Document Number March 23, 2016 Yokogawa Electric Corporation. Data Acquisition/Recorder. Data Acquisition and Monitoring. Paperless Recorder

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Yokogawa Field Instruments Pressure & Temperature development & Process Analyzers from a engineering perspective Erik Visser & Loek van Eijck 16-11-2017 1 Yokogawa Industrial Automation Data Acquisition/Recorder Controller Production Management Asset Management and Operational Efficiency Data Acquisition and Monitoring Analytical Paperless Recorder Chart Recorder Single Loop & Temperature Controller Signal Conditioner Power Monitor Production Control and Safety Management Oxygen Analyzer ZR Pressure ph Transmitter FLXA21 Level Conductivity Transmitter FLXA21 TruePeak Tunable Diode Laser TDL Process Gas Chromatograph GC8000 Wireless FT-NIR Data Acquisition and Logic Control Analysis and Quality Control Pressure/Differential Pressure EJA-E/EJX Flow Differential Pressure EJA-E/EJX with seals Field Wireless Temperature Sensing and Actuation Variable Area Rota Meter Coriolis Rota Mass Vortex DY-F Differential Pressure EJA-E/EJX Magn. flow AXF/RXF/AXR DTSX 1

Pressure Transmitters EJX EJA-E Multi-Variable Pressure Transmitters (only EJX) EJX Wireless 3 Dpharp Specification DPharp Evolution & History 4 2

Piezo-element based transmitters 5 Single Crystal Materials Single crystal materials have the following generic properties; Superior elasticity High long term stability Hysteresis free Therefore sensors based upon these materials are able to offer higher long term precision Sapphire Silicon Quartz Ruby Diamond Page 6 3

The Resonant Sensor 7 Working Principle of the Sensor 8 4

Dpharp Specifications Multi-Sensing principal (DP/SP sensing) Resonator 1 Resonator 2 Tension ε ε L H Compression L Resonator 1 Resonator 2 ε ε L H Compression SP P ε H P SP Frequency (khz) 150 120 90 60 DP f1 f2 Frequency (khz) 150 120 90 60 SP f1 f2 30 5,000 10,000 30 5,000 10,000 9 EJX & EJA 10 5

DPharp App 11 Distributed Temperature Sensor E. Visser 6

Introduction DTS Technology The fiber optic Distributed Temperature Sensing (DTS) method using the Raman-effect has been developed at Southampton University in England, UK in the early 80 s. The DTS method is based on Optical Time-Domain Reflectometer (OTDR) technology and uses a technique derived from telecommunication cable testing. The fiber optic-based DTS method measures temperature using optical fiber instead of thermocouples or thermistors DTS systems represent a cost-effective method for obtaining thousands of accurate, high-resolution temperature measurements. DTS technology offers a safe and non-intrusive measurement with has the capability to pinpoint the precise location of any warm or cold spot instantly. Distributed Temperature Sensor (DTS) Optical Fiber is Temperature Sensor DTS Instrument (interrogator) Safe No electronics explosion proof & non-inductive Distributed Measurement: Every 1m average temperature measurement of 30km fiber = 30,000 sensors! T 1 T 2 T 3 T 4. Backscattered light provides temperature at every 1m. Multi-mode optical fiber 1m light pulse Specialty Optical Fiber Cable (example) T 29,996 T 29,997 T 29,998 T 29,999 T 30,000 7

Distributed Temperature Sensor (DTS) Principle Measurement Distributed Measurement - 1m spatial resolution Measurement of 50 km Optical fiber = 50,000 sensors! Backscattered light provides temperature at every 1m Standard multi-mode optical fiber DTS Instrument (interrogator) T 1 T 2 T 3 T 4. Distributed Temperature Sensor (DTS) Principle Spectrum Light is backscattered from natural anomalies within the fiber This happens at all points within the fiber Range gating allows specific sections along the fiber s length to be examined laser pulse Backscattered light laser detection Scattered light spectrum Optical fiber Raman Anti-Stokes Raman Stokes Temperature dependent Frequency shift 8

DTS Measurement Principle Principle Spectrum annotation by SensorTran Main Specification Item DTSX200(Mid-Range) Specification DTSX3000(Long Range) Distance range 6km 10, 16, 20, 30, 50Km Performance Temperature resolution (1 Sigma) 0.2 ºC ( 3 km, 10 min ) 0.6 ºC ( 3 km, 1 min ) 1.1 ºC ( 3 km, 10 sec ) 0.03 (10Km, 10min ) 0.06 (16Km, 10min ) 0.20 (30Km, 10min ) Spatial resolution 1m 1~2m Optical switch 2ch, 4ch, 16ch (Option) Measurement temperature range -200 ~ +500 ºC (depends on the optical sensor cable specification) Operation ambient Network interface Ambient temperature Ambient humidity LAN -40 ~ + 65ºC 20 80% RH (no condensation) Modbus/TCP HTTP(S) PUT/GET (Secured Protocols) SFTP/SCP (Secured Protocols) Power consumption 10W (Operating) 2W (Power saving) 16W (Operating) 2.W (Power saving) 9

Temperature Resolution Resolution Distance Longer the Fiber Length Less accurate temperature measurement Longer the Measurement time More accurate temperature measurement DTSX Applications 10

Applications: Pipeline Leak Detection Quick detection of small leakage events and monitoring of the pipeline temperature profile. Pipelines such as LNG, LPG, ammonia, ethylene create cold zones which can be easily detected when leaks occur. DTSX3000 LNG Tank lead detection DTSX can identify small leakage Outer Tank Inner Tank Optical Fiber Cable (with SUS tube) Splicing Box CH1 CH2 DTSX200 Detecting the leakage 22 11

Applications: Downstream and Others Refinery and Plants Vessel Hot Spot Tank & Pipeline Leak Detection Fire Detection Industrial Facilities Tunnels Structures & Buildings Process Analyzers from a engineering perspective Loek van Eijck Analyzer Center Europe November 2017 24 12

Yokogawa Analytical History YOKOGAWA founded as electric meter research institute As of January 2017 1915 1959 1965 1977 1985 1995 2005 2015 2016 1917 First electronic meters in Japan 1957 First 4 W Tx in Japan 1959 First GC in Japan 1915 Founded by Dr. Tamisuke Yokogawa 1970 First Zirconia in Japan 1975 1994 World s 1 st World s 1 st PTB & Online BASEFA Sensor certified 2W diagnostics Transmitter EXA 402 1994 2. Generation GC 2005 World s 1 st Touch screen liquid analysers United Control Houston 1967 founded as independent system integration company 1985 Incorporated as 1997 Yokogawa Measurementation Electric Inc. Corporation acquired 51% of MI Analytical Specialties 1994 TDLS manufacturer Reflux sampler manufacturer 1998 Established Singapore Operation, MS Pte Ltd 2011 3. Generation GC 2000 Yokogawa Electric Corporation 100% of MI 2008 M&A of Analytical Specialties 2015 World s 1 st TDLS with SiL 2, in built reference cell Joined Yokogawa 25 Process Analyzers Solutions 26 13

Analyzer Solutions Why do we need process analyzers? Each plant has a laboratory for measuring chemical components and/or physical properties So, WHY? - Fast results - No human interference - No influence on sample composition 27 Analyzer solutions contribute to the plant performance Process Analyzers contribute to: Product Quality Throughput / Yields Optimization Debottlenecking of the plant unit Increase yield of product (control of chemical reaction) Plant Safety Prevention of explosions Health safety aspects 14

System Integration solution Process Analyzer 80 % of Analyzer System problems are caused by a wrong design of the Sample Conditioning System Engineering To implement a process analyzer require engineering Site Survey/Feasibility study Front End Engineering design Project management & Detailed engineering In-house fabrication and assembly In-house Testing & FAT (acceptance test) Start-up/Commissioning Maintenance support 30 15

Overview Process Analyzer System Flowchart Process Plant Control Shelter or Cabinet 1 2 3 DCS 1 Sample Preconditioning System 2 Sample Conditioning System 3 Analyzer Deliverables Yokogawa Analyzer Solutions examples Analyzer Cabinet s/houses Samples Systems Analyzer panels 16

Process Gas Chromatograph example 33 Process Gas Chromatograph (GC) Process GC Most versatile multi-component analyzer GC application engineer start with process datasheet GC chemist develop separation concept followed by GC hardware configuration System Integration engineer Detail engineering how to handle the process stream to provide a representative sample. From process to analyzer 34 17

Engineering details Sample system & GC 35 Engineering result Sample Conditioning System Process Gas Chromatograph GC columns system Result: Chromatogram 36 18

Erik Visser Team Leader Sales & Marketing Process Control Instrumentation M: +31 (0)6 22973398 F: +31 (0)88 4641111 Email: erik.visser@nl.yokogawa.com Loek van Eijck Analyzer center Europe Yokogawa Europe Solutions B.V. Euroweg 2, 3825 HD Amersfoort P.O. Box 163, 3800 AD Amersfoort Questions? 19