Overview of Haarslev s Approach to THP

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Overview of Haarslev s Approach to THP Josh Mah 2017 Biosolids Workshop Ohio Water Environment Association Master Your Process

INTRODUCING HAARSLEV INDUSTRIES - Global market leader in rendering - Headquartered in Denmark - Founded in 1973 - ~1200 Employees - Revenue just shy of $300M (in USD) in 2016-25 offices serving 120 countries (US HQ Kansas City, MO) - Factories in Denmark, Germany, China, Turkey, Peru, Brazil, US - 17 service centers globally

HAARSLEV INDUSTRIES - Cooking tough industrial materials since 1973 - Atlas-Stord: Batch thermal hydrolysis for ~60 years - Continuous hydrolysis of feathers and hair: Patented in 1986 - Complete line of animal carcass handling equipment - Fish factories in Artic/Antarctic ship hulls: 24/7 365 - Main products of the Environmental Division: Continuous Thermal Hydrolysis System Sludge Belt Dryers and Disc Dryers Waste Food Depacker

SOME QUESTIONS ABOUT THP? - How hard is it to operate? - How complicated or complex is the THP unit? - How big is the THP system? - How many moving parts need to be maintained? - What do you want to get out of THP? - How does continuous THP work? - What are the benefits of continuous THP?

HAARSLEV S CONTINUOUS HYDROLYSIS SYSTEM - THP = Cooking sludge = Not magic! - Target 160C for 30 minutes - Potential vendor differentiators: Quality of thermally hydrolyzed sludge Quality of mechanical components Thermal and electrical efficiency Footprint Capital Cost and Operating Cost Simplicity (Operations and Maintenance)

HAARSLEV S CONTINUOUS HYDROLYSIS SYSTEM - Continuous System: Preheater is fed continuously from pre-dewatering (typically a cake bin) The Pressurizer feeds 1/40 th of main reactor volume every ~90 seconds - Think of this like a piston pump After sludge leaves the pressurizer, remainder of process operates with continuous flow

KEY ASPECTS OF OUR SLUDGE COOKING PROCESS - Significantly different way of heating the sludge No indirect heat exchangers (i.e. tube-in-tube) Direct steam injection (8 bar required, 10-12 bar supply typically) Steam is injected into small (50 gallon) batches of sludge every 90 seconds Steam is used to push the liquified sludge into the main reactor vessel Very few pumps, motors or moving parts High turndown ratio and relatively smooth steam demand Permits feed TS to at least 22%, which increases throughput and reduces steam consumption on a dry solids basis

KEY ASPECTS OF OUR SLUDGE COOKING PROCESS - Completely different way of cooling the sludge No indirect heat exchangers (e.g. tube-in-tube) Direct evaporation with an indirect condenser Might sound complicated and confusing, but it is as simple as it gets Basically, non-contact cooling Moving parts = some valves, discharge pump, vacuum pump, cooling supply pump Condenser is extremely compact relative to other solutions Permits up to 22% TS cake feed - Sludge cooler may not be necessary with WAS-only THP configurations

Feed pump Cooling water T = 15 C Q = 4 m³/t wet sludge Condenser Gases to digester or Odour treatment Vacuum pump Vapour (recycled steam) Scrubber Dewatered Sludge DS = 14-22 % T = 15 C Reactor Economiser Cooler Condensate pump Feed pump Preheater T = 85 C Pressuriser T = 130 C P = 0-8 bar T = 165 C P = 6 bar T = 105 C P = 0.2 bar T = 60 C P = -0.8 bar Steam T = 180 C P = 10 bar Dilution water T = 15 C Feed pump Product pump To digester DS = 10 % T = 40 C

HAARSLEV S PREHEATER - Triple purpose Dispose of used steam Recover thermal energy from used steam Reduce viscosity of cake fed to pressurizer - Mechanically agitated Reduces backpressure on economizer, which improves thermal efficiency Permits up to 22% TS cake feed Not a pressure vessel Operates under very slight vacuum to contain odors

HAARSLEV S PRESSURIZER - A feed pump to the main reactor using steam as the piston - Small 12 bar pressure vessel (~200 liters) - 90 second operating cycle - Cake fed by PC pump at atmospheric pressure (steam off) - Feed valve closed, steam valve opened - Heating / pressurizing for ~45 seconds to 8 bar (~90% total steam dose) - Valve to main reactor opens, flow to 6 bar by differential pressure - Steam and discharge valve close, cycle repeats - Well-proven system in rendering

HAARSLEV S MAIN REACTOR - Feed to top of reactor vessel from pressurizer - Sludge is liquified at this point - Downward plug flow - Typical 30 minute retention time (2-12 cubic meters) - Additional steam fed into headspace to maintain temperature (~10%) - Discharge regulated by nozzle and automated valve - No mechanical agitator in the pressure reactor - No radioactive level sensors

HAARSLEV S ECOMOMIZER - Receives depressurized sludge from main reactor vessel - Target pressure of 0.2 bar gauge (~105C) - Flashed steam returned to preheater - Vessel is typically ½ the volume of main reactor - Not necessarily a pressure vessel

HAARSLEV S SLUDGE COOLER - Conceptually: reverse action of a steam boiler - Two parts: Cooling vessel - another tank (not a pressure vessel) A tube-in-shell condenser Headspace of cooling vessel connected to condenser by large diameter pipe - Steam is condensed on the inside wall of the condenser - As volume is collapsed from vapor to liquid, vacuum is created - Steam vapor in hot sludge is evaporated under vacuum - Thermal energy is extracted from the sludge to the condenser - Result is non-contact cooling of sludge in one tank by separate condenser

Feed pump Cooling water T = 15 C Q = 4 m³/t wet sludge Condenser Gases to digester or Odour treatment Vacuum pump Vapour (recycled steam) Scrubber Dewatered Sludge DS = 14-22 % T = 15 C Reactor Economiser Cooler Condensate pump Feed pump Preheater T = 85 C Pressuriser T = 130 C P = 0-8 bar T = 165 C P = 6 bar T = 105 C P = 0.2 bar T = 60 C P = -0.8 bar Steam T = 180 C P = 10 bar Dilution water T = 15 C Feed pump Product pump To digester DS = 10 % T = 40 C

Sludge from preheater Steam P V V Pressurizer: Working volume is 1/40 th of the Hourly flow capacity 0 8 bar cycles every 90s Main reactor: 62.5% working volume (at 30 min HRT, hourly flow capacity is 1.25 the tank volume) Additional steam Economizer ( flash tank ): Receives depressurized sludge at 0.2 bar gauge) Recycle steam to preheater Cooler (2 nd flash tank): Operates under -0.8 bar gauge) 6 bar constant 0.2 bar constant -0.8 bar constant Larger diameter vapor pipe (8-12 ); vapor velocity at up to 50m/s Vapor Pipe P Cooling water return Condenser: Tube-in-shell condenser with high density bundle of small (~1/2 dia) cooling elements Vacuum purge Collapsing water vapor in condenser drives the vacuum Condensate out (can feed back to sludge as dilution water) Cooling water supply V Pressurizer: Cycles from unpressurized cake feeding through 90% steam delivery every 90 seconds (40 times per hour). 90% of steam dose delivered in the Pressurizer Downward plug flow The pressure release from 6 bar to ~ ATM is how thermal energy is released Similarly, the pressure release from ~ ATM to -0.8 bar is how thermal energy is released V HCHS 2 = 2 cubic meter total reactor volume = 2.5 cubic meters per hour throughput Flow rate control device (not exactly a valve) P Cooled sludge

Reference WWTP Grevesmühlen, Germany Application: Client: Location: Size: HCHS 2 Product: Zweckverband Grevesmühlen WWTP Grevesmühlen, Deutschland Secondary and digested sludge Steam production: exhaust heat of CHP Throughput: 2 t/h (wet) 8 10 t DS /d Dry Solids: Dewatering 1: 15-20% Dewatering 2: 33% Spec. steam cons.: 190 kg Steam /m³ Spec. elec. cons. Operation time: Commissioning: 2014 5 kwh/t wet sludge 24 h/d, fully automatic

Reference WWTP Wola Dalsza, Łancut, Poland Application: Client: Location: WWTP Wola Dalsza Łancut, Poland Size: HCHS 2 Product: Primary and secondary sludge Steam production: burning of biogas Throughput: 1.1 t/h (wet) 4.2 5.3 t DS /d Dry Solids: Dewatering 1: 16-20% Dewatering 2: 31% Spec. steam cons.: 170 kg Steam /m³ Spec. elec. cons. Operation time: Commissioning: 2014 4 kwh/t wet sludge 24 h/d, fully automatic

Reference WWTP Wola Dalsza, Łancut, Poland Reactor Economiser Cooler Condenser Pressuriser Feed

VALUE OF A CONTINUOUS PROCESS - Continuous process flow results in optimized vessel sizes and energy recovery Lower peak flowrates -> smaller vessel sizes - Lower capital cost - Reduced footprint Continuous steam consumption at all capacities Indirect evaporative cooler is a substantially smaller heat exchanger

VALUE OF HIGHER DRY SOLIDS CONTENT - Higher %TS feed results in higher dry solids throughput Flexible in dry solid content with a range of 14-22% DS Operation at higher solid content improved steam economy - Effect of increasing DS from 16.5% to 22 % 33 % increased capacity of the same installation 28 % reduced steam consumption 16.5 % DS 22 % DS Flow to HCHS (t/h) 9,9 6,9 Steam consumption (t/h) 1,6 1,1 Steam consumption kg/t DS 978 705

COMBINING THP WITH THERMAL DRYING - Reduced anaerobic digester volume from THP - Reduced water evaporation load from better dewatering = smaller dryer - Use of primary sludge for cooling and dilution of hot hydrolysed secondary sludge can eliminate the cooling requirement - Alleviates the need to rely completely on the AD for Class A Digester Hydrolysis Anaerobic Digestion De-watering Low temperature Belt-Drying

HAARSLEV S LOW TEMPERATURE BELT DRYER

HAARSLEV S DISC DRYER

THANK YOU FOR YOUR ATTENTION! - Josh Mah Process Engineer / Technical Sales Joshua.Mah@Haarslev.com - Keith Hamilton Director of Sales and Marketing, Environmental Division Keith.Hamilton@Haarslev.com - Haarslev, Inc. (USA) 9700 NW Conant Av Kansas City, MO 64153 - Haarslev.com

Cooling water T = 15 C Q = 4 m³/t wet sludge Condenser Gases to digester or Odour treatment Vacuum pump Scrubber Vapour (recycled steam) Dewatered Sludge DS = 14-22 % T = 15 C Reactor Economiser Cooler Condensate pump Preheater T = 85 C Pressuriser T = 130 C P = 0-8 bar T = 165 C P = 6 bar T = 105 C P = 0.2 bar T = 60 C P = -0.8 bar Steam T = 180 C P = 10 bar Dilution water T = 15 C Feed pump Product pump To digester DS = 10 % T = 40 C