Power Input of High-Speed Rotary Impellers K. R. Beshay, J. Kratěna, I. Fořt, O. Brůha

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Poer Input of High-Speed Rotary Impellers K. R. Beshay, J. Kratěna, I. Fořt, O. Brůha This paper presents the results of an experimental investigation of the poer input of pitched blade impellers and standard Rushton turbine impellers in a cylindrical vessel provided ith four radial baffles at its all under a turbulent regime of flo of an agitated liquid. The influence of the geometry of the pitched blade impellers (pitch angle, number of blades) and the off-bottom impeller clearance of both high-speed impellers tested on the impeller poer input is determined in to sizes of the cylindrical vessel (0.3 m and 0.8 m diameter of vessel). A strain gauge torquemeter is used in the small vessel and a phase shift mechanical torquemeter is used in the large vessel. All results of the experiments correspond to the condition that the Reynolds number modified for the impeller exceeds ten thousand. The results of this study sho that the significant influence of the separating disk thickness of the turbine impeller corresponds fairly ell to the empirical equations presented in the literature. Both the influence of the number of impeller blades and the blade pitch angle of the pitched blade impeller ere expressed quantitatively by means of the poer dependence of the recently published correlations: the higher the pitch angle and the number of blades, the higher the values of the impeller poer input. Finally, it follos from results of this study that the impeller off-bottom clearance has a eak influence on the poer input of the Rushton turbine impeller, but ith decreasing impeller off-bottom clearance the poer input of the pitched blade impeller increases significantly. Keyords: impeller poer input, Rushton turbine, pitched blade impeller. 1 Introduction High-speed rotary impellers are generally used for mixing lo-viscosity liquids and dispersions under a turbulent regime of flo of an agitated batch [1, 2, 3]. Their main advantage is that they can reduce investment costs for complex gear boxes because their high speed involves transferring the poer input from the driving motor to the impeller predominantly via frequency of revolution at a moderate level of torque. The main types of high-speed rotary impellers suitable both for blending pure liquids and for mixing solid-liquid suspensions, gas-liquid dispersions and liquid- -liquid emulsions are the standard Rushton turbine impeller (Fig. 1) and the pitched blade impeller (see Figs. 2 and 3). Their design is very ell defined and their manufacture is rather simple. The poer input of the standard Rushton turbine impeller (SRTI) and pitched blade impellers (PBI) has in many cases of impellers been studied experimentally, and the results of the experiments have been published in dimensionless form by means of similarity criteria [2] a [3]: 60 l Fig. 1: Sketch of Rushton turbine impeller (Czech standard CVS 691021) /T = 1/3, / =0.2, 1 / = 0.75, l/ =0.25 Po Po Re, geometry of the system (1) here the poer number P Po (2) 3 5 n and the Reynolds number (modified for impeller) Re n2. (3) The geometry of the agitated system is characterised simplexes of geometric similarity, e.g. H/T, /T, /T, h/t, n B, b/t, and t/ (see List of Symbols) necessary for scaling up the impeller poer input from the pilot plant to industrial size. For Reynolds number greater than ten thousand the poer number is independent of this criterion and Eq. (1) can be simplified into the form Po PoH T, T, h T, b T, nb, t (4) Published experimental studies have dealt ith a quantitative description (usually in the poer form) of dependence (4) both for SRTI [3, 4, 5, 6] and PBI [6, 7, 8, 9]. The results of these studies confirm the strong effect of various simplexes of geometric similarity on the impeller poer input, e.g., the relative thickness of the turbine separating disc t/ or the pitch angleofthepbi.ontheotherhand,theexperimentalstudies enable us to neglect the influence of certain simplexes on the impeller poer input, e.g. the vessel diameter/impeller diameter ratio /T of the SRTI or the relative thickness of the blades of the PBI. The aim of this study is to compare the experimentally investigated poer input of the SRTI and PBI determined in to mixing vessels of different sizes under a turbulent regime of an agitated liquid and look for the influence of the main geometric characteristics of the to impellers on the impeller poer input. The experimental results ill be expressed by means of the above introduced dimensionless variables, and the statistically calculated poer correlations ill be compared ith results published in the literature. 18 Czech Technical University Publishing House http://ctn.cvut.cz/ap/

/2 a) b) c) Fig. 2: Sketch of pitched blade impellers (Czech standard CVS 691020) /T =1/3,/ =0.2, = 45 o 2 Experimental The poer input of the SRTI and the PBI as investigated through measurements in to experimental test rigs having the same geometrical parameters as shon in Fig. 3. The first (larger) test rig, shon in Fig. 4, had a flat-bottom cylindrical vessel 0.8 m in diameter, made of Perspex and equipped ith four equally-spaced baffles mounted on the all and ith aidthofb = 0.1T. The orking fluid used throughout the measurements as ater, at a temperature of 20 C, hose height H as equal to the vessel diameter T. Thetorqueas h b n T H Fig. 3: Geometrical parameters of the agitated vessel. (H/T =1, b/t =0.1,/T =1/3) measured by a phase-shift mechanical torquemeter hose output, in the form of an electrical signal, as fed to a data acquisition system. The torquemeter as mounted, under the variable-speed driving motor, above the tank. The rotational speed as measured by means of a photoelectric cell and a notched disc mechanism. In the smaller-size test rig shon in Fig. 5, a flat-bottom, cylindrical vessel ith four baffles at its all, as again used. The vessel had a diameter of T = 0.3 m and as filled ith ater at temperature 20 C to a height of H = T. A strain gauge torquemeter, mounted on the motor shaft, as used to measure the torque, and the signal as fed to a data acquisition system. The rotational speed as measured, as in the case of the larger-size test rig, by a photoelectric mechanism. Table 1 shos the geometrical details of the impellers used in this study. For the large-vessel test rig three impellers ere investigated, namely: a standard Rushton turbine impeller (SRTI), a 6-blade pitched blade impeller ith blade angle = 45 (6PBI45) and a 4-blade pitched blade impeller ith = 45 (4PBI45). For the small-vessel test rig, to types of impellers ere investigated. These ere the Rushton turbine impeller (SRTI) and pitched blade impellers ith the folloing geometry: 6 blades and pitch angle = 45 (6PBI45), 4 blades, = 45 (4PBI45), 4 blades, = 30 (4PBI30), 4 blades, = 20 (4PBI20), 3 blades, = 45 (3PBI45), 3 blades, = 35 (4PBI35) and 3 blades, = 24 (4PBI24). All had a relative diameter /T = 0.33. All experiments ere made at three levels of off-bottom clearance, namely: h/t = 0.2, 0.35, 0.5 except for the SRTI, here measurements ere made at only to off-bottom clearances: h/t = 0.33 and 0.5. The off-bottom clearance as measured from the bottom of the vessel to the loer edge of the impeller using a ruler, ith a precision of ± 1 mm. The error in measuring the blade angle of the pitched blade impellers can be considered ± 1. A sufficiently ide range of Reynolds number as obtained by varying the rotational speed of the impeller (n). This quantity as kept constant during measurements to ithin ± 2 rpm. Therefore, the maximum experimental error Czech Technical University Publishing House http://ctn.cvut.cz/ap/ 19

Fig. 4: Layout of the large size test rig Table 1: Geometrical specifications of impellers Impeller t [mm] [mm] /T l/ / 1 / n B [deg] Large vessel STRI 2.50 260 0.33 0.25 0.2 0.75 6 90 6PBI45 255 0.32 0.2 6 45 4PBI45 260 0.33 0.2 4 45 Small vessel SRTI 1.55 100 0.33 0.25 0.2 0.75 6 90 6PBI45 100 0.33 0.2 6 45 4PBI45 100 0.33 0.2 4 45 4PBI30 100 0.33 0.2 4 30 4PBI20 100 0.33 0.2 4 20 3PBI45 100 0.33 0.2 3 45 3PBI35 100 0.33 0.2 3 35 3PBI24 100 0.33 0.2 3 24 encountered in measuring speed reached 2 % for lo Reynolds numbers (n = 200 rpm), hile this error fell to less than 0.25 % for higher Reynolds numbers (n = 1000 rpm). The main factors affecting the accuracy of the impeller poer input measurements ere the static and dynamic frictions. The static friction effect as reduced to its minimal value by using a proper bearing and driving motor. The most dominant factor, i.e., the dynamic friction, as closely monitored during the experiment to ensure that steady state values of the torque ere recorded. For this purpose, the motor as alloed to run before each set of experiments at high speed (1000 rpm) for one hour, in order to reach the orking temperatures of the bearings and motor. The motor as then set to the loest speed for the particular impeller and alloed to run for 5 minutes till steady state conditions prevailed. Passive torque (torque readings ithout installing the impeller) as then recorded for 3 minutes. Then the speed as increased by an increment of 40 rpm and the passive torque as recorded again for 3 minutes, and so on until the maximum alloable rotational speed as reached. The motor as then stopped and the impeller as attached and positioned at an off-bottom clearance level. The motor started once again at 20 Czech Technical University Publishing House http://ctn.cvut.cz/ap/

Fig. 5: Layout of the small size test rig the loest measuring speed and as left for 5 minutes before recording the torque. Torque data as then collected for 5 minutes, and three collections ere recorded at each speed and off-bottom clearance to obtain the average poer input. The passive torque as measured once again at the end of each speed range. This experimental technique as repeated for each impeller and at each off-bottom clearance for both test rigs. The average poer number of each impeller across a speed range as then calculated. The average relative standard deviation ascalculatedandfoundtobeintherange2.3 16%.This experimental methodology as adopted to completely eliminate the dynamic resistance of the equipment. 3 Results and iscussion The mean poer number defined as the average poer number across the speed range of the impeller (from lo speed to the speed at hich aeration occurs) as measured by Table 2: Average values of Po (T =0.8m) Impeller SRTI Poer Input Measured at h/t =0.33 h/t =0.5 6.51 6.32 h/t =0.2 h/t =0.35 h/t =0.5 6PBI45 1.63 1.52 4PBI45 1.48 1.31 1.20 the large vessel test rig. The results for the three impellers investigated are reported in Table 2, at the above mentioned off-bottom clearances. The corresponding results obtained using the small vessel test rig are given in Table 3 for the eight impellers studied. Table 3. Average values of Po (T =0.3m) Impeller Poer Input Measured at h/t =0.33 h/t =0.5 SRTI 5.41 5.44 h/t =0.2 h/t =0.35 h/t =0.5 6PBI45 1.84 1.69 1.55 4PBI45 1.44 1.28 1.22 4PBI30 0.71 0.64 0.59 4PBI20 0.32 0.29 0.28 3PBI45 1.16 1.04 0.97 3PBI35 0.75 0.69 0.65 3PBI24 0.39 0.36 0.33 The experimental results for the SRTI obtained by the large test rig here the Reynolds number as in the range 1.510 5 <Re<310 5 and those obtained using the small test rig in the range 310 4 <Re<610 4 sho more or less constant poer input over Reynolds number range. Only a 4 % change of Po is observed in the recorded date, in accordance Czech Technical University Publishing House http://ctn.cvut.cz/ap/ 21

ith [3], although a change of 10 % [5] and even larger changes [6] have been reported. Another significant result obtained from Tables 2 and 3 is that the poer input of SRTI varies very slightly (almost constant) ith off-bottom clearance. Only a change of 3 % is observed in Po due to change of C/T from 0.33 to 0.5. This agrees ell ith the literature [3, 9]. No, the poer inputs of the present study are compared ith those obtained from the empirical correlation proposed by Bujalski et al [4], relating the poer number to the relative blade thickness (t/) and the vessel diameter, via: 0. 195 0. 063 t T Po 2512., (5) T0 here T 0 = 1 m. Good agreements are obtained, e.g., for the large test rig Po = 6.2 compared to an averaged value of 6.4 of the present study, and for the small test rig the agreement is even better, i.e., Po = 5.3 compared for 5.425 for the present ork. Similar findings ere also reported by Rutherford et al [5]. The effect of the off-bottom clearance as investigated in the present ork for the pitched blade impellers in both the large and small vessel test rigs. It is clear from the values reported in Tables 2 and 3 that Po decreases, as expected, ith increasing h/t, in agreement ith previous investigation [7]. Asthepitchedbladeimpellerspumptheflodonards, it creates a region ith large turbulence underneath it. For the smaller bottom clearances, the fluid velocities in the region bounded by the vessel bottom and the impeller are higher, and thus higher friction and higher rate of mechanical energy dissipation are generated, hich leads to higher poer numbers. For higher off-bottom clearances, loer turbulence leads to loer poer numbers. The effect on poer input of the number of blades of the pitched blade impeller at = 45 and the effect of changing at n B = 4 and 3 ere also investigated in the present ork at different off-bottom clearances. The poer input data are depicted in Table 3. These and other data for the pitched bladeimpellerereusedtoobtainacorrelationintheform: 0996 0 682 0. 178. h Po n 1. 995. B sin. (6) This formula correlates the poer input of the pitched blade impeller to the different parameters investigated. The average error (difference beteen the measured values and those obtained from the correlation) as found to be 1.49 %. This correlation can be compared ith a similar general correlationfoundbymedek[7]givenintheform: h T H Po 1507n 0 701 0. 165 0. 365 0. 140. 2. 077. B sin (7) T hich as reduced, according to the present geometry, i.e., T/ =3andH/T =1.0,totheform: 10092 0 701 0. 165. h Po n 2. 077. B sin (8) A close inspection of Eq. (6) and Eq. (8) reveals that the present results correlate ell ith those of Medek [7]. In fact the to correlations are almost identical since the variation in the constant and the various exponents are negligibly small. 4 Conclusions The poer input of the pitched blade impellers and the standard Rushton turbine impellers ere investigated using to cylindrical vessels of different diameters. The effect of several parameters including the vessel diameter, the off-bottom clearance, the number of blades of the pitched blade impellers and the pitch angle ere studied. It has been found, for SRTI, that Po remains almost constant over the tested Reynolds number range and it also remains constant at off- -bottom clearances greater than 1/3. A correlation relating the poer input of the pitched blade impeller to the number of blades, off-bottom clearance and the pitch angle as obtained from the measured data and compared ith the corresponding correlation and good agreement as obtained. Acknoledgement This research has been subsidised by Research Project of the Ministry of Education of the Czech Republic J04/98: 212200008. List of Symbols b h H l n n B P Po Re t T baffle idth, m impeller diameter, m off-bottom clearance, m total liquid depth, m idth of Rushton turbine discs, m rotational speed, rps number on blades poer required by the impeller, W poer number Reynolds number thickness of Rushton turbine disk, m vessel diameter, m height of blades, m pitch angle, dynamic viscosity of agitated liquid, Pas density of agitated liquid, kg/m 3 References [1] Holland, F. A.. Chapman, F. S.: Liquid Mixing and Processing in Stirred Tanks.NeYork,ReinholdPubl.Corp., 1966 [2] Nagata, Sh.: Mixing Principles and Applications. Tokyo, Ne York, Kodansha Ltd., John Wiley and Sons, 1975 [3] Strek, F.: Mixing and Mixing Equipment (in Czech). Prague, SNTL, 1997 [4] Bujalski, W., Nieno, A. W., Chatin, S., Cooke, M.: The ependency on Scale of Poer Numbers of Rushton isk Turbine. Chem. Eng. Sci., 42 (2), 1987, pp. 317 326 [5] Rutherford,K.,Mahmoudi,S.M.S.,Lee,K.C.,Yianneskis, M.: The Influence of Rushton Impeller Blade and isk Thickness on the Mixing Characteristics of Stirred Vessel. Trans. Inst. Chem. Engrs., 74 (part A), 1996, pp. 369 378 22 Czech Technical University Publishing House http://ctn.cvut.cz/ap/

[6] Chapple,., Afacan, A., Kresta, S. K.: The Effect of Impeller and Tank Geometry on Poer Number for a Pitched Blade Turbine. Trans. Inst. Chem. Engrs, (in press) [7] Medek, J.: Poer Characteristics of Agitators ith Flat Inclined Blades. Int. Chem. Eng., 20 (4), 1980, pp. 664 672 [8] Medek, J.: Hydrodynamic Characteristics of Pitched Blade Impellers (in Czech). Technika v Chemii, 74, 1991, pp. 22 28 [9] Ibrahim, S., Nieno, A. W.: Poer Curves and Flo Patterns for a Range of Impellers in Netonian Fluids: 40<Re<510 5. Trans. Inst. Chem. Engrs., 73, 1995, pp. 485 491 r. Karam R. Beshay phone: 002 02 2408223 fax: 002 02 5714185 e-mail: krbeshay@hotmail.com Mech. Eng. ept. Faculty of Engineering Cairo University Cairo, Egypt Ing. Jiří Kratěna oc. Ing. Ivan Fořt, rsc. phone: +420 2 2435 2713 fax.: +420 2 2431 0292 e-mail: fort@fsid.cvut.cz epartment of Process Engineering oc. Ing. Oldřich Brůha, CSc. epartment of Physics Czech Technical University in Prague Faculty of Mechanical Enginering Technická 4, 166 07 Praha 6, Czech Republic. Czech Technical University Publishing House http://ctn.cvut.cz/ap/ 23