WHITE PAPER: IMPROVED RELIABILITY AND SAFETY IN A NEW STATE OF THE ART FABWIDE HEAT SOURCING AND CONTROL SYSTEM

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WHITE PAPER: IMPROVED RELIABILITY AND SAFETY IN A NEW STATE OF THE ART FABWIDE HEAT SOURCING AND CONTROL SYSTEM SAFETY AND RELIABILITY Applicable to ammonia, CO 2, and other gases requiring hea ng before delivery to tool. ABSTRACT Customer feedback, opera ng experience and evolving control technology have contributed to the development of the Versum Materials GASGUARD ev Heat Control System, designed to deliver state-of-the-art fabwide heat sourcing and control of electronic specialty gases requiring hea ng before delivery to the tool. In comparison with current methods used to heat cylinders of ammonia, CO 2 and other gases, the ev Heat Control System is a self-contained system with state-of-the-art over-temperature protec on, a single power feed, GFCI protec on, integrated monitoring and control, and Class 1, Division 2 approval. These improvements are expected to enhance the reliability and safety of gas hea ng systems and further lower the cost of ownership for semiconductor manufacturers, research and development organiza ons, universi es, and others who use electronic specialty gases and chemicals. INTRODUCTION About one-third of the gas cabinets in a fab have heat tracing; large fabs may have hundreds of such cabinets. Obviously, lowering the cost of ownership for equipment for hea ng certain electronic specialty gases is vital to semiconductor manufacturers, in addi on to achieving enhanced reliability and safety. Today s typical heat control systems, introduced in 1999, are similar to the GASGUARD Legacy Heat Trace System shown in Figure 3. While these systems con nue to operate safely and reliably, there is room for improvement, especially in developing more customer-friendly features. Fig. 3 GASGUARD Legacy Heat Trace System Retransmit signal of temperatures. Requires standard customer board (monitoring, no control) AP11 Retransmit signal of temperatures. Requires standard customer board and thermocouple kit (monitoring, no control) Heat Heat Trace Thermocouples Temp Control and Thermocouples Temp Control and Heat Blanket (Silicone and Insula on) Heat Trace

The latest GASGUARD ev Heat Control System shown in the Figure 4 block diagram is a four-zone heat control applica on that incorporates several key improvements: Lower installa on costs Over temperature protec on reliability Integrated solid-state monitoring and control Stronger, single piece blanket. Single power feed GFCI protec on Class 1, Division 2, ATEX, CE, CSA and other approvals Equally important, this latest heat control system is self-contained, which eliminates issues associated with, for example, remote loca ons for the blanket controller and other electrical components. : 120VAC or 208-240VAC to AP11 Heater AP 11 Thermocouples (4x) Overtemp Switches (2x) Cabinet with 2 blankets and 2 heat traces Fig. 4 System Architecture Control Signals to Blankets and Heat Trace SYSTEM OVERVIEW This latest addi on to the evolving GASGUARD delivery systems and equipment product line introduced by Air Products in 1983, includes a GASGUARD AP11 controller, a GASGUARD AP1602 ECC heater/controller board and a gas cabinet with two blankets and two heat traces that can accommodate two A or B size cylinders with automa c crossover and automa c purge. A second cabinet version is available that will accommodate three cylinders, the third being a purge cylinder that does not require hea ng. The Versum Materials GASGUARD ev Heat Control System incorporates a newly redesigned heater blanket manufactured and supplied by blanket, Salt Lake City, Utah. INDIVIDUAL COMPONENTS AP11 : A key feature of the 8-inch high controller mounted on the top of the cabinet is its user-friendly 10.4 color touch screen for all data entry, i.e. set points, and for con nuous heat trace monitoring, which helps ensure that any problems that do occur can be quickly addressed. (Figure 5) The fully configured and fully automated modular AP11 controller displays more informa on for the ev heat control system, including its two heat trace and two blanket temperature readings and alarm set points. The controller s high-speed microprocessor means faster screen updates. Other advantages of the state-of-the-art AP11 controller are solenoid management allowing uninterrupted gas supply while the controller is in service, simplified troubleshoo ng using smart indicators, its focus on reliable performance based on its design and tes ng processes, for example, HALT methodology and an op onal Auto Recovery System (ARS) that provides a second microprocessor for redundancy and to enhance up me. Fig. 5 AP11

AP1602 Heater/: This specially designed heat control board is located inside of the AP11 controller is responsible for the integrated monitoring and control of temperature and protec on against cylinder overhea ng. (Figure 6) Fig. 6 Packaging Fig. 7 Blanket on Cylinder Blanket: The nine-layer silicone rubber blanket has single-piece construc on for both the heater and insula on, dual voltage (120V or 208-240V), and hardwired over temperature protec on via redundant bimetallic switches for central and redundant thermocouples. A single blanket part number covers all A and B cylinders. (Figure 7) DESIGN HIGHLIGHTS The design team that developed the Versum Materials ev Hea ng Control System addressed and solved several perceived issues with current heat sourcing: Liquefied compressed gases are hazardous and must be safely used. By increasing over-temperature protec on reliability, cylinders are protected against overhea ng. Safety redundancy is also built in Rather than undergoing a peaks and valleys flow of heat, the ev system with its diversifica on of method provides very steady temperature and pressure to ensure uninterrupted gas flow. Oscilla on is measured at less than a degree The blanket is considered to be an innova on. Stronger, made from silicone rubber and now a single piece, it means faster cylinder changes. Heat trace components are included and the blanket is already wired into the system By incorpora ng everything into a single cabinet and one loca on, issues that can result from dealing with remote equipment, such as blanket controllers, or miswiring of cable ends in two loca ons, are eliminated Customers are freed from dealing with most power requirements and cer fica ons, which means significant savings in installa- on costs. The pre-tested, skid-mounted ev system is virtually a single plug-in to a standard breaker. No holes have to be drilled in the cabinet. Previously, there were five on-site power connec ons required of the end user. GFCI protec on is now included, and the system is approved for Class 1, Division 2. It is approved for shipment globally The life span of the ev system has been extended, largely by the replacement of electromechanical switches with solid state circuitry Heat trace switches in current systems can only be reset by removing the cylinders. The new system allows all se ngs to be changed via the AP11 controller screen.

Requirements: Voltage: 120V or 208-224V Single Phase : 100-150 VA Typ./Frequency: 50 to 60 Hz/ Current: 30 AMP Max. Pneuma cs: 85 PSIG (586 Kpa) to 95 PSIG (655 Kpa) Relay Outputs: Form C (Single Pole Double Throw) Dry Contacts Max 24 VDC 1.0 AMP Hard Conduit or Wireway (By Customer) A ached Conduit Ground Clamp Use ALPHA *1239 1 32/8 (34.9mm) Flat Braid or equiv. Fig. 8 GASGUARD ev schema cs SPECIFICATIONS Size Weight Single Feed: ed Separate from Heaters (2-Cyl): Heaters ed Separate from Heaters (3-Cyl): Heaters 2-Cyl: 92.1875 H x 24.125 W x 26.4375 D 3-Cyl: 92.1875 H x 38.125 W x 26.4375 D 2-Cyl: 425 lb. empty 3-Cyl: 525 lb. empty 2-Cyl: 120 VAC, 12A, 50/60Hz, 3-wire or 3-Cyl: 208-240 VAC, 6A, 50/60Hz, 3-wire 120 VAC, 11A, 50/60Hz, 3-wire 100-240 VAC @ 150 VA maximum, 50/60Hz, 3-wire or 208-240 VAC, 6A, 50-60Hz, 3wire 100-240 VAC @ 150 VA maximum, 50/60 Hz, 3-wire

SUMMARY As designed, and compared with currently available systems, the Versum Materials ev Hea ng Control System offers the best available technology for fabwide heat sourcing and control for ammonia, CO 2 and other specialty gases. Among its many advances are improvements in reliability, safety, monitoring and control, over-temperature protec on reliability, power requirements, installa on costs and blanket design. CONTACT Kerry M. Lanza: kerry.lanza@versummaterials.com For more informa on, please contact us at: VERSUM MATERIALS, INC. VERSUMMATERIALS.COM The informa on contained herein is offered without charge for use by technically qualified personnel at their discre on and risk. All statements, technical informa on and recommenda ons contained herein are based on tests and data which we believe to be reliable, but the accuracy or completeness thereof is not guaranteed and no warranty of any kind is made with respect thereto. Versum Materials, Inc. 2017 325-16-008-GLOBAL-Mar17