. 1.1/1.2). Do not mount horizontally. Safety precautions Stainless steel tube of 6/4 mm (OD/ID) is recommended for the supply and drain lines. Long runs of these are not recommended. Steam should be brought as close as possible in wider bore tubing and then reduced to 6 mm size. Steam lines should be lagged to protect operatives, and to prevent undue heat loss. It is also desirable to arrange for a supply of sterile air to the rinsing chamber (see 5.1.1, 5.1.4 and Fig. 10). If calibrating the O 2 sensor in the rinsing chamber, it is mandatory to connect a supply of sterile air (see 5.1.4 and Fig. 10). 4.8 Connecting the air supply for actuating the pneumatic housing InTrac 797-P Figure 9 Actuating air supply The pneumatically operated housing requires an oil- and dustfree, non-condensing air supply. The pressure must be in the range of 3-8 bar, and at least 1 bar more than the vessel pressure (not neglecting the hydrostatic head). The compressed air fittings shown in Fig. 9 are from the pneumatic Festo set, obtainable as an accessory (see 7.2). 4.9 Temperature sensor A sensor for monitoring the sterilization temperature can be fitted after removing the 1/8" screw plug on the twin-chamber lock. A suitable temperature sensor type Pt100-764/5m is included in our list of optional accessories (see section 7.2). 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

14 InTrac 797-M/-P 5. Operation 5.1 Sterilizing the electrode 5.1.1 General The electrode or sensor can be sterilized either when inserted into the reactor (see 5.1.2) or gently under controlled conditions in the twin-chamber lock (see 5.1.3). When sterilizing is done in the inserted position, the twin-chamber lock must be sterilized as well to ensure maximum sterility. We recommend using a sterilization procedure that exposes the electrode to as little temperature shock as possible. Inserting the steam-heated electrode into the cold reactor contents, for example, puts a severe thermal stress on the glass electrode. The following chapters 5.1.2 and 5.1.3 describe the sterilization of the electrode or sensor using a minimum amount of piping and valving. We advise fitting the steam line with a sterilizable air filter through which air can be fed to the twin-chamber lock as it cools down from the sterilizing temperature. For applications in media with solids loading, we also recommend the installation of a flushing water line for rinsing the lower rinsing chamber. An example of such a sophisticated installation is given in chapter 5.1.4. Important: When employing a 12 mm O 2 sensor and calibrating it in the rinsing chamber, it is mandatory to connect a supply of sterile air (see 5.1.4 and Fig. 10). 5.1.2 Sterilizing the electrode in the reactor 1. Insert the electrode as in section 4.3. 2. Insert the housing as in section 4.5. 3. Insert the retractable member. Valve settings as in Table 1/F. 4. Sterilize the electrode in the reactor. Valve settings as in Table 1/A. 5. As soon as the reactor reaches the sterilizing temperature the twin-chamber lock must also be sterilized. Purge with steam until the rinsing chambers are hot (valve settings as in Table 1/G), then establish valve settings as in Table 1/E to sterilize (recommended sterilizing conditions: 20 minutes at 121 C). This procedure ensures the condensate trap is not overloaded. 6. Close all valves (valve settings as in Table 1/F). 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 15 5.1.3 Sterilizing the electrode in the twin-chamber lock 1. Insert the electrode as in section 4.3. 2. Insert the housing as in section 4.5. 3. Sterilize the electrode in the twin-chamber lock. Purge with steam until the twin-chamber lock is hot (valve settings as in Table 1/C), then establish valve settings as in Table 1/D to sterilize (recommended sterilizing conditions: 20 minutes at 121 C). This procedure ensures the condensate trap is not overloaded. 4. Set valves as in Table 1/B and vent chambers through sterile air filter if possible (see 5.1.1). 5. Insert sensor into sterilized reactor. Valve settings as in Table 1/F. Table 1: Typical operating situations for InTrac 797 electrode housing Situation 1 Steam 2 Flush- 3 Con- Position of electrode in inlet ing water densate InTrac 797 housing outlet drain A Sterilizing in CLOSED CLOSED CLOSED reactor 1 3 2 B Electrode CLOSED CLOSED CLOSED retracting 1 3 2 C Rinsing twin- OPEN OPEN CLOSED chamber lock with condensate/steam D Sterilizing the OPEN CLOSED OPEN twin-chamber lock 3 1 2 1 E Sterilizing the OPEN CLOSED OPEN electrode 3 2 1 F Electrode CLOSED CLOSED CLOSED extending 3 2 1 G Rinsing twin- OPEN OPEN CLOSED chamber lock with condensate/steam 3 3 2 2 1 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

16 InTrac 797-M/-P 5.1.4 Piping and valving for demanding applications 1 2 Steam Air Flow restrictor 7 5 6 4 3 Flushing water Figur 10 Connections for flushing water and air The recommended steam pressure is 2.2 bar. Valves 3, 5 and 6 have to be mounted as close as possible to the T-connectors to ensure good heat transfer up to the valves. The flow restrictor (diameter 0.5 mm) on the condensate side of the filter is a simple means to save an extra steam trap or a bleed valve. The flushing water enters the lower rinsing chamber through the bottom to remove the air readily. The upper rinsing chamber does not require rinsing because it remains clean under all operating conditions. We recommend to use a 0.2 µm pore size filter with a flow capacity of 100 m 3 /h such as Emflon 2 from Pall corporation (type: MCY4463V002PVH4). 1. Sterilization: First, valves 2, 3, 5 and 7 are closed, valves 1, 4 and 6 are opened to purge with steam until the twin-chamber lock is hot. Valve 6 is then closed and valve 7 opened for sterilization. 2. Airing: After sterilization, valves 1 and 7 are closed and valve 2 is opened to let air enter the system during cool down from sterilization temperature. 3. Rinsing: To rinse the lower rinsing chamber, valves 1, 2, 4, 6 and 7 are closed and valves 3 and 5 are opened. Rinsing water can be removed from the chamber by either purging with steam as described under section 1 above or by blowing out with air while valves 2, 4 and 6 are open and valves 1, 3, 5 and 7 are closed. 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 17 5.2 Removing the electrode without stopping process 1. Close all valves. 2. Withdraw the retractable member. 3. Flush twin-chamber lock with condensate/steam for a few seconds (valve settings as in Table 1/C) or rinse thoroughly with water (see Fig. 10). 4. Remove cable grommet (C) from protective sleeve (see Fig. 8). 5. Unscrew protective sleeve (A) from adapter (B). 6. Disconnect electrode cable from electrode. 7. Turning the hexagon head, draw the electrode in a straight line out of the housing. The sensor or electrode may now be serviced (e.g. calibrated, see section 4.2). 5.3 Inserting the electrode without stopping process 1. Unscrew protective sleeve (A) from adapter (B) (see Fig. 8). 2. First place the white slipring (002011055) on the electrode, then the O-ring (203021000). 3. Push the electrode fully into the housing and screw in fingertight. 4. Pass the plug of the electrode cable through the protective sleeve (A), and screw to the receptacle of the electrode (see Fig. 8). 5. Screw the protective sleeve (A) fingertight to adapter (B). 6. Draw cable grommet (C) over the cable and press it into protective sleeve (A). 7. Sterilize the sensor according to section 5.1.3. 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

18 InTrac 797-M/-P 6. Maintenance 6.1 Calibration intervals for ph electrodes The frequency of calibration depends upon the required accuracy and the nature of the process. We advise frequent calibration to start with. If the zero point and slope do not vary significantly, then the time between calibrations can be extended. 6.2 Cleaning the electrode Each time the electrode is retracted into the maintenance position, it should be flushed with steam condensate for a few seconds (valve settings as in Table 1/C) or thoroughly rinsed with water (see Fig. 10). Warning! When the electrode retracts, small amounts of process medium cling to the electrode and so find their way into the housing. If the substances are toxic, environmentally harmful or pathogenic, they must be properly disposed of. The sensor/electrode may be further cleaned by any of the standard procedures to be found in the instruction bulletin for the product. 6.3 Storing the electrode For ph electrodes, the tip should be kept either in the watering cap filled with reference electrolyte or, if the electrode is mounted in the housing, in the water-filled rinsing chamber. The O 2 sensor should be stored with O 2 electrolyte in its membrane body. Important: Store cleaned electrodes in a clean place. 6.4 Replacing the O-rings The time between O-ring changes depends on how often the retractable member is inserted and withdrawn, and also upon the compatibility of the Viton material of the O-rings with the process medium. For details of the O-rings, see section 7.2 Service kit and Fig. 11 Exploded drawing. 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 19 7. Specifications 7.1 Technical data InTrac 797-M InTrac 797-P Mode of operation manual pneumatic Control air Pressure in reactor 3 to 8 bar, oil- and dustfree, non-condensing depending on sensor specification, but not more than 6 bar Temperature ranges: Retractable member 0 to 130 C, steam sterilizable Headpart 0 to 80 C Weld-in socket Insertion length D= 25 mm, L= 40 mm, 15 chamfer H= 75 mm Materials: Parts in contact stainless steel DIN 1.4435 with medium Headpart POM (polyoxymethylene) and PP (polypropylene) Seals in contact Viton with medium Other seals Nitrile, Buna Flushing connections Weight d= 6 mm / 4mm 2 kg 7.2 Ordering information Standard scope of delivery Description Order no. InTrac 797-M / 75 manual, with: 007973007 Protective sleeve In Trac 797-P / 75 pneumatic, with: 007973009 Protective sleeve In Trac 797-M / 75 FSC, for turbidity measurements 007973012 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

20 InTrac 797-M/-P Spare parts and accessories Description Order no. Service kit small ( A in exploded drawing): 007972003 1 pc. O-ring 21.95 x 1.78 Viton 2 pcs. O-ring 10.50 x 2.70 Viton R9 Service kit complete ( B in exploded drawing): 007972002 5 pcs. Gasket 10/14/0.8 1 pc. Quad ring 20.22 x 3.53 Buna 1 pc. O-ring 25.00 x 4.00 Nitril 1 pc. O-ring 31.47 x 1.78 Viton 1 pc. O-ring 21.95 x 1.78 Viton 1 pc. O-ring 18.72 x 2.62 Viton 1 pc. O-ring 25.12 x 1.78 Viton 1 pc. O-ring 10.50 x 2.70 R9 Viton Weld-in socket, straight, L= 40 mm, steel DIN 1.4435 007641017 Weld-in socket, angl. 15, L= 40 mm, steel DIN 1.4435 007641014 Pressure connection set 201022000 Protective sleeve, cable grommet 5 mm 007642163 Protective sleeve 007642148 Cable grommet 5 mm 007641236 Electrode holder 007771004 Locking pin, complete 007772000 One-way restrictor valve GRL 1/8" 201021049 Serto connection, steel 18/8 201021007 O-ring 25.00 x 4.00 nitrile 203001117 O-ring 10.50 x 2.70 Viton R9 203021000 O-ring 18.72 x 2.62 Viton 203021113 O-ring 21.95 x 1.78 Viton 203021114 O-ring 31.47 x 1.78 Viton 203021115 Quad ring 20.22 x 3.53 Buna 203031200 Fitting Set for InTrac 796/InTrac 797 Serto 007972006 Fitting Set for InTrac 796/InTrac 797 Swagelok 007972007 Fitting Set for InTrac 796/InTrac 797 Gyrolok 007972008 Pneumatic operation set Festo 007772004 Gasket 203051004 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

InTrac 797-M/-P 21 Cable grommet Protective sleeve Electrode holder B 20 303 1200 B 20 300 1117 Locking pin (797-M) Spacer bushing One-way restrictor valve (797-P) - part of pneumatic Festo set A,B B B 20 302 1000 20 302 1113 20 302 1115 Cylinder screw B B B 20 302 1131 20 302 1113 SERTO connection Rinsing chamber-upper Rinsing chamber-lower A,B B 20 302 1114 20 302 1113 Cap nut Figur 11 Exploded drawing 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 797-M/-P-01-CH Printed in Switzerland 20 606 1183

22 InTrac 797-M/-P Temperature sensor Description Order no. Temperature sensor Pt100-764/5m 101003104 Electrodes Description Order no. ph electrode: InPro 3000/ 325 52000195 ph range: 0 to 14 Pressure range: up to 4 bar Temperature range: 0 to 130 C Installed length: 325 mm ph electrode: InPro 3100/ 325/ Pt100 52000663 ph electrode: InPro 3100/ 325/ Pt1000 52000664 ph range: 0 to 14 Pressure range: up to 6 bar Temperature range: 0 to 130 C Installed length: 325 mm ph electrode: 405-DPAS-SC-K8S/ 325 104054482 ph range: 0 to 12 Pressure range: up to 2.5 bar Temperature range: 0 to 130 C Installed length: 325 mm Redox electrode: Pt 4805-DPAS-SC-K8S/ 325 105053337 Pressure range: up to 2.5 bar Temperature range: 0 to130 C Installed length: 325 mm O 2 sensor: InPro 6100/320/T/N: 52200102 InPro 6100/320/T/P: 52200109 InPro 6100/320/S/N: 52200118 InPro 6100/320/S/P: 52200126 Pressure range: 0.2 to 5 bar Temperature range: measurement: 0 to 80 C sterilization: 0 to 130 C Installed length: 320 mm Turbidity sensor: OFS12S-297I 00824500 Pressure range: up to 6 bar Temperature range: -30 to 130 C Installed length: 297 mm 797-M/-P-01-CH 10/03 Mettler-Toledo GmbH, CH-8606 Greifensee 20 606 1183 Printed in Switzerland

BR D Mettler-Toledo Ind. e Com. Ltda., Alameda Araguaia, 451 - Alphaville, 06455-000 Barueri / SP Brazil, Tel. +55 11 4166-7400, Fax +55 11 4166-7401 Mettler-Toledo GmbH, Ockerweg 3, 35396 Gießen Germany, Tel. +49 641 507-333, Fax +49 641 507-397 F Mettler-Toledo Analyse Industrielle Sàrl, 30 Bld. de Douaumont, BP 949, 75829 Paris Cedex 17, France, Tel. +33 1 47 37 06 00, Fax +33 1 47 37 46 26 USA Mettler-Toledo lngold, Inc., 36 Middlesex Turnpike, Bedford, MA 01730 USA, Tel. +1 781 301-8800, Fax +1 781 271-0681, Toll free +1 800 352-8763 Mettler-Toledo GmbH, Process Analytics, Industrie Nord, CH-8902 Urdorf, Switzerland Tel. +41 1 736 22 11, Fax. +41 1 736 26 36 Subject to technical changes. 10/03. Mettler-Toledo GmbH. Printed in Switzerland 20 606 1183