HIGHEST EFFICIENCY VERTICAL BASKET CENTRIFUGES

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HIGHEST EFFICIENCY VERTICAL BASKET CENTRIFUGES

Ferrum Ltd. Centrifuge Technology T 41 62 889 14 11 Industriestrasse 11 F 41 62 889 15 13 CH-5503 Schafisheim centrifuges@ferrum.net Switzerland www.ferrum.net Spomasz Wronki Ferrum Group ul. Powstańców Wlkp. 23 T 48 672 545 169 PL-64-510 Wronki handel@spomasz-wronki.com.pl Poland www.spomasz-wronki.com.pl Ferrum Inc. Centrifuge Technology T 1 877 933 3778 16225 Park Ten Place F 1 877 711 2329 Suite 500 sales@ferrumus.com Houston, TX 77084 www.ferrumus.com USA Ferrum Technologies India Private Ltd. 105, Shree Saiishwati Co-op. Hsg. Soc. T 91 222 431 4299 Mogul Lane F 91 222 432 2276 400016 Mahim, Mumbai sale@ferrumin.com India www.ferrum.net Ferrum Canning and Centrifuge Technology (Kunshan) Co., Ltd. No. 329, Jujin Road T 86 512 3662 5104 Zhangpu Township F 86 512 3662 5100 215321 Kunshan City centrifuge@ferrumchina.com Jiangsu Province www.ferrumchina.com P.R. China

APPLICATIONS SPECIFIC DESIGNS CHEMICAL INDUSTRY Chlorides Trichloroisocyanuric acid Sodium dichloroisocyanurate Sulphates Gypsum Iron sulphate heptahydrate Fibrous Products Nitrocellulose Chips - Fibres CMC FINE CHEMICAL AND PHARMACEUTICAL INDUSTRY Fine Chemicals Pigments Herbicides, insecticides Pharmaceuticals Antibiotics, APIs Intermediates Vitamines A, E Foods Amino acids CUSTOMISED SOLUTIONS Ferrum vertical scraper and top discharge centrifuges have been proven in numerous applications in the chemical, fine chemical and pharmaceutical industry. Our centrifuges offer a broad range of applications, from pilot plants and small-scale production to continuous production applications. Scraper centrifuges are used for products that can be filtered with solids concentrations as low as 2 w% and particle sizes down to 4 μm. 01

VERTICAL SCRAPER CENTRIFUGES BOTTOM DISCHARGE PRINCIPLE OF OPERATION AND APPLICATIONS The VBC type vertical scraper centrifuges (Vertical Bottom discharge Centrifuge) work discontinuously. The solids are discharged vertically downwards in a completely closed system. Applications include the demanding operating conditions of the chemical industry as well as utilisation in complex pharmaceutical processes. As a result of high modularity and the comprehensive range of optional equipment, the latest VBC centrifuge can be optimally adapted to your requirements. MODULARITY AND OPTIONAL EQUIPMENT Robust and reliable design in accordance with the latest standards, directives and GMP requirements Optimally designed functional parts for efficient and reliable process cycles with low vibration Reliable sealing of the bearing housing using the latest generation of sealing systems Application-specific feed and wash systems: feed and wash pipe or inclined feed and wash disk Position of filtrate discharge as well as cover opening can be selected as required Scraper unit systems: scraper knife over the entire basket height or scraper knife with vertical movement Motor arrangement: above or below the base plate Systems for effective residual heel removal, even for products that are difficult to remove CIP systems, entire process area can be flooded Various diagnostic and monitoring systems Ferrum InertoSafe inertisation systems (PL d, SIL 2 certified) State of the art control systems and HMI panels VBC-S, Vertical scraper centrifuge with swivel open cover and housing 02 03

TYPE VBC-W SPECIAL DESIGN FEATURES Simple, fast disassembly of the basket for best inspection of the process area Clean room design using membrane connection possible Pressure vessel design on request Large diameter / radius for all connections allowing improved CIP efficiency, reduced CIP time and reduced CIP liquid requirements Light weight design for minimised static loads Reduced building volume requirements Complete flooding of the product contacted area possible VBC-W with housing welded directly onto base plate Centrifuge basket Scraper knife over the entire basket height, feed and wash pipe Scraper knife with vertical movement, feed and wash disk Drive and control unit P-100

TYPE VBC-C SPECIAL DESIGN FEATURES One piece stator, housing support and base plate cast iron construction Low centre of gravity for stable vibration free operation Design with flat cover (optionally with convex cover) Manual cover opening with lifting gear or with hydraulic activation High flexibility allowing client a high degree of freedom to influence final design features VBC-C with cast iron base TYPE VBC-S SPECIAL DESIGN FEATURES Swivel open convex cover for easy access to internals Swivel open housing for optimised inspection, even below the basket without the need to disassemble the basket Light weight design for minimised static loads Clean room design using membrane connection possible Minimised down time between product changes thanks to simple inspection of all product contacted parts VBC-S with housing open VBC-S with cover open

VERTICAL CENTRIFUGES TOP DISCHARGE PRINCIPLE OF OPERATION AND APPLICATIONS The VTC type vertical centrifuge (Vertical Top discharge Centrifuge) is used for batch type operations. The product is discharge through the top of the centrifuge. This design is suitable for products that can not be discharged using a scraper unit or in cases where crystal breakage must be prevented. The applications range from kilo-lab units and pilot plant scale to fullsize production units in the chemical and pharmaceutical industries. MODULARITY AND OPTIONAL EQUIPMENT Reliable sealing of the bearing housing using the latest generation of sealing systems Easy maintenance thanks to modular design Application-specific feed and wash systems Easy, quick disassembly of basket Robust and reliable design in accordance with the latest standards and directives State of the art control systems and HMI panels Various CIP systems 04 05

TYPE VTC SPECIAL DESIGN FEATURES Various solids discharge systems: manual discharge, filter bag lift-out devices Motor arrangement: above or below the base plate Light weight design with minimum loads on civil structure Cake loosening device with vertical movement Design allowing various positions for the filtrate discharge and cover opening Complete flooding of the product contacted area possible Filter bag with removable basket brim Lifting device for fi lter bag Discharge device for fi lter bag 06 07 Special design with enclosed motor compartment

TYPE VTC-M MOBILE SPECIAL DESIGN FEATURES Compact dimensions Swing-open housing for optimal inspection Designed for use in an Ex zone 1 area Complete mobile unit for easy transfer from room to room All instruments, motors and electrical components completely protected in a stainless steel housing TYPE VTC-I ISOLATOR SPECIAL DESIGN FEATURES Compact design ideal for installation inside an isolator Process area and technical area separated by using a membrane connection Various discharge systems: manual or using filter bag Easy inspection of product contacted parts even when installed in an isolator Isolator installation

BOTTOM DISCHARGE CENTRIFUGES PRINCIPLE OF OPERATION Highest efficiency Solid-liquid separation with the bottom discharge centrifuge is effected discontinuously in a sequence of specific process steps. The individual process steps last from a few minutes to several hours depending on the characteristics of the product. Depending on the type of control system, the process can be operated fully automatic, semi-automatic or manual. Feed and wash pipe, scraper knife over entire basket height Inclined feed and wash disk, scraper knife with vertical movement

Filling and intermediate centrifugation Washing Centrifugation Scraping, solids discharge Residual heel removal Basic design: feed pipe and wash pipe, scraper knife over the entire basket height Design with feed and wash disk, scraper knife with vertical movement Filling Intermediate centrifugation Washing Centrifugation Scraping, solids discharge Residual heel removal The suspension is applied evenly to the centrifuge basket via the feed pipe or optionally via the inclined feed disk. The fill level control prevents overfilling of the basket. The basket accelerates to centrifuge the liquid from the surface of the cake. After intermediate centrifugation, wash liquid is sprayed evenly on to the product cake; this liquid enters the centrifuge via the inclined feed disk or the wash pipe. After washing, centrifugation takes place until the required residual moisture of the filter cake is reached. At reduced speed, the scraper knife swings into the filter cake and scrapes out the product vertically downwards. If required, the residual heel removal on the scraper device can be switched on during scraping. The heel can be blown into the solids discharge using pressurised gas pulses applied via nozzles outside the basket or, if necessary, additionally via nozzles on the scraper device. If the process area is purged with inert gas, nitrogen is used for blowing off the heel. 08 09

TOP DISCHARGE CENTRIFUGES PRINCIPLE OF OPERATION Simple but proven The solid-liquid separation is effected discontinuously in a sequence of specific process steps. The individual process steps last from a few minutes to several hours depending on the characteristics of the product. Depending on the type of control system, the process can be automatic, semi-automatic or manual. Filling and intermediate centrifugation Washing Centrifugation Cake loosening device Solids discharge Design with cake loosening device and lifting device Filling Intermediate centrifugation Washing Centrifugation Cake loosening device The suspension is applied evenly to the centrifuge basket via the feed pipe or optionally via the inclined feed disk. The fill level control prevents overfilling of the basket. The basket accelerates to centrifuge the liquid from the surface of the cake. After intermediate centrifugation, the wash liquid is sprayed evenly on to the product cake; this liquid enters the centrifuge via the inclined feed disk or the wash pipe. After washing, centrifugation takes place until the required residual moisture of the filter cake is reached. The product can be released using a cake loosening device. Depending on the product, this will make subsequent discharge easier. Feed and wash pipe, cake loosening device Filter bag with lifting device 10 11 Special design with enclosed motor compartment

CIP AND SIP SYSTEMS PURE AND CLEAN CIP system For cleaning the centrifuge process area, a CIP system (Cleaning In Place) can be integrated in all our vertical centrifuges. This system is used during a product or batch change to eliminate the risk of cross-contamination. The CIP nozzles, the feed and wash system as well as the residual heel removal outside the basket can be used to clean the process area. SIP system After the CIP cleaning, SIP cleaning (Sterilisation In Place) can be undertaken. To kill microorganisms, the process area is wetted with disinfectant (e.g. hydrogen peroxide, sodium hydroxide, etc.) via the CIP system. Optional flooding of the process area The centrifuge can be flooded with CIP liquid to just below the cover. This process permits contact between the cleaning liquid and the soiled surfaces for as long as required and therefore maximum effect. GMP design for efficient cleaning Our designs comply with the latest GMP guidelines. The hygienic cleaning of the process area is made possible by a clean finish, excellent surface quality, compliance with minimum radii and the use of FDA-approved open O-rings. Low solvent consumption The compact design as well as optimised cleaning programs ensure efficient cleaning with low solvent consumption. Ribofl avin Test - before CIP VERIFIABLE CLEANNESS We optimise the CIP programs for the different centrifuge types with the aid of riboflavin tests. This way it is ensured that even with low solvent consumption, all surfaces in the process area are wetted with cleaning liquid. Riboflavin tests can be demonstrated on request during the FAT (Factory Acceptance Test). Ribofl avin Test - after CIP

AUTOMATION SYSTEMS RELIABLE CONTROL Automation of centrifuges is of central importance to Ferrum. Ferrum has invested many years into the development of centrifuge automation systems. Proven, standardised hardware and software modules are used as a basis and are supplemented with customer specific elements. OVERVIEW OF THE RANGE OF CONTROL SYSTEMS AND DRIVES Safety analyses, safety circuits Automation of the process, software programming Design and installation of cabinets for control systems and drives, as well as operator panels Sensors and monitoring equipment Connection to distributed control systems, remote maintenance Explosion protection up to Ex zone 1 (according to Directive 2014/34/EU) Documentation: diagrams, concept descriptions, operating instructions, safety certificates, etc. Commissioning of complete systems on-site DRIVE SYSTEMS AND SAFETY CONTROL SYSTEMS Our drive systems and safety control systems guarantee a safe and optimised operation of the centrifuge. The systems are state of the art. They are continuously developed and adapted to our risk analyses as well as to the latest directives and standards. Frequency converters of the latest generation with integrated safety functions are used to control the speed. CONTROL SYSTEMS AND TERMINALS TO FACILITATE EASE OF USE The control and visualisation software permits easy operation and control of the solid-liquid separation process. Thanks to our extensive range of different control systems, operator panels and components from leading suppliers, we efficiently implement comprehensive customer requirements. Ferrum can supply operator panels for fully automatic and visualised process control systems with integrated safety functions which can be controlled by a safety control system. The centrifuge can be operated in an automatic, semi-automatic, manual or service mode. A wide range of production recipes can be saved in an easy-to-use recipe management system. Terminal with process visualisation for Ex zone 1 Terminal with process visualisation for Ex zone 2 Special design with enclosed motor compartment

EXPERIENCE FERRUM INNOVATION PULL ACTION FILTER CENTRIFUGES The Pull Action Filter Centrifuge is an innovation by Ferrum which allows automatic discharge of the product without the use of a scraper knife system and therefore minimising crystal breakage. Bottom discharge of the solids by pulling the filter cloth using a pneumatic cylinder No scraper knife unit required No residual heel No crystal breakage 12 13

WORLDWIDE MAIN OFFICES SERVICE CENTRES REPRESENTATIVES 1 BRAND 3 BUSINESS UNITS CANNING TECHNOLOGY CENTRIFUGE TECHNOLOGY MANUFACTURING Ferrum Ltd. Centrifuge Technology Industriestrasse 11 5503 Schafi sheim Switzerland T 41 62 889 14 11 F 41 62 889 15 13 centrifuges@ferrum.net www.ferrum.net 06.18 en