Premium Laboratory Equipment. Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

Transcription

1 Premium Laboratory Equipment 2017 Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

2 [ Support made easy While you concentrate on research, we ll look after your support needs As we want you to have more time to concentrate thoroughly on your research, the whole Heidolph team enthusiastically provides you with extensive support and helps to reduce your workload. [ What s in it for me? Watch our corporate video and learn about all benefits and services of Heidolph and our partners! Seit der Firmengründung vor über 75 Jahren steht Heidolph Instruments für hochqualitative und zeitgemäße Laborgeräte Made in Germany. Unsere strikten Qualitätsgrundsätze und ein kundenorientierter Service haben unser Wachstum untermauert Available at and on our Youtube-Channel! und doch muss man zu jeder Zeit die Zeichen der selbigen erkennen. In unserer schnelllebigen Umwelt, in der neue Technologien einen verkürzten Lebenszyklus aufweisen und der rasante Fortschritt einen neuen Takt dirigiert, ist es wichtig, dass ein Unternehmen dynamisch und erfinderisch zu Werke geht und nichts als gegeben akzeptiert. Unser neues Logo steht sinnbildlich für ein neues Kapitel in unserer Firmengeschichte welches alte Stärken bewahren und neue mit sich bringen soll. Mit dem Engagement und der Kreativität unserer Mitarbeiter entwickeln wir Laborgeräte die neue Maßstäbe setzen werden und die dem tiefsten Wünschen der Anwender gerecht werden. Neue Technologien werden zudem ungeahnte Möglichkeiten aufzeigen, die das Forschen effektiver, einfacher und sicherer machen wird, damit Sie auch in Zukunft sorgenfrei Forschen können. Guaranteed response to any request within 24 hours Lead times below 2 weeks for standard equipment Free demo evaluation units for up to 14 days Research made easy Our Service Commitment: Repair turn-around time within 4 working days The most common spare parts are locally available Immediate after-sales service provided by more than 80 distributors worldwide Installation and training on site Application support by chemists Our Quality Commitment: Increased lifespan of 10 years on average Reduced maintenance and spare parts cost over the entire lifespan Long-lasting service life of all products due to corrosionresistant electronics and maintenance-free motors Low product failure rates 3-year warranty - without compromises 2 3

3 Heidolph North America Product Offering Evaporation About Heidolph North America Other Bio Tools Air Sterilizers Reactors Synthesis Mixing & Sensitive Stirring Heidolph North America, a subsidiary of Heidolph GmbH, originally founded as Heidolph Brinkmann LLC in 2008 is an organization focused on providing unparalleled sales and service support of high quality laboratory products to the U.S. scientific community. Heidolph North America sells, supports and services products such as Heidolph rotary evaporators, Heidolph Tuttnauer sterilizers, Heidolph Radleys synthesis tools, and Heidolph AirClean Systems ventilation solutions. Our corporate headquarters is based in the Chicago area providing dedicated customer service, shipping, logistics, technical support, and sales management to the US and Canadian laboratory equipment market. We believe in our Research made easy philosophy of prompt customer service of all Heidolph products and supported by our industry leading 3 year warranty. Heidolph Instruments GmbH, founded in 1938 as a manufacturer of precision drive motors and engineering, is a manufacturer of high quality laboratory equipment, specializing in rotary evaporation, shakers, overhead stirrers, peristaltic pumps, and magnetic hotplate Products Rotary Evaporators Magnetic Stirrers Overhead Stirrers Ultrasonic Baths Water Distillers Vacuum Pumps/Controllers Rotary Evaporator Enclosures Industrial Rotary Evaporators Shakers/Mixers/Vortexers Bench top, Vertical, Pre & Post Vacuum & Industrial Sterilizers Carousel Parallel Synthesis workstations Reactors Findenser Heat On blocks system Glovebox Systems Drying & Deoxygenating solvent EPA & OSHA compliance Solution Applications Evaporation Synthesis Sterilization Cell Culture Heating/Stirring SPE Purification Chemical Inhalation Safety Process Optimization Liquid Handling/Dosing Mixing/Dispersing Solids stirrers. From Life Science to Rocket Science, our products and expertise help support the top scientific minds in North America Jim Dawson President 4 Our Chicago area office provides National Customer Service, Product Repair, Technical Support, Warehousing and Field Sales Management. 5

4 Summary Hei-VAP Rotary Evaporators Intelligent Evaporation 10 Hei-VAP Industrial Large-Scale Rotary Evaporators Industrial Evaporation 36 Hei-VOLUME Automatic Modules Automated 24/7 Evaporation 50 Hei-PLATE Magnetic Stirrers Safe Heating and Mixing 60 Hei-TORQUE Overhead Stirrers Powerful Stirring 80 Made in Germany Made in Germany is an internationally recognized quality seal for reliability, long performance life and low failure rates. In an era of accelerated economic globalization this is becoming an important competitive factor. Heidolph Instruments is committed to designing and manufacturing premium high-quality products exclusively in Germany. Hei-MIX Shakers and Mixers Temperature-Controlled Shaking 98 Hei-FLOW Peristaltic Pumps Precise Dosing and Dispensing 120 Hei-Lab App - Technical Service 142 Sterilizers/Autoclaves (Tuttnauer) 144 Ductless Enclosures 160 Synthesis Workstations and Reactors (Radleys) 166 For all components, Heidolph has defined the highest quality standards: Maintenance-free motors Made in Germany eliminate down times, frequent warranty periods and costly repairs it s for these reasons that we stand behind our products designed to provide you years of continuous operation. Our This accounts for product adjustments and for production volume equally. A high level of innovation in combination with short lead times make your Heidolph purchase a truly worthwhile investment, considering the average operational lifespan of 10 years! North Rhine- Westphalia Bremen Schleswig- Holstein Lower Saxony Hamburg Saxony-Anhalt Thuringia Mecklenburg- West Pomeranai Berlin Saxony ISO Certificate 190 Contacts at Heidolph 191 Imprint 193 Germany-based R&D and production facilities allow for responding to customer Rhineland- Palatinate Hesse requests quickly. Saarland Schwabach Baden- Württemberg Bavaria 6 7

5 Improve your evaporation process 8 9

6 Intelligent Evaporation Hei-VAP Rotary Evaporators Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

7 Leading Safety Standards Two independent safety circuits avoid an overheat situation of your heating bath: If bath temperature overshoots by 5 C and if your water bath runs dry, heating will be switched off automatically To avoid an overtemperature situation and potential thermal damage to your sample, you can individually pre-program a maximum temperature on the Hei-VAP Precision, at which the bath powers off In case of a power cut, all motor lift models will remove the flask from the heating bath preventing safety hazards and potential thermal damage to your sample To protect you from splashes and scalding, the Hei-VAP heating bath features an integrated pour spout to remove bath fluid safely Heating bath is constructed with a double wall for your protection against burns and scalding The guard hood covers the bath even if the heating bath is adjusted horizontally to its most extreme limit A metal support between the heating bath and the base unit prevents bath instability To protect your heating bath against short-circuits and systematic corrosion, the cable coupling complies with the protection class IP 67 For your protection, the operating panel is located near the base so as to keep your hands out of the dangerous zone of rotating flasks, steam and splashing bath fluids All heating baths feature non-slip handles with safety grip to protect you from scalding bath liquids and allow for easy installation/removal of the bath A separate on/off switch for heating prevents unintentional heat-up. The button is illuminated for visual control In case of an overshoot of any parameter setting, all models will show a warning on the operating panel Glassware assemblies are optionally available with transparent plastic safety coating ensuring ultimate protection while allowing visual control at all times IQ-OQ documentation is available for Hei-VAP models on request Do you demand the highest safety standards, perfectly engineered ease of use and reduced cost of ownership? Hei-VAP heating bath Intelligent Evaporation stands for an overheat protection design that prevents water baths running dry, provides a detachable panel for superior ease of use from outside closed fume hoods and offers a proven vacuum seal and vapor tube system guaranteed for years of operation! YOUR ADVANTAGES The Hei-VAP heating bath reaches a temperature of 210 C The universal heating bath can even accommodate 5-liter flasks The heating bath can be adjusted horizontally up to 200 mm To prevent short circuits and corrosion, the cable coupling complies with the protection class IP 67 Non-slip handles for safe transportation eliminate the risk of scalding An integrated pour spout to remove bath fluid safely Patented 210 C Detachable panel clamping sleeve IP 67 Easy-Clip XL condenser 12 13

8 Superior Ease of Use The detachable operating panel enables convenient handling from outside closed fume hoods The patented evaporating flask clamp Easy-Clip cannot be lost due to a connection to the vapor tube coupling ring The integrated screwed ring allows you to remove sticking evaporating flasks from the vapor tube just in seconds in a safe manner The universal heating bath can be adjusted horizontally up to 200 mm and offers efficient space to accommodate even 5-liter flasks The innovative ventilation and replenishment valves no longer have ground joints, which enables maximum tightness, grease-free operation and prevents glass breakage For your convenience, the height of 160 mm and the angle of the evaporating flask can be adjusted easily from 20 to 80 The optional automatic module Distimatic Bench-top allows for continuous and unattended automatic operations All components in direct or indirect contact with the medium are equipped with FDA-compliant materials for an extended application range Reduced Cost of Ownership Achieve up to 40 % higher evaporation rates due to unique tightness and industry-leading condensing surface with the XL condenser The high resistant and durable PTFE vacuum seal with FKM O-ring achieves maximum tightness and reduces spare part budgets The patented clamping sleeve ensures a long life performance of the vapor tube Increase your range of applications by using 5-liter flasks in the universal bath at no additional cost Maintenance-free and non-sparking motors reduce repairs and down times significantly to ensure years of continuous operation The flange on the condenser side of the drive is made of PPS (Polyphenylene sulfide), a robust industrial-designed resin with superior chemical resistance which provides more chemical resistance than stainless steel or welded aluminum. This reduces corrosion to a minimum which results in additional savings on maintenance and replacement components Spend your working hours more effectively on other challenges which require your attention and evaporate large quantities continuously with the automatic module Distimatic Bench-top Maximize your initial investment significantly: the automatic module Distimatic Bench-top is an affordable and more flexible alternative to large-scale rotary evaporators Reduce your maintenance costs. The sealed housing protects your rotary evaporator from aggressive fumes, liquids and vapors to prevent internal corrosion. This results in an increased lifespan of 10 years on average at a reduced maintenance and repair cost 14 15

9 Vapor tube with patented clamping sleeve Intelligent Evaporation YOUR ADVANTAGES The patented clamping sleeve system allows easy removal of the vapor tube from the drive Years of performance life reduce your spare parts budget up to 75 % The Hei-VAP vapor tube does not get stuck in the drive, thus eliminating the risk of broken glass Immediate removal of the vapor tube from the drive facilitates your work Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. New, FDA-compliant, transparent and uv-resistant tubing, with higher chemical resistance Achieve up to 40 % higher evaporation rates due to tightness and industry-leading 2,200 cm² condensing surface with the XL condenser The new highly resistant vacuum seals allow for long lasting constant application and reduce spare parts budgets. Also available as FFKM version for application with extremely aggressive solutions Patented flask clamp Easy-Clip YOUR ADVANTAGES Easy-Clip can t get lost due to a direct connection to the drive Superior ease of use due to the patented Easy-Clip, which provides an easy removal of sticking flasks and non-sticking vapor tube with patented clamping sleeve that eliminates broken glass and reduces spare parts cost significantly The integrated screw thread allows an easy removal of sticking flasks The Easy-Clip is made of highly resistant synthetic material which ensures a long life performance The innovative ventilation and replenishment valves no longer have ground joints, which enables maximum tightness, grease-free operation and prevents glass breakage 210 C Safety heating bath with handles and pour spout will power off if temperature overshoots by 5 C or runs dry Operating panel YOUR ADVANTAGES Changing all parameters from outside closed fume hoods guarantees the highest safety level The detachable operating panel enables safe and convenience handling from outside closed fume hoods Bath power cable coupling complies with protection class IP 67 to prevent corrosion and short circuits Standard for all models is a panel with 1 m cable connection. Thus data security is guaranteed at any time Immediate access to the panel ensures ultimate control of the process while increasing your ease of use A separate on/off switch for heating prevents unintentional heat-up the button is illuminated for visual control For unlimited evaporation: In conjunction with the automatic module Distimatic Bench-top allows you unlimited and automated distilling in 24/7 operation. An affordable alternative to large-scale rotary evaporators A separate on/off switch for heating prevents unintentional heat-up the button is illuminated for visual control A metal support between the heating bath and the base unit prevents bath instability 16 17

10 Hei-VAP Value / Hei-VAP Value Digital Hei-VAP Advantage Superior ease of use due to direct control The Hei-VAP devices with hand lift are optimally suited for all standard applications. Controlling parameters is done so with the simple turn of a knob Wide range of possibilities for reproducible results With the Hei-VAP Advantage you have a direct view on all parameter settings and are able to expand your application range The convenience of large dial controls for adjustment of rotation speed and bath temperature Hei-VAP Value Digital models come with a digital display for set and actual heating bath temperature Adjust the required angle of the evaporating flask individually according to your needs Available in hand lift or motor lift configurations Experience the advantages of our large digital 3.5 LCD display which indicates rotation speed, heating bath and vapor temperature Experience the advantages of the automatic process timer which turns off your evaporator at a preprogrammed time and removes evaporating flasks from bath on motor lift models Upgrade your Hei-VAP Advantage to a Hei-VAP Precision: Limit the height of your evaporating flask in just seconds The patented flask clamp Easy-Clip allows a simple and safe removing of the evaporating flask due to the force of unscrewing the Easy-Clip Upgrade-KIT Advantage Precision-HL P/N Upgrade-KIT Advantage Precision-ML P/N For your protection, the detachable operating panel is located below the bath and outside the danger zone. To conveniently run your unit from outside a fume hood, detach your panel and place it in your preferred location Large digital LCD display which allows you to monitor all parameters even from a distance Convenient motor lift adjusts height by the press of a button Hei-VAP Value Digital HL/G5B P/N Hei-VAP Advantage ML/G3B P/N Model Hei-VAP Value hand lift (HL) Hei-VAP Value Digital hand lift (HL) Glassware standard coated standard coated G1 Diagonal G3 Vertical G3 XL Vertical G5 Dry Ice Condenser G6 Vertical for Reflux Model Hei-VAP Advantage hand lift (HL) Hei-VAP Advantage motor lift (ML) Glassware standard coated standard coated G1 Diagonal G3 Vertical G3 XL Vertical G5 Dry Ice Condenser G6 Vertical for Reflux

11 Hei-VAP Precision Maximum capabilities due to integrated vacuum control The Hei-VAP Precision provides you with the maximum range of parameters, including but not limited to, reproducible applications and fully automated processes. Even solutions with different boiling points can be identified and distilled»» Reduce your process times significantly via automated distillation programs For automated distillation choose between these three programm opportunities: SET pressure Available in hand lift or motor lift configurations Experience the advantages of our large 4.3 color graphic display which features all parameters, integrated vacuum controller and includes programs for automated distillations Make your life easier by utilizing the integrated software support which leads you through the capabilities of the evaporator For data management Hei-VAP Precision models feature a USB interface Save time by configuring the unit - all connected devices will be recognized by the evaporator, which eliminates the need to configure the unit manually Now you can manage even the most demanding applications easily and prevent foaming, excessive bubbling or bumping Save time with your individualized pre-programmed parameter settings for your 30 most common applications used on a daily basis by saving them in a Favorites section Each ramp offers 20 separate steps for demanding applications Apply an individual name to those ramps to avoid a mix-up Experience the advantages of the automatic process timer which turns off your evaporator at a pre-programmed time by raising the flask on motor lift models and releasing vacuum Control your process individually by preprogramming vacuum gradients Hei-VAP Precision models feature a built-in vacuum controller as a standard 1000 mbar 1000 mbar Program: SETpressure Control parameter: manually set pressure Manually set vacuum Program: AUTOeasy Control parameter: pressure Program for solvent separations This program holds a pre-set vacuum constant. During the evacuation you have the full flexibility to choose another level of vacuum by the press of a button. Optionally, the process can be predefined via programmable ramps AUTO easy Supports the automatic pressure control for solvent separations The pressure level for the first boiling point is found automatically. This program can be used with all Heidolph glassware assemblies and does not require any accessories Finds boiling point automatically and holds vacuum constant AUTO accurate For increased safety all bath temperature adjustments can be limited Even from a distance you will be able to monitor the numbers on the display easily Hei-VAP Precision ML/G5B P/N mbar Program: AUTOaccurate Control parameter: vapor temperature Final vacuum individually adjustable Finds multiple boiling points automatically Stop Supports very precise automatic pressure control for solvent separations This program works similar to AUTO easy but in addition is able to identify multiple boiling points automatically by reducing vacuum accordingly. Also the AUTO accurate program delivers the finest and most precise vacuum control. To take advantage of this program, the optional AUTO accurate -sensor is required. This program cannot be used on Heidolph G1 and G5 glassware assemblies. Leading parameter of this program is the vapor temperature Large color graphic display for all parameters and automated programs Model Hei-VAP Precision hand lift (HL) Hei-VAP Precision motor lift (ML) Glassware standard coated standard coated G1 Diagonal G3 Vertical G3 XL Vertical G5 Dry Ice Condenser G6 Vertical for Reflux

12 Glassware Accessories Glassware set includes one 1,000-ml evaporating flask and one 1,000-ml receiving flask All glassware sets are also available with transparent plastic halar coating for G5B and abcite coating for G1B/ G3B/ G6B Evaporating flasks and vapor tube come standard with 24/40 joint size and also available with 29/32 ground joints Also available upon request: glassware sets for Soxhlet extraction and descending condenser system All glassware sets feature GL 10 thread; the inlet tube can be connected with a threaded fitting Glassware sets G3 and G6 allow for the automated distillation program AUTO accurate on Hei-VAP Precision models Evaporating flasks NS 29/32 NS 24/40 Evaporating flask* 50 ml Evaporating flask 100 ml Evaporating flask 250 ml Evaporating flask 500 ml Evaporating flask 1,000 ml Evaporating flask 2,000 ml Evaporating flask 3,000 ml Evaporating flask 5,000 ml XL Condenser For maximum evaporation performance The new XL condenser with industry-leading condensing surface of 2,200 cm 2 achieve up to 40 % higher evaporation rates. Available in G3 XL and G9* XL versions P/N coated * Evaporating flask NS 14.5 incl. adaptor (NS 29 or NS 24) Receiving flasks standard coated Receiving flask - NS 35/ ml Receiving flask - NS 35/ ml Receiving flask - NS 35/ ml Receiving flask - NS 35/20 1,000 ml Receiving flask - NS 35/20 2,000 ml Receiving flask - NS 35/20 3,000 ml Glassware set G1 Diagonal condenser for all standard distillations; the option with the most affordable price Glassware set G3 Vertical condenser for all standard destillations; the option with the smallest space requirements, also available as XL version Powder flasks NS 29/32 NS 24/40 Powder flask 500 ml Powder flask 1,000 ml Powder flask 2,000 ml P/N coated P/N coated Spider NS 29/32 NS 24/40 Spider with 6 distillation sleeves NS 14,5 20 ml Spider with 12 distillation sleeves NS 14,5 20 ml Spider with 20 distillation sleeves NS 14,5 20 ml Glassware set G5 Dry Ice condenser for low-boiling solvents Glassware set G6 Vertical condenser; centerpiece with valve for reflux distillation Spider NS 29/32 NS 24/40 Spider with 5 flasks NS ml Spider with 5 flasks NS ml Evaporating cylinder NS 29/32 NS 24/40 Evaporating cylinder 500 ml Evaporating cylinder 1,500 ml P/N coated P/N coated Foam brake NS 29/32 NS 24/40 Foam brake with flask clamp * For use with distimatic bench-top 22 23

13 Accessories Vacuum Pumps Advantages of all chemical-resistant diaphragm vacuum pumps Guard hood P/N Strong and transparent guard hood to protect you from implosions Provides easy and immediate access to flask and bath Guard shield P/N Strong and transparent guard shield for your protection while changing flasks Attached at the edge of the bath Vapor temperature sensor P/N For Hei-VAP Advantage and Hei-VAP Precision All components which come in contact with media are built from chemically resistant fluoropolymer The durable PTFE design guarantees an superior diaphragm lifespan The head cover and clamping disc have a stable core made of metal which offers unsurpassed long-term performance of your operational parameters The direct pump drive (without belt) is exceptionally quiet, creates a very low vibrational environment and reduces the need of wear and tear parts to a minimum The gas ballast valve has been optimized to prevent media condensing in the pump RPM-Regulated Vacuum Pumps AUTO accurate -sensor P/N For Hei-VAP Precision Only in combination with glassware set G3 and G6 Tubing P/N (package 12 m) P/N (by meter) Tubing for vacuum and water connection. Available as package (12 meter piece incl. hose clamps) or in individual length (by meter) y-connector P/N Vacuum seal P/N (PTFE / FKM) P/N (PTFE / FFKM) Standard PTFE / FKM spare seal Ultra resistant PTFE / FFKM seal for applications with highly abrasive solutions Pressure»» Highest distillation rates possible and reducing process time by 30 %»» Stable distillation conditions account for solvent recovery up to 99 % Fully automatic control with speed adjustment recovery rate YOUR ADVANTAGES Speed adjustment stops completely if vacuum is reached and runs intermittently at very low speed to hold vacuum constant Increased diaphragm performance life due to periods of nonoperation Aqua-Stop P/N The integrated valve closes automatically by turning off the evaporator. The system saves money by reducing your consumption of cooling tap water. Moreover the safety mechanism avoids flouding in your laboratory. (Only for Hei- VAP Advantage and Hei-VAP Precision) Spare Part Set: Hei-VAP Coupling NS24 P/N Includes: 1x Coupling T68x3, 1x Tension Spring, 1x Clamping Sleeve, 1x Swing Clamp NS24 Spare vapor tube NS 24/40 P/N Heating bath liquid P/N Heating bath liquid up to 220 C (5 L) = continuous evaporation RPM regulated pumps adjust their speed individually when the required vacuum level is reached Time Low energy consumption due to intermittent operation Significant noise and vibration reduction due to periods of nonoperation Operates without vacuum valve Most precise vacuum level at all times 24 25

14 Valve-Regulated Vacuum Pumps RPM-Regulated Vacuum Pumps Standard vacuum pumps can be controlled manually or via valve operated vacuum controllers Rotavac Rotavac Hei-VAC Valve Tec Valve Control Pump Standard vacuum pumps can be controlled manually or via valve operated vacuum controllers Rotavac Rotavac Rotavac Vario Pumping Unit Vario Tec Vario Control Recommended for solvents with low or medium boiling points Suction capacity for up to 3 rotary evaporators at the same time Part Number Condenser Part Number n/a Two-stage diaphragm pump Optional Package choices Valve-Tec w/ Manual Vacuum Controller P/N Can be combined with a condenser Yes Yes No Vacuum Control Manual Vacuum Controller Manual Vacuum Controller Manual Vacuum Controller Maximum Pumping Speed (m 3 /h) Three-stage diaphragm pump Precise vacuum control avoids bumping and eliminates foaming for your evaporation solution Due to automatic vacuum supply to the process parameter you have more time for important laboratory activities Two-stage diaphragm pump Recommended for solvents with low or medium boiling points Three-stage diaphragm pump Even if the gas ballast valve is open an excellent ultimate vacuum is reached when working with easily condensable vapors. This makes distilling high boiling point solvents such as DMF or DMSO possible at low bath temperatures Ultimate Vacuum (mbar) Power input (W) Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 145 x 315 x x 245 x x 143 x 175 Manual/Digital Manual Manual Manual Recommended with Rotary Evaporator Model Hei-VAP Value and Hei-VAP Advantage Hei-VAP Precision Hei-VAP Precision Part Number Condenser Part Number PC510 NT PC3001 Vario Pro Chemical-resistant Yes Yes Yes Can be combined with a condenser Yes Yes Yes Maximum Pumping Speed (m3/h) Ultimate Vacuum (mbar) Power input (W) Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 263 x 193 x 156 x x 236 x x 236x 196 Recommended for medium-sized vacuum applications involving common solvents Optimizes vacuum conditions automatically by precisely and continuously adjusting the diaphragm pump s motor speed ME1 Diaphragm Pump ME1 Diaphragm Pump Part Number Part Number Condenser Part Number n/a n/a Can be combined with a condenser No No Vacuum Control CVC 3000 CVC 3000 Maximum Pumping 2 2 Speed (m 3 /h) Ultimate Vacuum (mbar) 7 2 Condenser Part Number Suction Capacity (m 3 /h) 85 Ultimate Vacuum (mbar) 100 Power input (W) 40 Weight (lb) 11 Dimensions (mm) 247 x 121 x 145 Power input (W) Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 419 x 243 x x 306 x 400 Manual/Digital Digital Digital 26 27

15 Vacuum Accessories Chillers Switchbox Manual vacuum controller Vacuum valve Hei-Therm Connect up to three rotary evaporators to one vacuum pump For Hei-VAP Value and Hei-VAP Advantage Required to control vacuum for Hei-VAP Precision models with valve-regulated pumps RL-720M Rotachill F250 Rotachill Duo F1000 Switchbox P/N Connect up to to three rotary evaporators to one pump and control vacuum individually Pump switches off automatically at required vacuum Reduces energy consumption of pump Increases performance life of the pump due to a complete switch-off if vacuum is reached Vacuum valve and non-return valve are required for every evaporator if you work with different pressures at the same time Delivery includes three non-return valves Designed for Hei-VAP Precision Manual vacuum controller P/N Control your house vacuum or any other vacuum source Pressure range from 0 to 1,020 mbar Scaling on display in steps of 50 mbar Connection for tubes with 8 mm inner diameter Support rod included A vacuum valve is not required Dimensions: L80 / W80 / H150 mm Vacuum valve P/N External attachment design for easy cleaning Can be combined with the Woulff Bottle to one unit Not required if you utilize a Manual vacuum controller Woulff bottle P/N Additional recovery of solvent to protect vacuum valve and vacuum pump Compatible with all Hei-VAP configurations 1800 Viewing radius swiveling monitor enables screen view from any angle Several temp and interface options Intuitive large digital display Quick cool down times and small coolant volumes Small footprint to reduce lab space Temp/cooling capacity for any size evaporator Environmentallyfriendly operation with low energy consumption Compact design Splash-proof membrane keypad w/led temp display Quick cool down times and small coolant volumes Small foot print to reduce lab space Temp/Cooling capacity for any size evaporator Compact design Splash-proof membrane keypad w/led Temp display Straight forward filling and draining Filling level indicator Part Number Recommended for 2 Evaporators No No No Yes Yes Working Temperature (C) -20 to to to to 40 0 to 40 Max Pressure Flow Rate (l/ min) Max Pressure (psi) Cooling +200C (W) Reservior Capacity (L) Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 541 x 221 x x 244 x x 400 x x 244 x x 490 x 640 Weight: 0.6 kg Dimensions: L80 / W160 / H45 mm Direct connection to the vacuum valve is possible Features connection to vacuum controller Volume of 250 ml 28 29

16 Equipment Combinations Overview of Hei-VAP units With the Hei-VAP series you can easily assemble your individual laboratory equipment - exactly to your requirements. Rotary Evaporator Vacuum source Accessories Please refer to the overview by Hei-VAP units for the possible configurations or contact us - we are happy to be at your service and will advise you in detail. Rotavac Vario Pumping Unit included not required Vacuum controller Vacuum valve»» Example configuration Rotavac Valve Control Rotary Evaporator Rotavac Valve Tec optional Manual vacuum controller House vacuum Hei-VAP Value / Hei-VAP Value Digital Vacuum source Rotavac Vario Pumping Unit included optional not required Vacuum controller Vapor temperature sensor (all glassware sets) Vacuum valve Rotavac Valve Control Rotavac Valve Tec optional Manual vacuum controller + Hei-VAP Advantage House vacuum Vapor temperature sensor (all glassware sets) Accessories Hei-VAP Advantage Rotavac Vario Pumping Unit Rotavac Valve Control Rotavac Valve Tec House vacuum included required optional Vacuum controller Vacuum valve Auto accurate-sensor (glassware G3/G6 only) Vapor temperature sensor (all glassware sets) included Vacuum controller Rotavac Vario Control not required Vacuum valve Rotavac Vario Tec optional Auto accurate-sensor (glassware G3/G6 only) Vacuum controller Vapor temperature sensor (all glassware sets) Vacuum valve included optional not required included in pumping unit, no further configuration required optional available as accessory not required due to rpm regulation Hei-VAP Precision Vapor temperature sensor (all glassware sets) As an aid to decision-making we have created different packages for you, from basic equipment up to automatic destillation with RPM-regulated vacuum pumps - for details see the following pages. Rotavac Valve Control with condenser Rotavac Valve Tec with condenser Rotavac Vario Control with condenser Rotavac Vario Tec with condenser Rotavac Vario Pumping Unit with condenser Manual vacuum controller Vacuum valve with Woulff bottle AUTO accurate - sensor Vapor temperature sensor 30 31

17 Hei-Therm Circulator Baths Heated Circulators The Heidolph Hei-Therm circulator baths are designed to help scientists with their rigorous temperature control requirements. Each unit is designed to give optimal control, reproducibility, and an intuitive operator interface. Pick from 3 different interface controllers depending on your applications and data control requirements. Open Bath Circulators Stainless steel or polycarbonate baths, sizes from 6 to 28 liters Large and Easy to Use Display Heat/Chemical Resistant Cover Plate Rotating Display for Ease of Use HL-7M circulator HL-15M circulator HL-7AD circulator HL-15AD circulator HL-28AD circulator HL-7AP circulator HL-15AP circulator HL-28AP ciruclator Part Number Working Temperature (C) +10 to to to to to to to to 200 Temp Stability (C) +/ / / / / / / / Pump Type Pressure Pressure Pressure/ Suction Pressure/ Suction Pressure/ Suction Pressure/ Suction Pressure/ Suction Pressure/ Suction Pump Speeds One One Variable Variable Variable Variable Variable Variable Reservior/Tank Material Stainless Steel Stainless Steel Stainless Steel Polycarbonate Stainless Steel Stainless Steel Stainless Steel Stainless Steel Included Software PolyTemp Viewer, USB driver PolyTemp Viewer, USB driver PolyTemp Viewer, USB driver PolyTemp Viewer, TDMS file viewer, USB driver, Excel Program Generator, PolyTemp Remote iphone application PolyTemp Viewer, TDMS file viewer, USB driver, Excel Program Generator, PolyTemp Remote iphone application Reservior Capacity (L) PolyTemp Viewer, TDMS file viewer, USB driver, Excel Program Generator, PolyTemp Remote iphone application Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 499 x 221 x x 368 x x 221 x x 368 x x 457 x x 221 x x 368 x x 457 x 422 M immersion circulator PC 8-M open bath circulator PC-14M open bath circulator PC-28M open bath circulator SS-6M open bath circulator SS-10M open SS-28M open bath circulator bath circulator Part Number Working Temperature (C) +10 to to to to to to to 135 Temp Stability (C) +/ / / / / / / Pump Type Pressure Pressure Pressure Pressure Pressure Pressure Pressure Refrigerated Circulators 180 Viewing Radius Swiveling monitor enables screen view from any angle Intuitive large digital display with programmable Time vs. Temperature ramps on AP models Heat/Chemical Resistant Top Plate DuraTop Energy Efficient WhisperCool technology reduces noise and energy consumption Several temperature and interface options Pump Speeds One One One One One One One Reservior/Tank Material Stainless Steel Polycarbonate Polycarbonate Polycarbonate Stainless Steel Stainless Steel Stainless Steel Reservior Capacity (L) Weight (kg) Dimensions (without condenser) (L x W x H) (mm) Heated Circulators 180 Viewing Radius Swiveling monitor enables screen view from any angle Compact design provides small footprint 109 x 97 x x 207 x x 208 x x 345 x x 206 x x 342 x x 342 x 457 Intuitive large digital display with programmable Time vs. Temperature ramps on AP models Heat/Chemical Resistant Top Plate DuraTop Immersion cooling coil cutouts on Top Plate RL-720M refrigerated circulator RL-720AD refirgerated circulator RL-1540AD refrigerated circulator RL-2830AD refrigerated circulator RL-720AP refirgerated circulator RL-1540AP refrigerated circulator RL-2830AP refrigerated circulator Part Number Working Temperature (C) -20 to to to to to to to 200 Nominal Cooling +20C (W) Temp Stability (C) +/ / / / / / / Pump Type Pressure Pressure Pressure/ Suction Pressure/ Suction Pressure/ Suction Pressure/ Suction Pressure/ Suction Pump Speeds One One Variable Variable Variable Variable Variable Reservior/Tank Material Stainless Steel Stainless Steel Stainless Steel Polycarbonate Stainless Steel Stainless Steel Stainless Steel Included Software PolyTemp Viewer, USB driver PolyTemp Viewer, USB driver PolyTemp Viewer, USB driver PolyTemp Viewer, TDMS file viewer, USB driver, Excel Program Generator, PolyTemp Remote iphone application Reservior Capacity (L) PolyTemp Viewer, TDMS file viewer, USB driver, Excel Program Generator, PolyTemp Remote iphone application 32 Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 541 x 221x x 221 x x 368 x x 457 x x 221 x x 368 x x 368 x

18 Technical Specifications - Rotary Evaporators Model Hei-VAP Value (HL) / Value Digital (HL) Hei-VAP Advantage (HL) Hei-VAP Advantage (ML) Hei-VAP Precision (HL) Hei-VAP Precision (ML) Hand / Motor lift hand lift hand lift motor lift hand lift motor lift Height adjustment speed manual manual 30 mm/s manual 30 mm/s Height adjustment (mm) Rotation speed (rpm) Rotation speed setting scale 3.5" LCD display 3.5" LCD display 4.3" LCD color graphic display 4.3" LCD color graphic display Drive brushless DC motor with electronic speed control Heating capacity (W) 1,300 1,300 1,300 1,300 1,300 Certificate Temp. range heating bath ( C) Temperature accuracy bath ( C) ±1 ±1 ±1 ±1 ±1 Overheat protection bath ( C) cut-off at 5 C over set temperature via separate Pt 1000 Bath temperature setting**** scale / digital 3.5" LCD display 3.5" LCD display 4.3" LCD color graphic display 4.3" LCD color graphic display Heating bath temperature control electronic / digital electronic / digital electronic / digital electronic / digital electronic / digital Secondary overtemp. cut-off ( C) Material heating bath stainless steel AISI 316L stainless steel AISI 316L stainless steel AISI 316L stainless steel AISI 316L stainless steel AISI 316L Diameter heating bath (mm) Volume heating bath (L) Display vapor temperature no yes yes yes yes required accessories vapor temperature sensor vapor temperature sensor vapor temperature sensor vapor temperature sensor To confirm the ability for continuous operation of the Hei-VAP series Rotary Evaporators Integrated vacuum controller no no no yes yes Timer no yes yes yes yes Vacuum program SET pressure ** no no no yes yes Vacuum program AUTO easy ** no no no yes yes Vacuum program AUTO accurate ** requires AUTO accurate -sensor Remote control function no no no yes yes - Lift no no yes no yes - Start rotation yes yes yes yes yes - Start vacuum no no no yes yes - Start heating bath yes yes yes yes yes Programmable ramps no no no yes yes Supply power (W) 1,400 1,400 1,400 1,400 1,400 Weight (w/o glassware assembly) (kg) Dimensions with glassware set G3 (mm) Width on extended heating bath (l x w x h) 477 x max. 739 x x max. 739 x x max. 739 x x max. 739 x x max. 739 x 808 Dimensions with glassware set G3 XL (mm) Width on extended heating bath (l x w x h) 477 x max. 739 x x max. 739 x x max. 739 x x max. 739 x x max. 739 x 888 Protection class*** (DIN EN 60529) IP 20 IP 20 IP 20 IP 20 IP 20 Hei-VAP series Rotary Evaporators feature overtemperature safety circuits according to DIN EN :2001 and DIN EN :2014 and therefore is designed for continuous operation. This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel. Condensing surface (cm 2 ) 1,400 1,400 1,400 1,400 1,400 Condensing surface XL Condenser (cm 2 ) 2,200 2,200 2,200 2,200 2,200 Schwabach, January 2017 Rate of evaporation* (L/h) Toluene Acetone Ethanol Isopropanol (IPA) Water G3 Vertical G3 XL Vertical Improvement with XL condenser (%) system limit reached with 1.4 L/h * With maximum condenser efficiency ** Only in combination with vacuum systems Standard supply voltage: 230 V - other voltages upon request, please specify for order *** IP 67 cable connection on heating bath **** Hei-VAP Value Digital: digital display Stefan Peters Research and Development Manager Marcell Sarré Quality Manager 34 35

19 Industrial Evaporation Hei-VAP Industrial Large-Scale Rotary Evaporators Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

20 Leading Safety Standards Newly designed EASY LOCK flask attachment allows for safe flask change An emergency off switch brings the entire unit to a complete stop To promote a safe use of the Hei-VAP Industrial evaporator the interface panel not only has all parameters for operation but also 5 key safety functions that require operator action prior to resuming process Features water level regulation system to prevent water spilling over bath and potentially flooding your lab Safety sensor stops rotation if bath guard hood is opened during operation thus providing user safety A temperature sensor powers off the bath in case of any uncontrolled heat-up To effectively prevent accidents while monitoring parameters the speed, bath temperature and vacuum setting must be confirmed on separate on/off buttons in order to start operation Automatic safety cut-off in an overpressure situation caused by glassware breakage or defective vacuum circuit Receiving cassette system protects glassware while providing superior flask support. Easy access to receiving cassettes via two latching high-impact transparent PMMA doors Ultimate safety is provided with the Hei-VAP Industrial model which comes standard with: a guard hood consisting of a metal frame and safety glass completely covering the bath. This prevents any operator contact with steam, splashing bath fluid and splinters of glass in case of implosion Excellent user safety is achieved by a transparent high impact PMMA door on a metal condenser housing covering the main glassware assembly Do you require safe and quick flask removal by one person with industry leading safety standards? Industrial Evaporation With the Hei-VAP Industrial series you are always on the safe side with the safety enclosure protecting you and your glassware! You can operate the Hei-VAP Industrial just by yourself, change flasks in seconds and operate the unit with ease. Touch-panel Self-filling water bath One-person flask changes EASY LOCK Visual control Transparent PMMA doors 38 39

21 Superior Ease of Use Intuitive touch screen control for easy operation Touch screen with glass surface for chemical resistance and easy cleaning EASY LOCK flask attachment for quick and easy flask changes Illuminated bath and evaporation flask allows for superior visual control Integrated heating coils guarantee the most convenient and fastest cleaning of the bath Receiver cassettes guard against glassware breakage while providing a self-standing flask support and quick removal of receiving vessels Save time with up to 250 pre-programmed steps of up to 999 process ramps Unique self-aligning flask support system allows for immediate one-person operation Reduce your process times by using the exclusive AUTO accurate program which automates your distillation using a vapor temperature system that takes the guesswork out of finding the correct vacuum setting every time No hassle and safety concern due to low fluid levels: self-filling water bath takes the worry out of running dry Receiving flasks feature reinforced bottom drain valves as standard and are protected by cassettes To prevent steam from building up within the guard hood, two strong blowers effectively ventilate the entire area to give you a clear view of the evaporating flask Now you can manage even the most demanding applications easily and eliminate foaming, excessive bubbling or bumping of solutions The automatic process timer turns off your evaporation at a pre-programmed time The optional automatic module Distimatic Industrial allows for continuous and unattended automatic operations Optional Base Cart provides you with a fully-maneuverable rotary evaporator while offering a storage space for vacuum pump, glassware, solvents or accessories Reduced Cost of Ownership Universal heating bath for water or other bath fluids allows for temperature settings up to 180 C Utilize the pre-heating option for your bath and start your application without any loss of time The water bath refill system allows you to step away from your evaporator at any moment and reduce your supervision responsibility to zero for baths that run dry or overheat No hidden cost: all components to control vacuum are included as a standard. This includes vacuum valve, vacuum controller, vacuum sensor and vapor temperature sensor AUTO accurate-evaporations drive your solution to a variable quantity or dryness, then shut off vacuum, heating bath and rotation, and ventilates the system to give you semi-automated capabilities at significant cost savings Spend your working hours more effectively on other challenges which require your attention and evaporate large quantities continuously with the automatic module Distimatic Industrial Maximize your initial investment significantly: the automatic module Distimatic Industrial is an affordable and more flexible alternative to common 50 or 100-liter evaporators Increased throughput at reduced energy consumption due to an industry leading leak-proof vacuum seal: final pressure below 1 mbar pressure increase below 1 mbar/h 41

22 Hei-VAP Industrial control panel Industrial Evaporation Menu Timer Vacuum (set & actual) Speed (set & actual) Bath temperature (set & actual) Vapor temperature Start/Stop all parameters Vacuum control mode Height adjustment of heating bath Separate on/off switches for all process parameters Indicating warm-up on/off switch Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. Illuminated bath and evaporation flask allows for superior visual control A guard hood consisting of a metal frame and safety glass covers the bath completely while providing clear visible monitoring Increased throughput at reduced energy consumption due to an industry leading vacuum leakproof USB interface The brand-new EASY LOCK flask attachment allows for single-user safe flask exchange Features level regulation system to prevent from spilling over and potential floods in lab Unique self-aligning flask support system allows for Two Programs for Process Control SET pressure AUTO accurate Excellent user safety: condenser and receiving flasks are protected by highimpact transparent PMMA doors immediate one-person operation Non-visible heating coils guarantee the most convenient and fastest cleaning of the bath Program for solvent separations This program holds a set vacuum constant and uses a hysteresis Optionally, the process can be predefined via programmable ramps Supports very precise automatic pressure control for solvent evaporation and separations This program identifies multiple boiling points automatically by reducing vacuum Intuitive touch screen control for ease of operation 1000 mbar Program: SETpressure Control parameter: manually set pressure 1000 mbar Program: AUTOaccurate Control parameter: vapor temperature Receiver cassettes guard against glassware breakage while providing a self-standing support Unit powers off all relevant functions in case of a bath overtemperature situation, overpressure and glassware breakage No hassle or safety concerns due to low bath fluid levels: the Manually set vacuum Final vacuum individually adjustable Finds multiple boiling points automatically stop self-filling water bath takes the worry out of running dry Automatic module Distimatic Industrial - For batch and continuous evaporation without limits - an affordable and more flexible alternative to common 50 or 100-liter evaporators Save time with up to 250 pre-programmed profiles of up to 999 process gradients 42 43

23 Hei-VAP Industrial Glassware Hei-VAP Industrial Highest safety and integrated vacuum control capabilities Includes leading safety standards and features for superior ease of use and reduced cost of ownership, plus: Excellent user safety with high-impact transparent PMMA door Glassware Shorty R Identical to glassware R, but features a condenser that is 320 mm shorter Distillation capacity remains the same. This assembly is ideal in laboratories for hood applications or where height is restricted Glassware R This glassware assembly includes one ascending condenser, one 20-l evaporating flask, one 10-l receiving flask and is recommended for all standard distillations Glassware Shorty RC Glassware RC Identical to glassware assembly Shorty R, but features two receiving flasks Identical to glassware assembly R, but features two receiving flasks Large touch screen control panel with illuminated displays for all process parameters, programmable ramps as described on page 42 Non-fogging safety glass and metal frame guard hood provides excellent user protection The evaporation flask is illuminated during operation for increased visibility Receiver cassettes and additional PMMA door housing protect against threat of glassware breakage Certification according to GMP available for this model: validation for installation (IQ) and operating qualification (OQ) Glassware A This glassware assembly includes one descending condenser, one expansion vessel, one 20-l evaporating flask, one 10-l receiving flask and is recommended for solvents that tend to splash and foam Glassware A2 This glassware assembly includes one ascending, one descending condenser and one expansion vessel, one 20-l evaporating flask, one 10-l receiving flask For low-boiling solvents and highest recovery rates Universal heating bath accommodates water or other bath fluids allowing for temperature settings up to 180 C Glassware AC Identical to glassware assembly A, but features two receiving flasks Glassware A2C Identical to glassware assembly A2, but features two receiving flasks Comes as standard with integrated refill water system, spillover prevention and a release valve at the bottom Optional Base Cart is fullymaneuverable with removable panels for storage of vacuum pump, glassware, solvents or accessories Glassware A1 This glassware assembly includes one ascending, one descending condenser, one 20-l evaporating flask, one 10-l receiving flask For low-boiling solvents and highest recovery rates Glassware K Condensate trap for low-boiling solvents; cooling by dry-ice Comes with one 20-l evaporating flask and one 10-l receiving flask Hei-VAP Industrial with glassware set RC (without Base Cart) P/N Glassware A1C Identical to glassware assembly A1, but features two receiving flasks Glassware KC Identical to glassware assembly K, but features two receiving flasks 44 45

24 Vacuum Pump Chillers Valve-regulated vacuum pump Rotavac 20 P/N Includes secondary condenser and air intake separation vessel Hei-VAP Industrial Rotachill FL4003 Hei-VAP Industrial Rotachill Eco FL2503 Part Number Working Temperature (C) 5 to to to to 40 Max Pressure Flow Rate (l/min) This vacuum system can be applied in many different fields in order to evacuate, evaporate and pump out gases and vapors. Thanks to the emission condenser it is possible to achieve a chemical recovery of almost 100% Excellent compatibility with chemicals and condensate Excellent ultimate vacuum of 2 mbar Very quiet and very low vibration Very high suction capacity of 3.0 m3 /h Weight: 19.9 kg Dimensions: W350 / D275 / H495 mm Max Pressure (psi) Cooling +20 C (W) Reservoir Capacity (l) Weight (kg) Dimensions (without condenser) (L x W x H) (mm) 775 x 483 x x 759 x x 368 x x 759 x 1151 Accessories - Hei-VAP Industrial Part Numbers Hei-VAP Industrial Hei-VAP Industrial Without Base Cart Evaporating flasks Evaporating flask 6 l P/N Evaporating flask 10 l P/N Evaporating flask 20 l (Included as a standard) P/N Powder flasks Powder flask 10 l P/N Powder flask 20 l P/N Receiving flask P/N With drain valves, 10 l (Included as a standard for all Hei-VAP Industrial models) Glassware R Shorty R RC Shorty RC A AC A A1C A A2C K Vacuum sensor P/N (Included as a standard for all Hei-VAP Industrial models) Vacuum valve P/N (Included as a standard for all Hei-VAP Industrial models) Tubing P/N (package 16 m) P/N (by meter) Tubing for vacuum and water connection. Available as package (16 meter piece incl. hose clamps) or in individual length (by meter) KC Limited budgets? Hei-VAP Industrial B Hei-VAP Industrial B Glassware R As shown above (Hei-VAP Industrial) - without: Shorty R Vapor temperature sensor P/N (Included as a standard for all Hei-VAP Industrial models) Base Cart P/N For all Hei-VAP Industrial models Heating bath liquid P/N Heating bath liquid up to 220 C (5 L) Metal frame and safety glass guard hood covering the bath High-impact PMMA door covering the glassware assembly High-impact PMMA latching door which cover the receiving flask cassettes Without Base Cart RC Shorty RC A AC A A1C A A2C K KC

25 Technical Specifications - Large-Scale Rotary Evaporators Model Hei-VAP Industrial Model Hei-VAP Industrial Rotation speed (rpm) Vacuum controller yes Rotation speed setting digital Heating bath lift motor lift Height adjustment speed (mm/s) 45 Height adjustment (mm) 180 Drive EC-motor Heating capacity (W) 4,000 Temperature range heating bath ( C) Temperature accuracy ( C) ±1 Overheat cut-off protection ( C) 110 (H 2 O) / 210 (oil) Bath temperature setting digital Automatic heating bath control micro processor Material heating bath V4A (1.4404) Diameter heating bath (mm) 400 Volume heating bath (l) 24 (H 2 O) / 22 (oil) Level regulation of water bath automatically due to level sensor and refill function Display vapor temperature (required accessories) Indicating range vapor temperature sensor ( C) digital temperature sensor (accuracy 0.1 C) Timer Vacuum control program SET pressure ** Vacuum control program AUTO accurate ** requires AUTO accurate -sensor Programmable ramps yes yes yes yes Supply power (W) 4,600 Weight (without glass assembly) (kg) approx. 120 Dimensions (l x w x h) (mm) 970 x 690 x 1,600 Protection class (DIN EN 60529) IP 20 Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel. Rate of evaporation (L/h) at 40 C * temperature difference - Toluene - Acetone - Ethanol - Water Maximum condensing surface (m 2 ) 1.2 Certificate To confirm the ability for continuous operation of the Hei-VAP Industrial series Large-Scale Rotary Evaporators * T = difference between heating bath temperature and boiling temperature ** Only in combination with vacuum systems Standard supply voltage: 230 V - other voltages upon request, please specify for order The Hei-VAP Industrial series Large-Scale Rotary Evaporators feature overtemperature safety circuits according to DIN EN :2001 and DIN EN :2014 and therefore is designed for continuous operation. This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Schwabach, January 2017 Stefan Peters Research and Development Manager Marcell Sarré Quality Manager 48 49

26 Automatic 24/7 Evaporation Hei-VOLUME Automatic Modules Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

27 General Automatic refill of the evaporation flask with the solvent mixture according to your settings. Continuous automatic discharge of condensate The worldwide unique automatic residue drainage offers unattended distillation for days The automatic module is compatible with all bench-top and large-scale evaporators from Heidolph The storage and the collecting tank can be replaced during the process Leading Safety Standards The complete system is sensorcontrolled and turns off the automatic module as well as all connected equipment completely in case of an emergency The system can be placed under a fume hood which ensures the highest safety level for the operator An easily accessible emergencybutton allows you to stop the process immediately by the operator Superior Ease of Use Do you require a system to evaporate unlimited volumes in a continuous and unattended process 24 hours a day/7 days a week? Take advantage of the wide range of possibilities to adjust the settings according to your individual needs The worldwide unique automatic residue drainage offers a wide range of new possibilities for automatic, continuous and unattended distillation The process can be terminated automatically after evaporation is completed or manually at any time by the operator Integrated plug connectors enable you to connect and to control also peripheral equipment from a central point Automatic 24/7 Evaporation Save time by using the automatic module Distimatic and distill large volumes in a continuous and unattended manner overnight and during the weekend! 24/7 Automatic discharge of condensate Automatic drainage of residue Automatic refill No bumping Reduced Cost of Ownership Affordable alternative to common 50 or 100 liter evaporators Reduce your investments by using your existing equipment - the automatic module is compatible to all rotary evaporators from Heidolph Increase your efficiency - the fully automatic process avoids the need of visual control and gives you time to focus on other tasks The unattended and continuous reconditioning of solvent avoids any bottlenecks of availability of solvents and reduce your investments in this way 52 53

28 The smart way to process large quantities automatically Automated 24/7 Evaporation The automatic module Distimatic is available for Hei-VAP rotary evaporators (Distimatic Bench-top) and Hei-VAP Industrial large-scale rotary evaporators (Distimatic Industrial) For distillation select between these two modes: Sensor-Mode: Refill and drainage are automatically sensor-controlled Time-Mode: All parameters controlled by individually pre-programmed automatic time intervals Process rates with bench-top evaporators for the most common solvents are: Water: 1.4 l/h Acetone: 6.0 l/h Toluene: 6.5 l/h Ethanol: 2.5 l/h Increased process rates with Hei-VAP Industrial large-scale evaporators, for example: Water: 4.5 l/h Acetone: 25.0 l/h Both modes are completed in an automated and unattended process of solvent separations of nearly 100 % Degree of concentration for final product can be determined to rule out dehydration, cristallisation and formation of powder Bumping is eliminated by continuously feeding small volumes Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. Automated in unattended distillation in two different modes Automatic refill of the evaporation flask and continuous automatic discharge of condensate For distillation select between these two modes: Automatic drainage of residue: residue in the evaporation flask will be drained off Compatible with all Hei-VAP rotary evaporators (Distimatic Bench-top) and Hei-VAP Industrial large-scale rotary evaporators (Distimatic Industrial) Applications are completed in an automated and unattended process of solvent seperations of nearly 100 % The automatic module Distimatic Bench-top can be used in common fume hoods due to the space saving design Sensor-Mode: Time-Mode: Refill and drainage are automatically sensor-controlled All parameters controlled by individually pre-programmed automatic time intervals Distimatic A sensor detects the fill-level inside the evaporation flask The desired/requested fill-level can be set individually Flask refill is achieved via valve control and under system pressure A sensor monitors the quantity of the solvent mixture and powers off the unit once it is completely processed The desired/requested fill-level can be set individually Flask refill is achieved via valve control and under system pressure according to pre-programmed cycles The process is powered off once the pre-programmed number of cycles have expired Wide range of possibilities to adjust settings according to your individual needs In case of an emergency the complete system will power off entirely Bumping is eliminated by continuously feeding small volumes 54 55

29 Functional Principle Functional Principle For unattended and continuous use including automatic drainage of residue Save time by distilling large volumes in a continuous and unattended manner overnight and during the weekend Automatic solvent supply of the evaporating flask Refilling with the Sensor-Mode runs automatically and is based on the desired level in the evaporation flask Refilling with the Time-Mode is done according to individual time parameters Automatic discharge of condensate A valve matrix controls the continuous discharge of the condensate from the system into a temporary storage flask. Afterwards the collected condensate will be discharged into the collecting tank by a diaphragm pump End of distillation process The process can be terminated automatically after evaporation is completed or manually at any time by the operator Distimatic Bench-top including automatic drainage of residue Vacuum valve Collector valve Ventilation valve Condensate pump 5 Residue pump Automatic drainage of residue Emergency sensor The residue in the evaporating flask will be drained into a collecting tank. Afterwards the process starts again automatically by refilling the evaporating flask Distimatic Bench-top / Distimatic Industrial The automatic module Hei-VAP Distimatic is compatible with all bench-top and large-scale evaporators from Heidolph Collector Level sensor 5 Refill valve 4 Refill sensor Overflow sensor Overflow sensor Distimatic Bench-top including automatic drainage of residue P/N (G9B) P/N (G9B XL) Distimatic Bench-top without automatic drainage of residue P/N (G9B) P/N (G9B XL) Distimatic Industrial including automatic drainage of residue and adaptor piece for glassware set A / A2 P/N Distimatic Industrial including automatic drainage of residue and adaptor piece for glassware set R P/N Distimatic Industrial without automatic drainage of residue P/N Residue Solvent Condensate Rate of evaporation at continuous operation Reach outstanding evaporation rates of up to 6.5 l/h with the Distimatic Bench-top and up to 25.0 l/h with the Distimatic Industrial 56 57

30 Technical Specifications - Automatic Module Distimatic Model Distimatic Bench-top without drainage of residue Distimatic Bench-top including drainage of residue P/N (115 V) Compatibility (Rotary Evaporators) Hei-VAP and Laborota 4000 series * Hei-VAP and Laborota 4000 series Separate control panel yes yes Display digital digital Automatic refill of sample yes yes Automatic discharge of condensate yes yes Automatic drainage of residue no yes Certificate Power input control box (VA) Noise level (db(a)) < 80 < 80 Total power multiple switched socket (W) 3,500 3,500 Weight (kg) 5 5 Measurements without mounted components (W x D x H) Permissible ambient conditions (mm) 300 x 200 x x 200 x C at 80 % rel C decreasing linearly up to max. 50 % rel m a.s.l., Contamination level 2 Overvoltage category II Protection class (DIN EN 60529) IP 54 IP C at 80 % rel C decreasing linearly up to max. 50 % rel m a.s.l., Contamination level 2 Overvoltage category II To confirm the ability for continuous operation of the Automatic Module Distimatic Model Distimatic Industrial without drainage of residue Distimatic Industrial including drainage of residue P/N (115 V) Glassware A Glassware R Compatibility (Rotary Evaporators) Hei-VAP Industrial and Laborota 20 series Hei-VAP Industrial and Laborota 20 series Separate control panel yes yes Display digital digital Automatic refill of sample yes yes Automatic discharge of condensate yes yes Automatic drainage of residue no yes Power input control box (VA) Noise level (db(a)) < 80 < 80 Total power multiple socket (W) 3,500 3,500 Weight (kg) 5 5 The Automatic Module Distimatic features overtemperature safety circuits according to DIN EN :2001 and DIN EN :2014 and therefore is designed for continuous operation. This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Measurements without mounted components (W x D x H) (mm) 300 x 200 x x 200 x 120 Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel m a.s.l., Contamination level 2 Overvoltage category II 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel m a.s.l., Contamination level 2 Overvoltage category II Protection class (DIN EN 60529) IP 54 IP 54 Schwabach, January 2017 All shown values relate on Automatic Module Disitmatic without any external accesory parts * Also compatible to some models of other manufacturers. To check the compatibility please contact your dedicated Heidolph contact person 58 Stefan Peters Research and Development Manager Marcell Sarré Quality Manager 59

31 Safe Heating and Mixing Hei-PLATE Magnetic Stirrers Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

32 Leading Safety Standards To prevent accidents or laboratory fires, all magnetic stirrers feature two independent safety circuits which switch off heating in case of any overtemperature situation In combination with Heat-On attachments you can convert your lab into a safety zone A residual heat indicator for all models prevents you from potential burning hazards For your safety, the unit will power off in case of a short-circuit, a damage to the temperature sensor, a motor failure or other incidences during operation To protect you from splashes and scalding from bath media, rotation speed ramps up slowly until unit has reached the pre-programmed speed A separate on/off switch for heating prevents unintentional heat-up. If heating is switched on, the on/off button is illuminated for visual control Even if the stirrer is exposed to the highest temperatures, damage is categorically ruled out all models come with a fire-resistant aluminum die-cast housing Have you ever heard of hotplates with fast heat-up times and chemical resistance? Safe Heating and Mixing The unique Kera-Disk heating plate of aluminum provides fast heating times, and the wafer-thin ceramic coating makes the heating plate both chemically and scratch resistant! 35 % faster heat-up times Highly resistant hot plate Separate button for heating Prevents unintentional heat-up Sealed housing 62 63

33 Reduced Cost of Ownership The hermetically-sealed housing protects all mechanical and electronic components from aggressive environments The maintenance-free non-sparking motors reduce down times The design and features give an increased lifespan of 10 years along with significantly reduced maintenance and repair costs Superior Ease of Use All units with digital display allow for easy setting and monitoring values on the illuminated readout You can even work with dry ice a robust thermal insulation prevents corrosion inside the housing by preventing condensate from collecting and dripping on any electronic components A free software program is available for the MR Hei-Connect and MR Hei-End which supports you to automate and to safe your process parameters The strong magnetic field allows for easy stirring of even higher viscosity media The unique Kera-Disk coating is extremely chemical-resistant and scratch-proof, and therefore the plate can be cleaned easily from solvents, oil or other contaminations The chemically resistant Kera-Disk hot plate allows for immediate heat transfer resulting in quick heat-up times In case the heating function fails, stirring will not be discontinued to avoid thermal damage to your sample 64 65

34 Kera-Disk top plate With Kera-Disk material coating, fast heat-up times and chemical resistance! YOUR ADVANTAGES Glass ceramic top plates offer the benefits of chemical and scratch resistance but produce longer heat-up times Aluminum top plates allow for immediate heat transfer but are not chemical-resistant or scratch-proof Safe Heating and Mixing Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. Kera-Disk top plates take the best of two worlds: The aluminum top plate allows for immediate heat transfer for quick heat-up times and a thin layer of ceramic coating makes the top plate chemical-resistant and scratch-proof The standard RS 232 interface of the MR Hei-Connect and MR Hei-End enables the documentation and controlling via PC. A free software is available on our website The chemically resistant Kera-Disk hot plate allows for immediate heat transfer resulting in quick heat-up times Hermetically-sealed housing protects all mechanical and electronic components from aggressive Performance and Accuracy Take advantage of a built-in PID controller that ensures fastest heat-up times while preventing an overtemperature situation of your sample temperature 800 W 600 W environments In case the heating function fails, stirring will not be discontinued to prevent bumping time Sealed housing The sealed housing of the MR series guarantees extended performance life and reduced maintenance! liquid YOUR ADVANTAGES Protection against aggressive fumes, liquids and vapors which prevents internal corrosion. This results in an increased lifespan of 10 years on average at reduced maintenance and repair cost The temperature sensor consists of two independent safety circuits which switches off heating in case of any overtemperature situation PC board motor gas Protection of all mechanical and electronic components against aggressive environmental conditions In case of a short-circuit, a damage or removal of the temperature sensor from the media, the unit powers off completely Damage to the stirrer is categorically ruled out even if exposed to highest temperatures all models come with a fire-resistant aluminum die-cast housing A separate on/off button for heating prevents unintentional heat-up the button is illuminated for visual control. In addition, the residual heat indicator prevents from potential burning hazards The hermetically-sealed housing that protects the PC board and the motor is marked in black. The way a liquid would take flowing down from the hotplate is marked in orange. As one can see, even if the liquid reaches the heat shields, it cannot ingress to the PC board and the motor but is drained off. The other line marked in orange shows that gas can neither ingress to the PC board nor to the motor. The apparent gap is due to temperature insulation. Because of that gap the temperature inside the magnetic stirrer stays substantially lower, which significantly increases the durability of the magnetic stirrer. For protection against liquid and gas, the heating elements are completely embedded in ceramic

35 Magnetic Stirring Hotplates Preferred use of the MR Series magnetic stirrers includes smooth to intense mixing and heating of low-viscosity fluids. Your first choice for decomposing organic and inorganic substances MR Hei-Tec Model for higher requirements with temperature sensor A digital display enables full process monitoring and precise setting of all parameters With a heating power of 800 W the hotplate reaches a maximum temperature of 300 C in a significantly reduced time period Safety circuits avoid an overheat situation of your hotplate: if the temperature overshoots the heating will be powered off immediately For standard applications without temperature sensor For higher requirements The strong magnetic field allows for stirring even higher viscosity media or volumes of 20 liters of water with ease Speed is adjustable from 30 respectively 100 to 1,400 rpm at an accuracy of up to ± 1 % for gentle mixing For comprehensive process documentation For highest safety This unit features a digital display and allows for easy setting and monitoring of values in the illuminated readout For your protection an independent safety circuit will switch off heating if hotplate temperature exceeds 25 C over set temperature Digital speed setting from 100 to 1,400 rpm at an accuracy of ± 2 % and temperature setting up to 300 C A separate on/off switch for heating prevents an unintentional heat-up. If heating is switched on the on/off button is illuminated for visual control. In addition, a residual heat indicator prevents from burning hazards when heat function is switched off An illuminated button indicates clearly if the stirring mode is activated Upgrade this magnetic stirrer with the optional Pt 1000 temperature sensor for precise temperature control, overshoot protection and reproducible results To protect your sample from overheating a safety circuit switches off heating if the temperature sensor is not immersed in your media vessel MR Hei-Tec P/N MR Hei-Tec with Pt 1000 P/N MR Hei-Standard MR Hei-Tec MR Hei-End MR Hei-Connect MR Hei-Standard Model for standard applications without temperature sensor Easy handling and direct access to all parameters due to two separate knobs For your protection an independent safety circuit will switch off heating if hotplate temperature exceeds 25 C over set temperature A separate on/off switch for heating prevents an unintentional heat-up. If heating is switched on the on/off button is illuminated for visual control. In addition, a residual heat indicator prevents from burning hazards when heat function is switched off Analog knobs allow for convenient speed setting from 100 to 1,400 rpm at an accuracy of ± 2 % and temperature setting up to 300 C MR Hei-Connect Model for comprehensive process documentation and reproducible results The MR Hei-Connect includes all features of the MR Hei-Tec unit but comes with an additional RS 232 interface Monitor and control your process with the Hei-Control software or your own program Benefit from reproducible results and the option to program ramps and interval processes MR Hei-Connect P/N MR Hei-Connect with Pt 1000 P/N Hei-Control software included in the scope of delivery MR Hei-Standard P/N

36 MR Hei-End Accessories Model for highest safety Exact settings and individual definition of safety parameters for highly sensitive media An independent safety circuit switches off heating at an operator-programmed temperature value above your set temperature An additional operational safety step is required to change parameters which prevents unwanted changes to the actual setting A separate on/off switch for heating prevents an unintentional heat-up. If heating is switched on the on/off button is illuminated for visual control Upgrade this magnetic stirrer with the optional Pt 1000 temperature sensor for precise temperature control, overshoot protection and reproducible results 1-l Heating bath PTFE-coated P/N l Heating bath PTFE-coated P/N l Heating bath PTFE-coated P/N Concave block adaptor For 1-l round-bottom flasks P/N The digital display allows for easy setting and monitoring of values on the illuminated readout. Speed setting from 30 to 1,400 rpm at an accuracy of ± 1 % and temperature setting up to 300 C Hotplate residual heat indicator in the digital display illuminates when unit is turned off and hotplate temperature is above 50 C to prevent accidental operator injury 1-l Heating bath for oil Max. temperature 250 C P/N l Heating bath for oil Max. temperature 250 C P/N l Heating bath for oil Max. temperature 250 C P/N Holding device MR For safe fixation on lab frames to gain extra lab space. Comes with clamp as standard P/N To protect your sample from overheating a safety circuit switches off heating if the temperature sensor is not immersed in your media vessel MR Hei-End P/N MR Hei-End with Pt 1000 P/N Software Hei-Control Utilize the optional software to control and document the entire process MR Hei-End and MR Hei-Connect featuring a digital RS 232 interface for connecting the optional software easily Pt 1000 clamping system (includes support rod and attachment with cable inlet) P/N Pt 1000 clamping system for bath attachments from 3 to 5 liter (includes support rod and attachment with cable inlet) P/N Pt 1000 temperature sensor stainless steel For MR Hei-Tec, MR Hei-Connect and MR Hei-End P/N Pt 1000 temperature sensor glass-coated For MR Hei-Tec, MR Hei-Connect and MR Hei-End P/N RS 232 cable (9-pole) For MR Hei-Connect P/N Stirring bars Stirring bars - cylindrical shape (25, 40, 50 mm each) Stirring bars - cross shape (16.5 mm) pack of 20 pcs. for 25-ml to 50-ml flasks RS 232 cable (15-pole) For MR Hei-End P/N P/N Connect up to four units at the same time Included in scope of delivery with MR Hei-Connect Compatible with MR Hei-End and Hei-TORQUE devices Free download of Hei-Control Software for MR Hei-Connect and MR Hei-End at Silicone protective cover Replaceable cover against splashes and dripping water For MR Hei-Tec, MR Hei-Connect and MR Hei-End P/N For MR Hei-Standard P/N Stirring bars Evaluation Kit pack of 10 pcs. Stirring bars - oval shape (15x6 mm) pack of 3 pcs. for 10-ml flasks Stirring bars - oval shape (25x10 mm) pack of 3 pcs. for 25-ml to 50-ml flasks Stirring bars - oval shape (30x10 mm) pack of 3 pcs. for 100-ml to 250-ml flasks

37 Heat-On Attachments Heat-On Attachments The Heat-On attachments are suitable to replace oil baths and heating mantles in your lab and reduce the risk of fire hazards. Moreover the attachments minimize the messy oil clearups that result from changing oil or removing flasks from an oil bath! Our attachments are by far the safest, fastest and most efficient method for heating and mixing solutions in round-bottom flasks from 10 ml to 5 liter Heat-On fits precisely to every flask, thus ensuring maximum surface contact and fast heat transfer. Eliminates the mess from cleaning flasks after removal from an oil bath or hazardous spills when an oil bath slips off a stirring plate. As a result, oil as a heat transfer media is made redundant and your lab is a safer place with the Heat-On block system Heat-On blocks Each Heat-On block is a stand-alone product that can be placed directly onto the stirring hotplate Heat-On 100-ml block with flask sidearm cutouts Heat-On 250-ml block Heat-On 250-ml block with flask sidearm cutouts Heat-On 500-ml block Heat-On 1-l block Heat-On 2-l block Heat-On 3-l block Heat-On 4-l block Heat-On 5-l block Heat-On accessories Support rod for bath attachments from 3 to 5 liter Retort clamp Boss head Flask Stand & Clamp Kit (including Support rod for bath attachments from 3 to 5 liter, Retort clamp, Boss head) Flask volume Volume of water Hotplate temperature Time to reach boiling 10 ml 6 ml 300 C 6.8 min 25 ml 15 ml 300 C 8.0 min 50 ml 30 ml 300 C 8.5 min 100 ml 60 ml 300 C 8.8 min 150 ml 100 ml 300 C 10.0 min Heat-On 250-ml block with flask sidearm cutouts Heat-On 2-l block 250 ml 150 ml 300 C 10.8 min 500 ml 300 ml 300 C 16.4 min Heat-On Multi-Well packages 1,000 ml 600 ml 300 C 21.1 min 2,000 ml 1,200 ml 300 C 35.1 min 3,000 ml 1,800 ml 300 C 47.3 min Package Heat-On Multi-Well Basic Including 1x Multi-Well holder and 3 inserts for 25-ml, 50-ml and 100-ml flasks Leading Safety Standards Superior Ease of Use 4,000 ml 2,400 ml 300 C 51.0 min 5,000 ml 3,000 ml 300 C 75.5 min Reduced Cost of Ownership Package Heat-On Multi-Well Including 1x Multi-Well holder and 6 inserts, 2 each for 25-ml, 50-ml and 100-ml flasks Heat-On 10-ml insert Heat-On 50-ml insert Prevents accidents, fires and contamination by completely banning all oil baths from your laboratory This unique design prevents glass breakage and protects you from spilled chemicals or solvents The high temperature range provides unlimited safety for applications up to 260 C A unique PTFE-coating on the aluminum Heat-On body allows for superior chemical resistance and many years of service life Precise temperature control inside the vessel or on the heating block with a thermocouple port that provides actual block temperature back to your MR series hotplate Increase your daily work throughput significantly and reduce your overall process times by quick changing of Heat-On blocks Save energy costs 1,000 ml of water heats up 66 % faster than conventional oil baths 150 ml of water boils in less than 11 minutes Multi-Well holder and inserts This unique Multi-Well holder is designed to hold either one or two inserts for flasks*. The inserts are available for 10-ml, 25-ml, 50-ml, 100-ml and 150-ml flasks. Flask inserts also feature cut-away sides for use with two or three-neck flasks and accept the optional safety lifting handles * Only accepts one 150-ml insert Insert for Multi-Well holder Heat-On 10-ml insert Heat-On 25-ml insert Heat-On 50-ml insert Heat-On 100-ml insert Heat-On 150-ml insert Heat-On Multi-Well holder P/N Heat-On safety lifting handles P/N

38 StarFish Workstations Have you always been looking for a system to perform numerous reactions on a small footprint to significantly reduce space and process times? With our attachments you can turn your magnetic stirrer into an efficiency-increasing reaction station for up to 45 samples simultaneously! Upgrade your magnetic stirrer to a product with multiple capabilities From simple heating and mixing tasks to chemical reactions under inert gas, concentrations or extractions - everyhing is possible No special glassware purchase required - use your own glassware and cherry-pick the appropriate attachments for your applications StarFish workstations are ideal for soxhlet applications PolyBlocks PolyBlocks are smaller segments (5 per StarFish) which can be mixed to accommodate any combination of vessels; allowing the use of different vessel types and sizes at the same time PolyBlock for 1 x 250-ml flask PolyBlock for 3 x 25-mm tubes PolyBlock for 3 x 24-mm tubes PolyBlock for 9 x 16-mm tubes PolyBlock for 9 x 12-mm tubes PolyBlock for 3 x 28-mm vials PolyBlock for 3 x 21-mm vials PolyBlock for 7 x 17-mm vials PolyBlock for 9 x 15-mm vials PolyBlock for 9 x 12-mm vials Base plate Base plate with optional handles fits securely onto the top plate maintaining good thermal contact with the heated surface Universal 5-way clamps The StarFish clamp allows you to hold glassware of virtually any size and comes with a choice of Silicone rubber or Velcro support straps StarFish base plate (145 mm) P/N StarFish base plate handles (pair) P/N way clamp (Velcro) P/N way clamp (Silicone strap and handle) P/N Each clamp features 5 telescopic arms which can be extended and locked in place to suit your needs. Using different straps on separate clamps allows you to grip the flask neck with the Silicone rubber strap for lifting, whilst the condenser above slides through the Velcro strap MonoBlocks MonoBlocks are single blocks with multiple wells all of the same size and are ideal for experiments using the same vessel MonoBlock for 5 x 250-ml flasks Inserts for MonoBlock 5 x 250 ml Water-Distribution Manifold Allows coolant from a single source to be evenly distributed to up to five condensers and then recombines the flow to one outlet pipe Two manifolds are used in each set-up, one to distribute water to the condenser and one to collect coolant for recirculation or to drain. Connectors feature leak-proof shut-off valves Water Manifold With connector P/N Numerous combinations Cherry-pick from different PolyBlock options in different sizes or one MonoBlock system for identical roundbottom flasks or vials. In addition, you can choose from a large selection of inserts ranging from 5 ml to 150 ml 150-ml Flask insert ml Flask insert ml Flask insert ml Flask insert ml Flask insert ml Flask insert MonoBlock for 16 x 25-mm tubes MonoBlock for 16 x 24-mm tubes MonoBlock for 40 x 16-mm tubes MonoBlock for 40 x 12-mm tubes MonoBlock for 16 x 28-mm vials MonoBlock for 20 x 21-mm vials MonoBlock for 40 x 17-mm vials MonoBlock for 40 x 15-mm vials MonoBlock for 40 x 12-mm vials Gas/Vacuum Manifold With connector P/N Gas/Vacuum-Distribution Manifold Allows gas or vacuum from a single source to be evenly distributed to up to five positions or vessels (does not control or regulate gas/vacuum flow). Connectors feature leak-proof shut-off valves Replacement Self Adhesive Velcro Pads, 200 mm (pack of 10) Replacement Velcro Loop Strips, 200 mm (pack of 5) Replacement Silicone Straps, 200 mm (pack of 5) mm Support rod mm Support split rod

39 Magnetic Stirrer without Heating Magnetic Stirrer Packages For gentle stirring in biology and microbiology applications Hei-Mix S Stir quickly and efficiently with an extended speed range up to 2,200 rpm Space-saving unit for efficiently mixing sample sizes up to 5 liter. Small footprint of L 140 / W 126 / H 80 mm only and the top plate comes with a diameter of 104 mm Ideal for titrations due to whitecolored top plate Long-lasting polyamide housing and PVDF top plate material MR Silver 1 Package MR Gold 1 Package MR Platinum Package P/N P/N P/N MR Hei-Mix S P/N This package includes: Magnetic Stirrer MR Hei-Tec Temperature sensor Pt 1000 (AISI 316Ti) Pt 1000 clamping system (includes support rod and attachment with cable inlet) MR Silver 2 Package P/N This package includes: Magnetic Stirrer MR Hei-Connect Temperature sensor Pt 1000 (AISI 316Ti) Pt 1000 clamping system (includes support rod and attachment with cable inlet) Interface cable RS 232 This package includes: Magnetic Stirrer MR Hei-Tec Temperature sensor Pt 1000 (AISI 316Ti) Pt 1000 clamping system (includes support rod and attachment with cable inlet) Heat-On Multi-Well system including Multi-Well holder and the following inserts: 2 x 25 ml, 2 x 50 ml, 2 x 100 ml MR Gold 2 Package P/N This package includes: Magnetic Stirrer MR Hei-Standard Heat-On Multi-Well system including Multi-Well holder and the following inserts: 2 x 25 ml, 2 x 50 ml, 2 x 100 ml This package includes: Magnetic Stirrer MR Hei-End Temperature sensor Pt 1000 (AISI 316Ti) Base plate MonoBlock for 5 x 250-ml flasks 2 x 100-ml flask insert 2 x 50-ml flask insert 1 x 25-ml flask insert 5-way clamp (velcro strap) 5-way clamp (silicone strap & handle) 2 x Water Manifold 1 x Gas/Vacuum Manifold 650-mm split rod 76 77

40 Technical Specifications - Magnetic Stirrers Model MR Hei-Mix S MR Hei-Standard MR Hei-Tec MR Hei-Connect MR Hei-End P/N (115 V) Speed range (rpm) 0-2, , , , ,400 Speed accuracy (%) ±5 ±2 ±2 ±2 ±1 Drive Shaded pole motor EC-motor EC-motor EC-motor EC-motor Operating mode continuous continuous continuous continuous continuous Display digital digital digital Certificate Analog/digital interface yes (digital) yes Heating power (W) 600 * 600 * 600 * 600 * Hotplate temperature ( C) Medium temperature, max. ( C) Accuracy temperature setting ( C) ±5 ±1 ±1 ±1 External temperature sensor Pt 1000 Pt 1000 Pt 1000 Pt 1000 Temperature accuracy with external temperature sensor ( C) ±1 ±1 ±1 ±0.2 Sensor breakage protection with Pt 1000 with Pt 1000 with Pt 1000 with Pt 1000 Temperature control Micro controller Micro controller Micro controller Micro controller Temperature accuracy hotplate ( C) ±5 ±5 ±5 ±5 Residual heat indicator yes yes yes yes To confirm the ability for continuous operation of the MR series Magnetic Stirrers with hotplate Safety circuit hotplate ( C) 25 C over hotplate temperature 25 C over hotplate temperature 25 C over hotplate temperature C over nominal temperature Stirring capacity, max. (H2O) (l) Load, max. (kg) Power consumption (W) Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel. Plate diameter (mm) ø 104 ø 145 ø 145 ø 145 ø 145 Plate material PVDF Kera-Disk (Silumin with ceramic coating) Kera-Disk (Silumin with ceramic coating) Kera-Disk (Silumin with ceramic coating) Weight (kg) C at 80 % rel C decreasing linearly up to max. 50 % rel. Kera-Disk (Silumin with ceramic coating) Dimensions (l x w x h) (mm) 140 x 126 x x 277 x x 277 x x 277 x x 277 x 94 The MR series Magnetic Stirrers with hotplate feature overtemperature safety circuits according to DIN EN :2001 and DIN EN :2014 and therefore is designed for continuous operation. This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Protection class (DIN EN 60529) IP 21 IP 32 IP 32 IP 32 IP 32 * 800 W for 230 V-units Standard supply voltage: 115 V - other voltages upon request, please specify for order Schwabach, January 2017 Stefan Peters Research and Development Manager Marcell Sarré Quality Manager 78 79

41 Powerful Stirring Hei-TORQUE Overhead Stirrers Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

42 Leading Safety Standards The electronic stirrers feature a smooth start operation which prevents spills and splashing media. The speed ramps up slowly until your set rpm has been reached An optional shaft guard prevents accidents Non-sparking motors for additional safety Important for continuous operation: the motor will be switched off if a high thermal load situation occurs to increase safety in your lab and to prevent accidents Safe start and stop of operation via slide touch panel to avoid accidental start-up To protect your stirrer against corrosion and short-circuits, all models comply with the protection class IP 54 Looking for an all-purpose stirrer with smart technology and highest performance to reduce your workload? Powerful Stirring The powerful Hei-TORQUE stirrers accomplish the most demanding tasks while providing the highest safety in combination with a unique user interface Glass panel Slide to Low noise start/stop below 50 db IP

43 Superior Ease of Use Quick and easy set-up in your lab due to a space-saving design RS 232 or USB interface to save all process data in a digital file Free software for all Hei-TORQUE Precision models aids you in automating your process and saves all data in electronic files Newest motor generation for maximum power at minimum noise level below 50 db All stirrers maintain exact speed under changing loads A through-shaft design allows for adjusting the impeller position to make height adjustments more convenient for you Reduce your work time and achieve excellent mixing results in challenging high-viscosity media A single grip allows you to re-adjust the height of your stirrer on the optional telescopic stand The outstanding product design with intuitive touch-panel made of glass has been honored with the prestigious if DESIGN AWARD in 2016 Reduced Cost of Ownership Reduce your maintenance costs: the sealed housing protects your stirrer from aggressive fumes, liquids and vapors to prevent internal corrosion. This results in an increased lifespan of 10 years on average while reducing maintenance and repair cost The high torque level accounts for better mixing results in less time to reduce your process time and working hours significantly Maintenance-free motors reduce repairs and down times significantly to ensure years of continuous operation The unique impeller technology for demanding applications that mixes gels and other similar media in shorter times which reduces process cost and working hours The sealed panel made of glass and the magnetic Smart-Knob further increase the tightness of the entire housing Free software for all Hei-TORQUE Precision models avoids the need for additional investments 84 85

44 Powerful stirring Powerful Stirring Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership YOUR ADVANTAGES An overtemperature sensor preventively shuts off the unit in dangerous heat-up situations particularly valuable for you in case of unattended continuous operation The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. All units are designed for continuous 24-hour operation including challenging high viscosity applications in polymer research The durable design of the Hei-TORQUE series promotes longevity in an aggressive environment: The sealed housing protects against corrosion, ensures years of maintenance-free operation and complies with the high protection class IP 54 Newest motor generation for maximum power at minimum noise level - below 50 db An overtemperature sensor prevents heat-up situations particularly valuable in unattended continuous operation The intuitive touch-panel made of glass for easy operation The sealed panel made of glass and the magnetic Smart-Knob further increase the tightness of the entire Impellers YOUR ADVANTAGES Stirrer guides for applications under vacuum or pressure, flex couplings and flex shafts increase your available options Sealed housing, which complies with the high protection class IP 54, guarantees longevity and maintenance-free 24-hour operation in an aggressive environment housing Safe start and stop of operation via slide touch panel to avoid unintended stirring Through thick and thin: large selection of impellers for every flow and viscosity Choose from high-quality stainless steel, plastics or PTFE-coated impellers we have the right one for your specific needs Reduce your process times by utilizing unique technology which creates turbulent flows and a new dynamic motion that stirs gels with ease Free software for all Hei-TORQUE Precision models to automate and to save all process parameters Reduce process times by utilizing unique VISCO JET impellers for mixing gels and other challenging media with ease 86 87

45 Hei-TORQUE Value Hei-TORQUE Precision These stirrers are ideal for standard stirring tasks. They are designed to mix and disperse media that require non-reproducible results in high-viscosity applications These stirrers are ideal for demanding tasks which have to be reproducible and documentable. The huge number of additional features and operation modes allows for a perfect adjustment to your individual application Indication of torque tendencies to monitor viscosity changes Digital 2.4 display for ease of operation Accurate torque indication shows any viscosity changes Constant speed even under changing loads Constant speed even under changing loads Digital 3.2 display for ease of operation: Allows for pre-programmed profiles Saves these profiles in memory Interval operation Watch rpm and torque graph life Timer / Countdown / Real time settings Safe start and stop of operation via slide touch panel to avoid unintended stirring Newest motor generation provides maximum power at minimum noise level Newest motor generation for maximum power at minimum noise level Safe start and stop of operation via slide touch panel to avoid unintended stirring Including free software to automate and to save all process parameters RS 232 or USB interface to save all process data in a digital file Hei-TORQUE Value 400 P/N Hei-TORQUE Precision 400 P/N

46 Overview Range of Performance The differentiation between performance and features enables you to easily configure the right stirrer for your specific application 100 Ncm Performance graph of: Hei-TORQUE Value 100 Hei-TORQUE Precision 100 Torque (Ncm) Drehzahl (U/min) Hei-TORQUE Value 200 Ncm Performance graph of: Hei-TORQUE Value 200 Hei-TORQUE Precision 200 Torque (Ncm) Drehzahl (U/min) Hei-TORQUE Precision 400 Ncm Performance graph of: Hei-TORQUE Value 400 Hei-TORQUE Precision 400 A two-gear stage design enables different torque ranges for flexible applications with high and low viscous media Torque (Ncm) I II Speed (rpm) Noise Level Newest motor generation and the complete removal of ventilation slots significantly increase the life-span and ensure stable stirring at clearly reduced noise compared to conventional overhead stirrers 100 Ncm 200 Ncm 400 Ncm Hei-TORQUE stirrers below 50 db High-end models Hei-TORQUE Precision 100 P/N (USB) P/N (RS 232) Hei-TORQUE Precision 200 P/N (USB) P/N (RS 232) Hei-TORQUE Precision 400 P/N (USB) P/N (RS 232) Basic models Hei-TORQUE Value 100 P/N Hei-TORQUE Value 200 P/N Hei-TORQUE Value 400 P/N Other brands above 60 db 90 91

47 Impellers Selection parameters Precise working with an overhead stirrer depends on the right choice of the stirrer tool. When choosing a stirrer tool you have to consider its different characteristics and their effects. For example, the flow which the tool causes in the medium, the tool s adequate field of application depending on the speed range, and the execution of the tool according to the viscosity it is destined for Application examples: Gassing of liquids < 500 mpa s: Radial Flow Impeller Homogenizing and suspending in liquids < 500 mpa s: Propeller-Type or Blade Impeller Medium with a viscosity > 500 mpa s: Anchor-Type Impeller, Blade Impeller BR 13, VISCO JET Stirring of gel: VISCO JET Please ensure that for radial flow, blade, half-moon and VISCO JET impellers the beaker size and position of your impeller complies with the shown guideline to achieve superior mixing results Operational guidelines Position of the stirring tool In center Distance to the bottom (h 3 /d ): Diameter vessel (h 1 /d 1 )=1 VISCO JET diameter ratio (d 2 /d 1 ): Circumferential speed 3-15 m/sec: Radial Flow Impeller 2-5 m/sec: VISCO JET, Blade and Anchor-Type Impeller d 2 d 1 h 3 h 1 min Propeller-Type Impeller These impellers are recommended for applications which require average or high speed For mixing tasks with medium or high viscosity Type Excellent mixing properties for homogenization and suspensions These models create an axial flow Prop. dia. [mm] Material Length [mm] Shaft dia. [mm] Max. rpm PR 39 Pitched-Blade Impeller 75 PTFE PR 30 Pitched-Blade Impeller 58 PR 31 Ringed Propeller PR 32 Ringed Propeller PR 33 Ringed Propeller stainless steel AISI 316Ti stainless steel AISI 316Ti P/N , ,000 2, Blade and Half-Moon Impeller These impellers are recommended for applications which require average speed For mixing tasks with little or average viscosity Models BR 12, BR 14 and HR 18 come with collapsible blade for narrow neck vessels Radial-Flow Impeller These impellers are recommended for applications which require average speed For mixing tasks with little or average viscosity up to < 500 mpa s Ideal for gassing of liquids These impellers create a radial flow Type Blade size [mm] Material Length [mm] Shaft dia. [mm] Max. rpm P/N Type Ø Turbine size [mm] Material Length [mm] Shaft dia. [mm] Max. rpm P/N BR 10 Cross-Blade Impeller 50 x 12 stainless steel AISI 316Ti , TR 20 Radial-Flow Impeller TR 21 Radial-Flow Impeller stainless steel AISI 316Ti stainless steel AISI 316Ti , , BR 11 Straight-Blade Impeller 50 x 12 stainless steel AISI 316Ti , BR 12 Pivoting-Blade Impeller 60 x 15 stainless steel AISI 316Ti , Anchor-Type Impeller BR 13 Square-Blade Impeller 70 x 70 stainless steel AISI 316Ti These impellers are recommended for applications which require a low speed For mixing tasks with medium or high viscosity BR 14 Collapsible-Blade Impeller 90 x 10 stainless steel AISI 316Ti Type Blade size [mm] Material Length [mm] Shaft dia. [mm] Max. rpm P/N HR 18 Half-Moon Impeller 65 x 18 x 3 PTFE AR 19 Anchor-Type Impeller 60 x 40 x 5 PTFE

48 VISCO JET Impellers Accessories The all-rounder for thick and thin Reduce your process times significantly while performing the best mixing results ever One system for literally all mixing tasks for low to high-viscosity media The turbulent flow which is created by a special cone principle even at low speeds is unique to the VISCO JET Even with high-viscosity media and gels which naturally do not mix when common impellers are used you will observe an immediate flow through the entire beaker This technology allows for de-gassing of gels while preventing air intake and foaming Universal stand S2 P/N Stand tube Ø: 25 mm Length: 700 mm Weight: 5.8 kg Stand S2 XXL P/N Stand tube Ø: 25 mm Length: 1,000 mm Weight: 6.0 kg Telescope stand P/N Stand tube Ø: 32 mm Adjustable length: 725-1,025 mm Weight: 7.7 kg Clamp P/N For stand S2, S2 XXL and telescope stand Ø mm Type Ø [mm] Material Length [mm] Shaft dia. [mm] Speed range [rpm] For vessel dia. [mm] P/N VISCO JET - 60* 60 stainless steel AISI 316Ti VISCO JET - 80* 80 stainless steel AISI 316Ti VISCO JET - 80* 80 impeller: plastic (POM) hub: brass shaft: polyamide-coated VISCO JET - 120* 120 stainless steel AISI 316Ti VISCO JET - 120* 120 impeller: plastic (POM) hub: brass shaft: polyamide-coated VISCO JET CRACK - 80* 80 stainless steel AISI 316Ti VISCO JET CRACK - 120* 120 stainless steel AISI 316Ti * A shaft is included as a standard Flex-coupling P/N Includes clamping stud for stirrer shaft Accepts Ø 10 mm shafts T-Handle P/N Flexible shaft P/N Comes with chuck Stirrer guide (NS 24/29 PTFE) P/N Stirrer guide (NS 29/32 PTFE) P/N PTFE with adjustable seal Accepts Ø 8 mm shafts Shaft guard P/N Material: PMMA Incl. adapter set Adjusts between 187 mm and 312 mm Shaft guard adapter set P/N VISCO JET - CRACK mm stainless steel VISCO JET - 60 mm stainless steel Application examples The only impeller world wide capable of completely mixing larger quantities of high-viscosity liquids and gels Fields of use: Beverage production, dairy products, food, sugar & candy production, chemistry/petro chemistry, ceramics, water treatment, cosmetics, colorant/paint production and paper manufacture, etc. RZR 1 For simple mixing tasks For media up to 40,000 mpa s and volumes up to 20 liters The RZR 1 is suitable for torque up to 100 Ncm at a power of 18 W For attaching an existing shaft guard to a Hei-TORQUE stirrer VISCO JET - 80 mm plastic (POM) Principle of functionality The VISCO JET Mixing System from VISCO JET Rührsysteme GmbH is the result of the so-called cone principle. Slim design fits nicely into your research environment A manual scale for speed adjustments from 35-2,200 rpm VISCO JET mm stainless steel Turbulent flows are created at the taper end by acceleration, displacement and retardation. These flows advance through the stirred medium and result in the new dynamic mixing motion RZR 1 P/N A 2-gear stage design allows for high torque at various speeds and provides excellent mixing in short times 94 95

49 Technical Specifications - Overhead Stirrers Model RZR 1 Hei-TORQUE Value 100 Hei-TORQUE Value 200 Hei-TORQUE Value 400 Hei-TORQUE Precision 100 Hei-TORQUE Precision 200 Hei-TORQUE Precision 400 P/N (115 V) Power rating, motor input/output (W) 77/18 90/50 120/80 150/90 90/50 120/80 150/90 Number of speed gears Speed range (rpm) , , , , , , ,000 Certificate Speed indicator scale digital monochrom 2.4" digital monochrom 2.4" digital monochrom 2.4" digital color 3.2" digital color 3.2" digital color 3.2" Speed control mechanic electronic electronic electronic electronic electronic electronic Torque, maximum (Ncm) Torque indicator symbol symbol symbol precise value precise value precise value Overheat protection Motor protection automatic cut-out temperature control software automatic cut-out temperature control software automatic cut-out temperature control software automatic cut-out temperature control software automatic cut-out temperature control software automatic cut-out temperature control software automatic cut-out temperature control software Viscosity, max. (mpa s) 40,000 60, , ,000 60, , ,000 Stirring cap. (H2O), max. (l) Analog / digital interface USB or RS 232 USB or RS 232 USB or RS 232 To confirm the ability for continuous operation of the Hei-TORQUE series Overhead Stirrers Admissible session continuous operation continuous operation continuous operation continuous operation continuous operation continuous operation continuous operation Counter/Timer yes yes yes Shaft diameter, max. (mm) Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel. Dimensions (wxhxd) (mm) 71 x 250 x x 328 x x 328 x x 328 x x 328 x x 328 x x 328 x 241 Stay bar size (dia. x l) (mm) 13 x x x x x x x 160 Weight (kg) Protection class (DIN EN 60529) IP 20 IP 54 IP 54 IP 54 IP 54 IP 54 IP 54 The Hei-TORQUE series Overhead Stirrers feature overtemperature safety circuits according to DIN EN :2001 and DIN EN :2015 and therefore is designed for continuous operation. This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Standard supply voltage: 115 V - other voltages upon request, please specify for order Schwabach, January 2017 Stefan Peters Research and Development Manager Marcell Sarré Quality Manager 96 97

50 Temperature- Controlled Shaking Hei-MIX Shakers & Mixers Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

51 Leading Safety Standards An overtemperature sensor preventively shuts off the unit in a dangerous heat-up situation particularly valuable in case of continuous operation or sensitive research Our shaker stays in place to rule out accidents: all models have been designed with a low center of gravity which prevents gliding at high speed, including placement on a damp surface All platform shakers come with a unique non-skid rubber mat that prevents vessels from sliding, including models performing three dimensional movements Superior Ease of Use Would you love to utilize a complete range of platform shakers which provides you with many possible movements? Your work requires multiple shaking motions and flask sizes? A large range of shakers and load capacities - from test tube shakers to large multitier platform shakers - serves your needs while making your life easy with one brand We offer selected accessories and attachments specific to each model that best matches your application needs Choose from six specific motions, from one to three dimensional movements: vibrating, orbital, reciprocating, rocking, wave and overhead rotation Within one specific shaking motion, you can even choose different shaking orbits and angles to differentiate between soft or rigid shaking Choose from three different load capacities of 2, 5 or 10 kg depending on model to save bench space or for high sample throughput Temperature- Controlled Shaking Choose from six specific motions - from one to three dimensional movements, from three different load capacities and optional upgrade to an incubator shaker! 3 different load capacities Different movement amplitudes Stays in place Temperature- Controlled Overheat protection Reduced Cost of Ownership Increase your sample throughput and reduce your process times with the modular system for shaking, mixing and heating all in one Are you working with heat-sensitive samples? Platform shakers come with an insulated system to prevent any heat transfer from the motor that could cause potential thermal damage to your sample. This saves you time and money Maintenance-free motors reduce repairs and down times significantly to ensure years of continuous operation backed by the Heidolph 3-year warranty Clear and self-explanatory front panel layout allows for easy operation The sealed housing on many models protects your shaker from aggressive fumes, liquids and vapors to prevent internal corrosion. This results in an increased lifespan of 10 years on average at reduced maintenance and repair costs

52 Always the right motion Our complete range of bench-top shakers provides you with any possible movement for your research. This makes us the right choice for the right motion of your application YOUR ADVANTAGES Temperature- Controlled Shaking Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. reciprocating rocking vibrating overhead No spills: You can select from a wide range of secure flask attachments for all common vessels and sizes No compromise: Shake whatever you want with this range of products, you will achieve outstanding mixing results, no matter how individualized your process requirement demands An overtemperature sensor preventively shuts off the unit in a dangerous heat-up situation particularly valuable in case of continuous operation Rule out accidents: all models have been designed Choose between different shaking motions, with a low center of gravity which prevents gliding at orbits, angles and load capacities: the right high speed, even on a damp surface model for your specific application wave orbital No limitations: Choose from six specific motions, from one to three-dimensional movements - many models offer options of different orbits and angles to provide increased mixing in the motion range Patented optional incubator system Temperature-controlled shaking is possible simultaneously for each application Unlimited visual reaction control at all times: the transparent, nonfogging PETG material offers it all YOUR ADVANTAGES Use your limited bench space more efficiently: The modular incubator system comes with the smallest footprint compared to any other common shaker system Instantly upgrade your platform shaker to an affordable incubator system using the modular concept Full flexibility! No matter how large your vessels are, three incubator hood sizes allow for volumes up to 2-liter Erlenmeyer flasks Immediate access: optional incubator hood opens instantly and interlocks in any position For applications in microbiology: the insulated drive system prevents any heat build-up from the motor and consequently thermal damage to your sample

53 Test Tube Shakers vibrating Ideal for mixing samples in Eppendorf tubes, vials and similar vessels of different diameters at extremely high speed rates. The ridged mixing orbit yields consistent results and is ideal for product dissolution Multi Reax The all-purpose model Reax top The standard model The strong 5-mm vibration orbit yields the best results even with high viscosity media or solids out of solution and quickly gives a smooth and even dispersion Unique shaker to accommodate up to 26 vessels with various diameters. Shipment includes as a standard: Attachment for 26 vessels with diameters from 10 to 16 mm Attachment for 12 vessels with diameters from 16 to 32 mm The 3-mm vibration orbit allows for excellent mixing results in large and solid samples Set and continuously adjust the variable speeds from 150 to 2,000 rpm on the digital display A digital process timer allows for unattended operation and can be set from 1 to 999 minutes. When the set time has elapsed, an acoustic alarm will sound and the operation stops Switch to continuous mode the unit performs a permanent vibration motion Switch to automatic mode - the unit will start once a vessel is pressed to the plate and will stop automatically once this pressure is released Fast and dependable mixing results due to high vibration frequency rates up to 2,500 rpm Plate for 20-mm diameter test tubes is included as a standard. Test tube tray for flasks up to 50-mm diameter is optionally available in the accessory section P/N Accessories: Category A Reax control The accurate model Includes all Reax top features, plus: Analog dial speed control with accurate rpm numbers setting Improve your results with the electronic speed control that provides constant rpm output even at very low speed and under changing loads P/N P/N Accessories: Category A

54 Platform Shakers vibrating Do you perform research which requires ridged or gentle shaking for small samples on microtiter plates or test tubes? Five options with different load capacities and shaking orbits are available for you! Vibramax 100 The compact model Vibramax 100 is a compact and space saving unit with a load capacity of 2 kg The 3-mm vibration orbit gives excellent results especially in large vessels allows for smooth to ridged mixing of viscous media and solids Set and continuously adjust the variable speed on the analog control knob from 150 to 1,350 rpm Optional attachment with tension rollers accepts any glassware size A large selection of attachments is provided for the use of various vessels and sizes An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops P/N Accessories: Category C P/N Accessories: Category B Vibramax 110 The efficient model Ideal for the optional attachment to use 49 test tubes that increases your throughput significantly The shaking orbit of 1.5 mm performs a gentle motion for sensitive samples Set and continuously adjust the variable speed on the analog control knob from 150 to 2,500 rpm An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops Titramax Titramax 100 The compact model Titramax 101 The strong model Titramax 100 is a compact and space-saving unit that accepts load capacities of 2 kg and space for four microtiter plates The 1.5-mm vibration orbit performs gentle mixing with best results using small sample volumes. The Titramax 101 has a 3-mm orbit which was designed for larger sample volumes Set and continuously adjust the variable speed on the analog control knob from 150 to 1,350 rpm An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops Titramax 1000 P/N Titramax Package This package includes: One vibrating platform shaker Titramax 1000 One heating module and One flat incubator hood P/N Titramax 100 (not shown) P/N Titramax 1000 The incubating model Titramax 101 P/N The use of six microtiter plates increases your throughput by 50 % The 1.5-mm vibration orbit performs gentle mixing with best results using small sample volumes Titramax 1000 is a medium-sized model and accepts load capacities of 5 kg This model is suitable for the modular incubator system and is recommended for applications which require variable temperature control up to 65 C Set and continuously adjust the variable speed on the analog control knob from 150 to 1,350 rpm An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops

55 Platform Shakers orbital Time and tranquility are required for the cultivation of cells The slow and constant rotation of the Rotamax and Unimax models keeps your samples continuously in motion Unimax 1010 The incubating model The Unimax 1010 is a medium sized model and accepts load capacities of 5 kg The shaking orbit of 10 mm performs a gentle motion for sensitive samples and supports culture plates and Erlenmeyer flasks Set and continuously adjust the variable speed on the digital display from 30 to 500 rpm This model is suitable for the modular incubator system and is recommended for applications which require variable temperature control up to 65 C An digital process timer allows for unattended operation and can be set from 1 to 999 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops P/N Accessories: Category D Unimax 2010 The resilient model The Unimax 2010 is a large model and accepts a load capacity of 10 kg for high sample throughput The shaking orbit of 20 mm performs a gentle motion for sensitive samples and supports culture plates and Erlenmeyer flasks Rotamax 120 The compact model Rotamax 120 is a compact and space-saving unit that accepts load capacities of 2 kg P/N Accessories: Category B P/N Accessories: Category E Set and continuously adjust the variable speed on the digital display from 20 to 400 rpm Increase your sample throughput with the optional multi-tier attachment for a variety of vessel sizes An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops Wide range of accessories, attachments and clamps for up to 16 Erlenmeyer flasks available The shaking orbit of 20 mm performs a gentle motion for sensitive samples and supports culture plates and Erlenmeyer flasks Set and continuously adjust the variable speed on the analog control knob from 20 to 300 rpm An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops Unimax Package This package includes: One orbital platform shaker Unimax 1010 One heating module and One high incubator hood P/N

56 Platform Shakers rocking Platform Shakers - reciprocating Focus on cell culture, mix in large media bottles and require a two-dimensional motion with flexibility to heat? The Duomax is available in two different angle configurations which are recommended for culture plates/bottles, media bottles and Erlenmeyer flasks to help cultivate cells Are you missing the right shaker for separations in chemistry or for the performance of soil tests? All Promax models are designed especially for phase separations using separatory funnels or applications that require reciprocating motion! Promax 1020 The incubating model The Promax 1020 is a medium-sized model and accepts load capacities of 5 kg Wide range of accessories, attachments and clamps for separatory funnels available With a stroke length of 32 mm the Promax model performs an ideal motion for separatory funnels Set and continuously adjust the variable speed on the digital display from 30 to 250 rpm This model is suitable for the modular incubator system and is recommended for applications which require variable temperature control up to 65 C An digital process timer allows for unattended operation and can be set from 1 to 999 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops P/N Accessories: Category D Duomax 1030 The incubating model The Duomax 1030 is a medium-sized model and accepts load capacities of 5 kg Choose your angle between these two options: tilt angle of 5 for soft and gentle movements or tilt angle of 10 for a much stronger motion Set and continuously adjust the variable speed on the analog control knob from 2 to 50 rpm ideal for media bottles This model is suitable for the modular incubator system and is recommended for applications which require variable temperature control up to 65 C An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops Features tilt angle of 5 P/N Features tilt angle of 10 P/N Accessories: Category D P/N Accessories: Category E Promax 2020 The resilient model The Promax 2020 is a large model and accepts a load capacity of 10 kg for high sample throughput With a stroke length of 20 mm this Promax model can mix larger volumes with ease Set and continuously adjust the variable speed on the digital display from 20 to 400 rpm ideal for separations Wide range of accessories, attachments and clamps for separatory funnels available An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops

57 Platform Shakers wave Incubator 1000 Nothing beats a three-dimensional motion: For best mixing results of viscous media such as gels for electrophoresis, you can also choose the tilt angle that works best for the application Polymax 1040 Your platform shaker has no space in your heating oven or incubator cabinet? Adjustable temperature and visual control are key priorities for you? This truly unique system enables you to perform a number of functions simultaneously - shaking, mixing and heating with visual reaction control. These platform shakers are compatible with the incubator system: Duomax 1030, Polymax 1040, Titramax 1000, Unimax 1010 and Promax 1020 Features tilt angle of 5 P/N Features tilt angle of 10 P/N Accessories: Category D The incubating model The Polymax 1040 is a medium-sized model and accepts load capacities of 5 kg Choose your angle between these two options: tilt angle of 5 for soft and gentle movements or tilt angle of 10 for a much stronger motion Use this model for any vessel from culture plates and media bottles to Erlenmeyer flasks there is no limit Set and continuously adjust the variable speed on the analog control knob from 2 to 50 rpm ideal for cell culture plates This model is suitable for the modular incubator system and is recommended for applications which require variable temperature control up to 65 C An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops YOUR ADVANTAGES Heating module allows for gentle temperature adjustments up to 65 C The electrical heater allows for quick and even temperature distribution throughout the entire enclosure Unlimited visual reaction control at all times: the transparent and non-fogging PETG construction offers it all Three options available: a flat hood for small vessels and microtiter plates, a high hood for all common medium-sized vessels and even a high hood XL for larger Erlenmeyer flasks up to 2,000 ml Immediate access: the incubator hood opens instantly and interlocks in any position Use ONE incubator for numerous shakers - interchangeability is ensured and takes less than 2 minutes. You can incubate and mix simultaneously or independently Polymax 2040 Heating module The resilient model The Polymax 2040 is a large model and accepts a load capacity of 10 kg for high sample throughput Choose your angle between these two options: tilt angle of 5 for soft and gentle movements or tilt angle of 10 for a much stronger motion Heating capacity of 300 W allows for quick temperature adjustments Digital temperature settings up to 65 C and separate display for actual temperature To protect your sample from thermal damages this unit features a safety circuit to prevent overheating Use this model for any vessel from culture plates and media bottles to Erlenmeyer flasks there is no limit Set and continuously adjust the variable speed on the digital display from 2.5 to 50 rpm ideal for cell culture plates Features tilt angle of 5 P/N Features tilt angle of 10 P/N Accessories: Category E Electrical heater comes with low-noise blower and provides accuracy of ± 2 C up to 50 C and ± 4 C over 50 C P/N An analog process timer allows for unattended operation and can be set from 1 to 120 minutes. When the set time has elapsed an acoustic alarm will sound and the operation stops

58 Incubator 1000 Overhead Shakers Incubator hoods Combine the heating module with an incubator hood of your choice: Complies with standards for the determination of elutriation with water Flat hood For small vessels Reax 20 The small incubator hood has a total height of 163 mm Overhead shakers for 4, 8 or even 12 bottles Recommended especially for microtiter plates, culture plates, small flasks, media bottles and Erlenmeyer flasks up to 100 ml Transparent and non-fogging PETG material allows for sample viewing and easy cleaning Flat hood P/N Set and continuously adjust the variable speed on the analog control knob from 1 to 16 rpm ideal for waste water analysis A model with a rotation speed of 2 to 32 rpm is available upon request Easy and fast attachments of bottles High hood Other vessels with mm height and max. 136-mm diameter can be used with attachments For high vessels and flasks The high incubator hood has a total height of 267 mm Reax 20/4 (not shown) P/N Accessories: Category G Reax 20/8 P/N Accessories: Category G Reax 20/12 (not shown) P/N Accessories: Category G Recommended especially for large flasks and media bottles, Erlenmeyer flasks up to 500 ml and mediumsized or large common vessels High hood P/N Transparent and non-fogging PETG material allows for sample viewing and easy cleaning Reax 2 Quickly clamps in 2 vessels of any size and accepts load capacities up to 1 kg Speed continuously adjustable from 20 to 100 rpm High hood XL Universal adaptor allows for the use of various vessels of mm height For 2,000-ml vessels The high hood XL has a total height of 428 mm In addition, an optional adaptor is available for the use of 20 test tubes at a time Recommended especially for 2,000-ml Erlenmeyer flasks Transparent and non-fogging PETG material allows for sample viewing and easy cleaning P/N Accessories: Category F High hood XL P/N

59 Accessories A Test tube tray, large For test tubes and flasks up to 50 ml P/N A Test tube holding device Attachment to hold one test tube safely for continuous shaking P/N A Attachment for 10 test tubes For up to 10 test tubes with Ø 10 mm, length up to 60 mm P/N A Test tube stand For up to 6 Eppendorf vessels (1.5 ml) P/N D Frame with tension roller Attachment with 2 tension rollers P/N D Spare tension roller 1 tension roller as accessory for attachment P/N P/N E Perforated platform 2000 Universal perforated platform allows for individual arrangement of vessels P/N E Frame tension roller Frame without tension roller P/N B Tension roller attachment Attachment with 2 tension rollers P/N B Spare tension roller 1 tension roller for attachment P/N P/N B Perforated platform 100 Universal perforated platform allows for individual arrangement of vessels P/N C Test tube attachment For up to 49 test tubes with Ø 12 mm, length up to 80 mm P/N For up to 36 test tubes with Ø 16 mm, length up to 80 mm P/N E Tension roller 1 tension roller for the frame P/N , please order 2 pcs. min. P/N E Multi-tier attachment Includes perforated platform 2000 and 4 supporting rods P/N F Adaptor for 20 test tubes Allows for simultaneously mixing 20 test tubes Ø mm with just one shaker P/N G Tension plate for caps Allows for the use of common bottles with Ø 94 mm P/N D 25-ml Erlenmeyer attachment Attachment for up to 22 Erlenmeyer flasks with a size of 25 ml P/N D 50-ml Erlenmeyer attachment Attachment for up to 14 Erlenmeyer flasks with a size of 50 ml P/N D 100-ml Erlenmeyer attachment Attachment for up to 9 Erlenmeyer flasks with a size of 100 ml P/N D 250-ml Erlenmeyer attachment Attachment for up to 5 Erlenmeyer flasks with a size of 250 ml P/N G Attachment for 0.5-l bottles (Set of 4) Allows for the use of four 0.5-l bottles P/N G Attachment for 1-l bottles (Set of 4) Allows for the use of four 1-liter bottles P/N S Separatory funnel clamp (250 ml, 500 ml, 1000 ml) For perforated platform 2000, space for max. 4 (250 ml), 3 (500 ml) or 3 (1000 ml) clamps P/N S Separatory funnel clamp (2000 ml) For perforated platform 2000, space for max. 2 clamps P/N D 500-ml Erlenmeyer attachment Attachment for up to 4 Erlenmeyer flasks with a size of 500 ml P/N D 1000-ml Erlenmeyer attachment Attachment for up to 2 Erlenmeyer flasks with a size of 1000 ml P/N D Perforated platform 1000 Universal perforated platform allows for individual arrangement of vessels P/N D Separatory funnel attachment Attachment for 4 separatory funnels (50 ml, conical) or 4 separatory funnels (100 ml, conical) P/N S - Clamps for the perforated platform 100, 1000 and 2000 Accessories for: Size 1 For 25-ml Erlenmeyer flasks Size 2 For 50-ml Erlenmeyer flasks Size 3 For 100-ml Erlenmeyer flasks Size 4 For 250-ml Erlenmeyer flasks Size 5 For 500-ml Erlenmeyer flasks Size 6 For 1000-ml Erlenmeyer flasks Size 7 For 2000-ml Erlenmeyer flasks A Reax top/control B Vibramax 100, Rotamax 120 C Vibramax 110 D Unimax 1010, Duomax 1030, Polymax 1040, Promax 1020 E Unimax 2010, Promax 2020, Polymax 2040 F Reax 2 G Reax 20/4 20/8 20/12 S Additional Accessories for Shakers & Mixers P/N For platform 100 max. 16 max. 16 max. 8 max. 5 max. 3 max. 2 For platform 1000 max. 20 max. 20 max. 14 max. 8 max. 4 max. 4 max. 2 For platform 2000 max. 36 max. 36 max. 23 max. 12 max. 9 max. 5 max

60 Technical Specifications - Shakers and Mixers Model Reax top Reax control Multi Reax Titramax 100 Titramax 101 Titramax 1000 Vibramax 100 Vibramax 110 Rotamax 120 Motion vibrating vibrating vibrating vibrating vibrating vibrating vibrating vibrating orbital Rotation speed (rpm) 0 2, , , , , , , , Rotation speed setting analog analog digital electronic contr. electronic contr. electronic contr. electronic contr. electronic contr. electronic contr. Orbit (mm) Operating mode automatic or automatic or timer or timer or timer or timer or timer or timer or timer or continuous continuous continuous continuous continuous continuous continuous continuous continuous Certificate Input power (W) Weight (kg) Dimensions (w x h x d) (mm) 134 x 105 x x 105 x x 172 x x 125 x x 125 x x 125 x x 125 x x 146 x x 125 x 310 Platform size (mm) 220 x x x x x x 220 Accessories included 2 carousel attachments space for 4 microtiter plates space for 4 microtiter plates space for 6 microtiter plates non-skid rubber mat non-skid rubber mat Load capacity (kg) Overheat protection Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel. non-skid rubber mat 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel. To confirm the ability for continuous operation of the Test Tube and Platform Shakers Protection class (DIN EN 60529) IP 22 IP 22 IP 30 IP 30 IP 30 IP 30 IP 30 IP 30 IP 30 Model Unimax 1010 Unimax 2010 Promax 1020 Promax 2020 Duomax 1030 Polymax 1040 Polymax 2040 Reax 2 Reax 20/4 Reax 20/8 Reax 20/12 Motion orbital orbital reciprocating reciprocating rocking wave wave overhead overhead Rotation speed (rpm) The Test Tube and Platform Shakers feature overtemperature safety circuits according to DIN EN :2001 and DIN EN :2015 and therefore is designed for continuous operation. Rotation speed setting digital digital digital digital electronic contr. electronic contr. digital analog electronic contr. Orbit / Stroke (mm) Angle ( ) 5/10 5/10 5/10 timer or timer or timer or timer or timer or timer or timer or Operating mode continuous continuous continuous continuous continuous continuous continuous Input power (W) This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Weight (kg) , 28, 33 Dimensions (w x h x d) (mm) 320 x 125 x x 135 x x 125 x x 135 x x 185 x x 195 x x 208 x x 180 x 235 Platform size (mm) 290 x x x x x x x 340 Reax 20/4 490 x 465 x 520 Accessories included non-skid rubber mat non-skid rubber mat non-skid rubber mat non-skid rubber mat non-skid rubber mat non-skid rubber mat non-skid rubber mat universal adaptor Reax 20/8 770 x 465 x 520 Reax 20/ x 465 x 520 selfresetting selfresetting selfresetting selfresetting selfresetting selfresetting selfresetting selfresetting selfresetting Load capacity (kg) selfresettinresettinresettinresettinresettinresettinresettinresetting self- self- self- self- self- self- self- selfresetting Overheat protection Schwabach, January 2017 Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel. Protection class (DIN EN 60529) IP 40 IP 20 IP 40 IP 20 IP 40 IP 40 IP 20 IP 21 IP 21 Standard supply voltage: 115 V - other voltages upon request, please specify for order Stefan Peters Research and Development Manager Marcell Sarré Quality Manager

61 Precise Dosing and Dispensing Hei-FLOW Peristaltic Pumps Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

62 Leading Safety Standards Important for continuous unattended operation: the motor will be switched off if a high thermal load situation occurs to increase safety in your lab and to prevent accidents Additional safety is provided by sparkless motors which reduce incidents All models feature a smooth start operation that prevents spilling and splashing of media. The speed will ramp up slowly until your set rpm has been reached Protection class IP 55 protects your unit from highly aggressive vapors or liquids and thus eliminates accidents, short-circuits and failures Use an optional foot-pedal remote control via cable to start and stop your pump drive outside a closed fume hood increasing your personal safety The pumped media remains in the tubing and never comes in contact with you keeping you and your application safe Superior Ease of Use Are you in need of a system that provides the most accurate pumping and dosing of aggressive, corrosive or even sterile media without any compromise to precision? The Hei-FLOW series is self-priming and comes without any valves, thus providing care-free operation Analog and digital interfaces facilitate operation, e.g. by connecting the optional foot-pedal Use your valuable lab space efficiently and stack one pump on top of the other to build a space-saving two-layer system Use a single-channel pump head and upgrade your model to multi-channel operation in just minutes with a different pump head Our clear and self-explanatory front panel layout is for your ease of operation Make your life easier and rely on the accurate liquid delivery starting from ml/min Precise Dosing and Dispensing The versatile Hei-FLOW series can offer you all these options with flow rates ranging from to 4,151 ml per minute depending on configuration! Reduced Cost of Ownership Reduce your maintenance costs: the sealed housing protects your pump from aggressive fumes, liquids and vapors to prevent internal corrosion. This results in an increased lifespan of 10 years on average while reducing maintenance and repair cost Complete packages including pump drive, head and compatible tubing reduce your selection process and give you a reduced package price Maintenance-free motors eliminate repairs and down times to ensure years of continuous operation Optional remote control Starting at ml / min Highest precision IP 55 Smooth start

63 Precise dosing and dispensing Are you in need of a system that provides the most accurate pumping and dosing of aggressive, corrosive or even sterile media without any compromise to precision? The versatile Hei-FLOW series offers you all these options - with flow rates ranging from to 4,151 ml per minute depending on configuration Precise Dosing and Dispensing Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a worthwhile investment. Pump heads YOUR ADVANTAGES If you are looking for standard pumping or highly accurate interval dosing and interval operation allowing for standstills and filling of flasks, the Hei-FLOW series has it all Your application media never comes in contact with the pump head eliminating cross-contamination and the need to clean the unit between projects The pumped media remains in the tubing and never comes in contact with you keeping you and your application safe The versatile Hei-FLOW series offers you all these options - with flow rates ranging from to 4,151 ml per minute depending on configuration Choose from six different pump drives, three pump heads for single-channel use, and three additional pump heads for multi-channel use that can accommodate up to twelve cassettes Are you engaged in a highly specialized application such as cell biology and do you need to transfer the cells without causing damage? Safety for continuous operation: the motor will be switched off if a high thermal load situation occurs to prevent accidents Protection class IP 55 to prevent corrosion and short circuits High precision even for flow rates starting at ml/min Optional foot-pedal remote control via cable to operate pump drive from outside closed fume hoods facilitate operation The Hei-FLOW series offers you solutions for standard applications and highly sophisticated challenges that require added control! YOUR ADVANTAGES For the use in cell biology, choose a pump head which features convex rollers that do not squeeze the tubing, as would conventional rollers Consequently, organic cell cultures are not crushed and your samples are safely transported A wide range of tubing material is available choose the most appropriate material for your research: whether FDA-approved material for food analysis or material for aggressive media such as acids you find it right here All models feature a smooth start operation which prevents spills and splashing media. The speed will ramp up slowly until your set rpm has been reached For the use in cell biology just use a pump head which features convex rollers and does not squeeze the tubing as conventional rollers

64 Hei-FLOW Value 01 / Hei-FLOW Value 06 Hei-FLOW Advantage 01 / Hei-FLOW Advantage 06 For standard applications and liquid transfer Pumps include leading safety standards and features for superior ease of use and reduced cost of ownership, plus: For reproducible results and liquid transfer Pumps include leading safety standards and features for superior ease of use and reduced cost of ownership, plus: Adjust the variable speed from rpm on the analog control knob. Your speed is held constant even under changing loads These models feature electronic speed control at an accuracy rate of ± 2 % At the press of a button the pump operates clockwise or counter-clockwise Control speed (rpm), direction and On/Off function via analog interface for 0 10 V or 4 20 ma Adjust the variable speed from rpm on the analog control knob. Your speed is held constant even under changing loads These models feature electronic speed control at an accuracy of ± 0.5 % These models connect to an optional foot-pedal remote control via cable to start and stop your pump drive outside a closed fume hood increasing your personal safety and superior ease of use in multiple sample fills A press of the max button accelerates the filling and draining of your tube At the press of a button the pump operates clockwise or counter-clockwise Hei-FLOW Value 01 Hei-FLOW Value 06 Hei-FLOW Advantage 01 Hei-FLOW Advantage 06 Flow rates of ml/min with single-channel pump heads Flow rates of 3.0-4,151 ml/min with single-channel pump heads Flow rates of ml/min with single-channel pump heads Flow rates of 1.0-4,056 ml/min with single-channel pump heads Low speed range from rpm High speed range from rpm Low speed range from rpm High speed range from rpm This pump drive is suitable for multi-channel operation Multi-channel flow rates from ml/min This pump drive is not suitable for multi-channel operation This pump drive is suitable for multi-channel operation Multi-channel flow rates from ml/min This pump drive is not suitable for multi-channel operation Upgrade your Hei-FLOW Value 01 for multi-channel operation in just minutes with a pump head adaptor: P/N Hei-FLOW Value 06 P/N Upgrade your Hei-FLOW Advantage 01 for multi-channel operation in just minutes with a pump head adaptor: P/N Hei-FLOW Advantage 06 P/N Hei-FLOW Value 01 P/N Hei-FLOW Value 01 Multi (incl. adapter for multi-channel pumps heads) P/N Hei-FLOW Advantage 01 P/N Hei-FLOW Advantage 01 Multi (incl. adapter for multi-channel pumps heads) P/N

65 Hei-FLOW Precision 01 / Hei-FLOW Precision 06 Single-Channel Pump Heads Reproducibility - pumping and dosing Pumps include leading safety standards and features for superior ease of use and reduced cost of ownership, plus: Control speed (rpm), direction and On/Off function via analog interface for 0 10 V or 4 20 ma or digital RS 232 interface Flow characteristic of pump heads in combination with various tubing diameters is pre-programmed for accurate flow rate numbers Digital read-out of: - Speed (rpm) - Tubing diameter - Flow rate in ml/min - Dosing volume - Interval dosing - Pause function Easily change all process parameters via control buttons These models connect to an optional foot-pedal remote control via cable to start and stop your pump drive outside a closed fume hood increasing your personal safety and superior ease of use in multiple sample fills These models feature electronic speed control at an accuracy of ± 0.5 % A press of the max button accelerates the filling and draining of your tube At the press of a button the pump operates clockwise or counter-clockwise Calibrate your flow volume and flow rate individually SP quick Fast and convenient tube changes Pump head features ball bearings Rollers made of stainless steel Low pulsation due to 5 roller system For tubes with a 1.6-mm or 2.5-mm wall thickness (wt) Depending on drive and tubing, flow rate ranges from 0.38 to 3,436 ml per minute SP standard SP quick P/N (wt 1.6 mm) P/N (wt 2.5 mm) Recommended for standard applications Pump head features ball bearings Convex rollers do not squeeze or crush organic cell cultures Rollers made of stainless steel and polyamide For tubes with a 1.6-mm or 2.5-mm wall thickness (wt) Depending on drive and tubing, the flow rate ranges from 2.0 to 4,151 ml per minute Flow rate (ml/min) SP quick Speed (rpm) SP standard P/N (wt 1.6 mm) P/N (wt 2.5 mm) SP vario P/N Hei-FLOW Precision 01 Flow rates of ml/min with single-channel pump heads Low speed range from rpm This pump drive is suitable for multi-channel operation Multi-channel flow rates from ml/min Hei-FLOW Precision 06 Flow rates of 1.0-4,056 ml/min with single-channel pump heads High speed range from rpm This pump drive is not suitable for multi-channel operation Flow rate (ml/min) SP standard / SP vario SP vario Suitable for most Heidolph tubing due to adjustable roller spacing Pump head features ball bearings Rollers made of stainless steel and aluminum Convex rollers do not squeeze or crush organic cell cultures Depending on drive and tubing, the flow rate ranges from 2.0 to 4,151 ml per minute Upgrade your Hei-FLOW Precision 01 for multi-channel operation in just minutes with a pump head adaptor: P/N Hei-FLOW Precision 06 P/N Speed (rpm) Hei-FLOW Precision 01 P/N Hei-FLOW Precision 01 Multi (incl. adapter for multi-channel pumps heads) P/N = Single-channel pump

66 Tubing Sizes for Single-Channel Pumps Multi-Channel Pumps Tubing sizes Inner diameter (mm) Outer diameter (mm) Wall thickness (wt) (mm) Max. pressure (continuous / short time) (bar) 0.7 / / / / / 1.5 Suction height (mh 2O) Average flow rates in combination with pump head and pump drive: SP quick min. max. min. max. min. max. min. max. min. max. Hei-FLOW Advantage 06 / Hei-FLOW Precision 06 (ml/min) , ,072 Hei-FLOW Value 06 (ml/min) , ,765 Hei-FLOW Advantage 01 / Hei-FLOW Precision 01 (ml/min) Hei-FLOW Value 01 (ml/min) SP standard / SP vario min. max. min. max. min. max. min. max. These pump drives can be configured for multi-channel use: Hei-FLOW Value 01, Hei-FLOW Advantage 01, Hei-FLOW Precision 01 Increase your throughput by running up to 12 individual cassettes on one single pump drive and pump head system Separate metering into multiple vessels with different feed rates in a single operation by using different tubing dimensions to adjust flow rate Save time: tubing change is done in just seconds In addition to standard pump heads which feature a 4-roller system you can choose 8-roller pump heads for low pulsation Change your cassettes easily, even during operation there are no restrictions Cassette adjustments and changes are simple, just click in place No additional purchase of a pump drive needed: upgrade your single-channel pump drive with just one adaptor for multi-channel use and pick the head/ cassette configuration that matches your application needs Hei-FLOW Advantage 01 + adaptor + pump head C 4 + cassette small Hei-FLOW Advantage 06 / Hei-FLOW Precision 06 (ml/min) , , ,056 Hei-FLOW Value 06 (ml/min) , , ,151 Hei-FLOW Advantage 01 / Hei-FLOW Precision 01 (ml/min) Hei-FLOW Value 01 (ml/min) Multi-channel pump heads Tubing P/N (per meter): Silicone Viton PharMed Tygon (standard) Tygon (hydrocarbon) Tygon 2001 (food) not suitable for pump drive Hei-FLOW Value Multi-channel pump head C 12 P/N Accepts 12 cassettes small Built-in reduction gear allows feeding of smallest quantities 8 rollers minimizing pulsation Multi-channel pump head C 8 P/N Accepts 8 cassettes medium or 4 cassettes large 4-roller design Multi-channel pump head C 4 P/N Accepts 4 cassettes small 8 rollers for low pulsation Tubing sizes Inner diameter (mm) Outer diameter (mm) Wall thickness (wt) (mm) Max. pressure (continuous / short time) (bar) 0.8 / / / 1.8 Suction height (mh 2O) Average flow rates in combination with pump head and pump drive: SP quick min. max. min. max. min. max. Hei-FLOW Advantage 06 / Hei-FLOW Precision 06 (ml/min) 58 1, , ,171 Hei-FLOW Value 06 (ml/min) 123 1, , ,436 Hei-FLOW Advantage 01 / Hei-FLOW Precision 01 (ml/min) Flow rate (ml/min) Pump head C Flow rate (ml/min) Pump head C Flow rate (ml/min) Pump head C Hei-FLOW Value 01 (ml/min) Speed (rpm) Speed (rpm) Speed (rpm) SP standard / SP vario min. max. min. max. Hei-FLOW Advantage 06 / Hei-FLOW Precision 06 (ml/min) 92 2, ,821 Flow rates pertain to water Hei-FLOW Value 06 (ml/min) 203 2, ,782 Hei-FLOW Advantage 01 / Hei-FLOW Precision 01 (ml/min) Hei-FLOW Value 01 (ml/min) Tubing P/N (per meter): Silicone Viton PharMed Tygon (standard) Tygon (hydrocarbon) Tygon 2001 (food) not suitable for pump drive Hei-FLOW Value = Multi-channel pump

67 Multi-Channel Cassettes Tubing Sizes for Multi-Channel Pumps Setting screws to adjust roller contact pressure Cassettes easily change even while pumping All cassettes accept different tube materials and sizes Tubing sizes Inner diameter (mm) Outer diameter (mm) Wall thickness (wt) (mm) Cassette small Flow rates from to 37 ml/min Stoppers secure tube in place Suitable for tubes with 0.9-mm wall thickness (wt) Tube diameters available: 0.2 / 0.5 / 0.9 / 1.4 and 2.8 mm Two-Stop Tubing (40 cm) required to operate cassette small Couplings and tube extensions allow extra hose length in 1-m increments Combinations: C 4 multi-channel pump head: Max. 4 cassettes small C 12 multi-channel pump head: Max. 12 cassettes small Cassette small P/N Two-Stop Tubing Max. pressure (continuous / short time) (bar) 0.5 / / / / / 1.5 Suction height (mh 2O) Average flow rates in combination with cassette, pump head and pump drive: Hei-FLOW Advantage 01 / Hei-FLOW Precision 01 min. max. min. max. min. max. min. max. min. max. max. number of cassettes Cassette small / pump head C 12 (ml/min) Cassette small / pump head C 4 (ml/min) Hei-FLOW Value 01 min. max. min. max. min. max. min. max. min. max. Cassette small / pump head C 12 (ml/min) Cassette small / pump head C 4 (ml/min) Tubing P/N: Silicone Two-Stop Tubing for cassette small Extension tube (per meter) Viton Two-Stop Tubing for cassette small Extension tube (per meter) Cassette medium Flow rates from 0.24 to 27 ml/min Tube available in requested sizes Suitable for tubes with 1.6-mm wall thickness (wt) Tube diameters available: 0.8 and 1.7 mm Combinations: C 8 multi-channel pump head: Max. 8 cassettes medium PharMed Two-Stop Tubing for cassette small Extension tube (per meter) Tygon (standard) Two-Stop Tubing for cassette small Extension tube (per meter) Fittings for extension tubes (PTFE) Tubing sizes Inner diameter (mm) Outer diameter (mm) Wall thickness (wt) (mm) Max. pressure (continuous / short time) (bar) 0.7 / / / / / 1.5 Suction height (mh 2O) Cassette medium P/N Average flow rates in combination with cassette, pump head and pump drive: Hei-FLOW Advantage 01 / Hei-FLOW Precision 01 min. max. min. max. min. max. min. max. min. max. max. number of cassettes Cassette medium / pump head C 8 (ml/min) Cassette large Flow rates from 1 to 364 ml/min Suitable for tubes with 1.6-mm wall thickness (wt) Tube diameters available: 1.7 / 3.1 / 4.8 and 6.4 mm Tube available in requested sizes Combinations: C 8 multi-channel pump head: Max. 4 cassettes large Cassette large / pump head C 8 (ml/min) Hei-FLOW Value 01 min. max. min. max. min. max. min. max. min. max. Cassette medium / pump head C 8 (ml/min) Cassette large / pump head C 8 (ml/min) Tubing P/N (per meter): Silicone Viton PharMed Tygon (standard) Tygon (hydrocarbon) Cassette large P/N Tygon 2001 (food) Flow rates pertain to Tygon (standard) tubing and water

68 Tubing Options Tygon standard PharMed Application: For standard applications Features: - Non-toxic, non-oxidizing - Good resistance to acids, bases and inorganic media - Very low gas permeability, good performance life Material: Thermoplastic soft PVC, transparent Temperature range: -50 to +75 C Complies with the standards: FDA (21 CFR ) and GLP Sterilization: Can be autoclaved for 30 min at 1 bar and 120 C (material may change color) or with ethylene oxide Restriction: Segregation of plasticizers is possible Use with: Acids: Lyes: Solvents: Pressure: Vacuum: Viscous media: Sterile media: good good unsuitable good good excellent conditional Application: Ideal for medical, lab and research uses Features: - High fatigue strength under repeated reversed bending stresses - Non-toxic, biocompatible - Very low gas permeability - Well suited to acids and bases Material: Thermoplastic elastomer on a polypropylene base with plasticizers; excellent tensile strength; opaque GLP, Pharmacopoea and Europaea Temperature range: -40 to +75 C sterilized by irradiation Restriction: Additives may migrate Complies with the standards: FDA (21 CFR ), USP Class VI, Sterilization: Can be autoclaved or sterilized with ethylene oxide or Use with: Acids: Lyes: Solvents: Pressure: Vacuum: Viscous media: Sterile media: good good unsuitable good excellent good excellent Tygon 2001 for food Silicone Use with: Acids: Lyes: Solvents: Pressure: Vacuum: Viscous media: Sterile media: excellent excellent good good good good good Application: Food industry, well suited to products with high fat content Features: - Extremely chemical-resistant; e. g. appropriate for the use of polar solvents - Plasticizer and oil-free - Superior flex life in peristaltic pumps - Translucent to ease visual inspection - Outstanding flexibility Material: Thermoplastic tube, transparent and GLP Temperature range: -78 to +71 C or with ethylene oxide Complies with the standards: USP Class VI, FDA (21 CFR ) Sterilization: Can be autoclaved for 30 min at 1 bar, sterilized by irradiation Restriction: Not suitable for pump drive Hei-Flow Value 06 Use with: Acids: Lyes: Solvents: Pressure: Vacuum: Viscous media: Sterile media: conditional conditional unsuitable satisfactory good satisfactory excellent Application: Platinum-coated silicone hose for use in pharmaceuticals and biology Features: - Extremely smooth interior prevents bacterial growth - Biocompatible, minimal adsorption and absorption - Best flow properties, high temperature stability - Absolutely inert, softener-free Material: Polydimethylsiloxane with siliceous earth and silicone additives; translucent white; excellent resistance to initial pressure Complies with the standards: USP Class VI, FDA, meets GLP and NSF Temperature range: -80 to +200 C Sterilization: Can be autoclaved for 30 min at 1 bar or sterilized by irradiation Restriction: Not suitable for concentrated solvents, oils, acids or dilute caustic soda; relatively high permeability to gas Tygon for hydrocarbons Viton Application: Especially for hydrocarbons, mineral oil products and distillates Features: - Ideal for petrol, kerosene, heating oil, cutting solutions and coolants on a glycol base - Resistant to ozone and UV Material: Thermoplastic soft PVC, translucent yellow Complies with the standards: GLP conform Temperature range: -40 to +75 C Sterilization: Sterilization is not recommended Restriction: Not suitable for concentrated acids, lyes, food and pharmaceutics Use with: Acids: Lyes: Solvents: Pressure: Vacuum: Viscous media: Sterile media: good good conditional good good excellent conditional Application: Excellent acid resistance at high temperatures Features: - Low gas permeability - Resistant to solvents and corrosives at high temperatures Material: Fluorocarbon rubber, thermoformed Viton B (67% fluorinated); opaque black Complies with the standards: GLP conform Temperature range: -30 to +205 C Sterilization: 16 hours at +250 C with hot air circulation recommended Restriction: Limited performance life Use with: Acids: Lyes: Solvents: Pressure: Vacuum: Viscous media: Sterile media: excellent excellent varies; tests recommended good good good satisfactory

69 Tubing Compatibility Chemical P S T TU TK V Chemical P S T TU TK V Chemical P S T TU TK V Chemical P S T TU TK V A Acetaldehyde D C D D D D C Calcium oxide A A A A A - H/J Hydrobromic acid, % D D A A A A Potassium hydroxide, <10 % in W. A A A D - B Acetic acid, 10 % in W. A A A A A - Carbon bisulfide D D D D D - Hydrochloric acid, 10 % in W. A D A A A A Potassium iodide, 56 % in W. A A A A A - Acetic acid, 100 % B D D D - - Carbon tetrachloride D D D D D A Hydrochloric acid, 37 % in W. B D A D A B Propanol (propyl alcohol) C A D D A B Acetic anhydride A A D D A D Chlorine, wet D D B B C B Hydrocyanic acid A A A A A A Pyridine C D D D C D Acetone D C D D C D Chloracetic acid, 20 % in W. B A A D A D Hydrofluoric acid, 10 % in W. D D C A A B Q/S Silicone oils C D B A B A Acetonitrile C D D D B D Chlorobenzene D D D D C A Hydrofluoric acid, 50 % D D D D A A Silver nitrate, 55 % in W. A A A A A A Acetyl bromide C D D D C - Chloroform D D D D C A Hydrogen peroxide, 10 % in W. A A A A A A Soap solutions B A A A A A Acetyl chloride C D D D C A Chlorobromomethane B D D D - A Hydrogen peroxide, 90 % in W. B C D D B - Sodium bicarbonate, 7 % in W. A A A A A A Aliphatic hydrocarbons D D D B D - Chromic acid, 20 % in W. A D B C B A Hydroiodic acid B B A A A - Sodium bisulfate A - A A A - Aluminum chloride, 53 % in W. A A A A A A Chromic acid, 50 % in W. C D C D - - Hypochlorous acid, 25 % in W A A A A A A Sodium borate A A A A A A Aluminum sulfate, 50 % in W. A A A A A A Copper salts A A A A A - Iodine solutions A C A A A - Sodium carbonate A A A A A B Alums A A A A A - Cyclohexane D D D C D A K/L Ketones D D D D C - Sodium ferrocyanide A A A D - - Ammonia, gas and liquid A D B B B D Cyclohexanone D D D D C D Lactic acid, 10 % in W. A A A A A - Sodium hydrosulfite A - A A A - Ammonium acetate, 45 % in W. A A A A A - Chlorosulfonic acid D D D D D D Lactic acid, 85 % in W. B D D D - - Sodium hydroxide, % in W. A A A D A B Ammonium carbonate, 20 % in W. A A A A A A D Diesel D D D B - - Lead acetate, 35 % in W. A A A A A - Sodium hydroxide, % in W. A C C D A B Ammonium chloride A C A A A A Dimethyl formamide B B D D A D M Manganese salts A A A A A - Sodium nitrate, 3.5 % in W. A A A A A - Ammonium hydroxide, 30 % in W. A D A C A B E Ethanol (ethyl alcohol) A B D B A A Magnesium chloride, 35 % in W. A A A A A A Sodium sulfate, 3.6 % in W. A A A A - A Ammonium nitrate A C A A A - Ether C D D C D - Magnesium sulfate, 25 % in W. A A A A A - Sodium sulfide, 13 % in W. A A A A A - Ammonium phosphate A A A A A - Ethyl acetate B D D D D D Mercury salts A A A A A - Stearic acid, 5 % in Alc. C D D B B - Ammonium sulfate B A A A A D Ethyl bromide D D D D C - Methane A - A A A A Sulfuric acid, 10 % in W. A A A B A A Amyl acetate B D D D D A Ethyl chloride C D D D D A Methanol A B D B A D Sulfuric acid, 30 % in W. A B A B A A Amyl alcohol D D D A A A Ethylamine D C D D B - Methyl Ethyl Ketone D D D D C D Sulfuric acid, % in W. D D D D C A Amyl chloride C D D D D - Ethylene chlorhydrin A B D B A A Monoethanolamine C D D D D D Sulfurous acid A A A A A A Aniline C D D D D D Ethylene dichloride C D D D D B N Naphtha D D D D D A T Tannic acid, 75 % in W. B A B D A - Aniline hydrochloride C D D D D B Ethylene glycol A A A A A A Nickel salts A A A A A - Tartaric acid, 56 % in W. A A A A A A Aqua regia (80 % HCI, 20 % HNO3) D D D D A - Ethylene oxide A D A A A D Nitric acid, 10 % in W. A C A D A A Tin salts A A A A A - Aromatic hydrocarbons A D D D D - F Fatty acids C B B C C C Nitric acid, 35 % in W. A D A D A A Toluene (toluol) D D D D C A Arsenic salts A A A A A - Ferric chloride 40 % in W. A A A A A B Nitric acid, % in W. D D D D D - Trichloroacetic acid, 90 % in W. B D A D A C B Barium salts A A A A A - Ferric sulfate 5 % in W. A A A A A A Nitrobenzene D D D D C - Trichlorethylene C D D D C A Benzaldehyde D C D D C D Ferrous chloride 43 % in W. A A A A A - Nitrous acid, 10 % in W. A B A C A - Trisodium phosphate A A A A A A Benzene D D D D - - Ferrous sulfate 5 % in W. A A A A A - O Oils, animal C A D A B - Turpentine D D D B A A Benzenesulfonic acid D D D D D A Fluoboric acid, 10 % in W. D D A A A - Oils, mineral D D C A D A Urea, 20 % in W. A A A A A - Boric acid, 4 % in W. A A A A A A Fluoroborate salts A - A A A - Oleic acid C B D B D B Uric acid A A A C A - Bromine D D D D D A Fluosilicic acid C B D B A - P Perchloric acid, 67 % in W. A D C D A A Xylene D D D D C B Butane A A A A B A Formaldehyde, 37 % in W. D C D D C D Perchlorethylene C D D D D A W/Z Zinc chloride, 80 % in W. A A A A A A Butanol (butyl alcohol) D B D A A A Formic acid, 25 % in W. A A A C A D Phenol, 91 % in W. A D D C A - Butyl acetate B D D D D - Freon 11 A A A A - - Phosphoric acid 25 % in W. A D A A A A Butyric acid B D D C D D Fruit juice A A A A A A Phthalic acid, 9 % in Alc. A B D C B - G Gasoline, high-aromatic D D D B D A Gasoline, non-aromatic D D D B D A Potassium carbonate, 55 % in W. A A A A A - Potassium cyanide, 33 % in W. A A A A - - Glycerin A A A A A A Tubing: P = PharMed S = Silicone T = Tygon standard TU = Tygon for hydrocarbons TK = Tygon 2001 for food V = Viton Resistance: A = excellent B = good C = conditional D = unsuitable - = not tested Please note: - All information provided here is not guaranteed to be correct - Recommended testing of tubing prior to application use

70 Accessories Foot-pedal P/N For start and stop (Hei-FLOW Advantage 01 / Hei-FLOW Advantage 06 and Hei-FLOW Precision 01 / Hei-FLOW Precision 06 only) Adaptor for multi-channel pump heads P/N To connect pump drive to multi-channel pump head Fitting for extension tubes P/N For tubing diameter mm

71 Technical Specifications - Peristaltic Pumps Model Hei-FLOW Value 01 Hei-FLOW Value 06 Hei-FLOW Advantage 01 Hei-FLOW Advantage 06 Hei-FLOW Precision 01 Hei-FLOW Precision 06 P/N (115 V) P/N (115 V) incl. multi-channel adaptor Flow rates single-channel pumps Flow rates multi-channel pumps (ml/min) (ml/min) , , , Certificate Flow rate accuracy * (%) ±5 ±5 ± 3.5 ± 3.5 ±1 ±2 Speed range (rpm) Speed setting scale scale scale scale digital digital Electronic speed control analog analog digital digital digital digital Control accuracy motor (%) ±2 ±2 ± 0.5 ± 0.5 ± 0.5 ± 0.5 Select direction of rotation CW / CCW CW / CCW CW / CCW CW / CCW CW / CCW CW / CCW Motor power (W) Supply power (W) Analog interface for speed 0-10 V / 4-20 ma direction of rotation start/stop for speed 0-10 V / 4-20 ma direction of rotation start/stop for speed 0-10 V / 4-20 ma direction of rotation start/stop Digital interface RS 232 RS 232 for speed 0-10 V / 4-20 ma direction of rotation start/stop To confirm the ability for continuous operation of the Hei-FLOW series Peristaltic Pumps Flow rate indicator digital digital Volume dosing (ml) , ,999 Interval dosing (ml) ,999 in breaks 0.1 sec 750 h Smooth start yes yes Electronic brake yes yes Foot-pedal connection yes yes yes yes Continuous operation (hours/days) 24/7 24/7 24/7 24/7 24/7 24/7 Safety feature overheat protection overheat protection electronic current limiter and overheat protection electronic current limiter and overheat protection electronic current limiter and overheat protection Weight (kg) Protection class (DIN EN 60529) IP 55 IP 55 IP 55 IP 55 IP 55 IP 55 Permissible ambient conditions 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel C at 80 % rel C decreasing linearly up to max. 50 % rel ,999 in breaks 0.1 sec 750 h electronic current limiter and overheat protection 5 31 C at 80 % rel C decreasing linearly up to max. 50 % rel. The Hei-FLOW series Peristaltic Pumps feature overtemperature safety circuits according to DIN EN :2001 and DIN EN :2015 and therefore is designed for continuous operation. This statement is made under the precondition that all units are operated in accordance with the operation manual and in accordance with good practice standards for safety in laboratories, rules for accident preventions, and compliance with directions on hazardous materials. Dimensions (w x d x h) (mm) 166 x 256 x x 256 x x 256 x x 256 x x 256 x x 256 x 225 * Flow-rate accuracy pertains to water without counter pressure Standard supply voltage: 115 V - other voltages upon request, please specify for order Schwabach, January 2017 Stefan Peters Research and Development Manager Marcell Sarré Quality Manager

72 Hei-Lab App AFTER-SALES SERVICE Research made easy! IQ-OQ Documentation & Certification IQ-OQ Certification for Rotary Evaporators IQ-OQ Documentation for Hei-VAP models P/N IQ-OQ Execution for Hei-VAP models P/N IQ-OQ Certification for Large-Scale Rotary Evaporators IQ-OQ Documentation for Hei-VAP Industrial models P/N IQ-OQ Execution for Hei-VAP Industrial models P/N IQ-OQ Certification for Automatic Module Distimatic IQ-OQ Documentation for Distimatic P/N IQ-OQ Execution for Distimatic P/N Boiling point calculator for 39 solvents Molar mass calculator and much more Get the Hei-Lab App for free at

73 Summary Benchtop Sterilizers 146 Economical Analog Sterilizers "M" 147 Automated Electronic Sterilizers "E" 147 Vertical Autoclaves "ELV" 150 Service HSG Pre & Post Vacuum Autoclave 153 Large Capacity Autoclaves 154 PUREWISE Water Distillers 157 Clean & Simple Ultrasonic Baths 158 Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

74 Heidolph Tuttnauer sterilizers for all your applications Safe benchtop steam sterilization Greater awareness of potential hazards. Ever more stringent regulations. Increasing emphasis on green facilities and processes. Now more than ever, it s critical to decontaminate your laboratory's equipment, materials and bio hazardous waste. That s what the Tuttnauer Company is all about. For more than 80 years, Tuttnauer has been designing and manufacturing a wide range of laboratory sterilization equipment to safe guard you and your lab. Tuttnauer s benchtop sterilizers provide a fast, safe, dependable and convenient means of sterilizing liquids, media, instruments, glassware, clothing and waste. The line includes a wide range of models from our economic manually controlled analog models to our electronically controlled models with a built-in printer for GLP-compliant documentation. Standard Operating Features Self-contained design eliminates external plumbing and hardwiring for easy installation Simple Operation ASME- stamped, 316 L stainless steel chamber ensures long-lasting reliability, durability and high corrosion resistance Fast/slow exhaust; fast exhaust allows quick cycle time of solids and slow exhaust prevents media and liquid boil-over Closed-door drying system maintains sterility Drying cycle removes residual moisture after sterilization Continuous pressure purge eliminates air pockets and ensures thorough, even sterilization Large-capacity reservoir provides an ample water supply to avoid frequent fill-ups; the water drain in conveniently located on top to allow for quick and easy cleaning of the reservoir Automatic shut-off feature saves energy One-year warranty Pre-Programed Cycles (E Models ONLY) Sterilization Programs Temperature Sterilization time Slow exhaust Dry time Unwrapped instruments 121 C (250 F) 15 minutes n/a none Standard Safety features Heat-insulated, double-locking door protects against accidental burns; the door cannot be opened while the chamber is under pressure Automatic low water level shut-off prevents damage to the heater elements if there is insufficient water for the sterilization cycle Over-temperature cut-off and over-pressure valve ensure safe operation UL- and CSA-approved Wrapped instruments and porous loads Liquids Dry ONLY 121 C (250 F) 15 minutes n/a Models EA- 30 min Models E/EK- 60 min 121 C (250 F) 30 minutes 15 to 20 minutes Not Allowed Alternative for when the dry time in the wrapped or unwrapped cycle is insufficient These economical, manually operated models feature analog controls and gauges for simple operation. If you re tight on space, the new compact Model 1730M is the perfect choice for your basic sterilization needs. Product features 60-minute cycle timer Temperature selection from 100 C to 134 C (212 F to 273 F) Combination pressure and temperature gauge with peak indicator Ordering Information P/N Every stage of the cycle, including water-fill, heating, sterilization, exhaust and drying, are microprocessor-controlled and completely automatic with these electronic models. The digital display continuously show you temperature, pressure and running time. Four fully adjustable, single-button programs make these sterilizers easy to use and ensure reproducible runs. The hand battery backup ensures that all parameter setting and controls are retained in the event of a power failure. Product features Sterilization time to 59 minutes Description Analog M models Model 1730M Model 1730M Model 2340M Model 2340M Model 2540M Model 2540M Model 3545M Model 3850M Model 3870M Temperature selection from 105 C to 137 C (221 F to 279 F) In-line particle filter to protect valves Electronic pressure and temperature sensors Low-water alarm- sounds when reservoir needs to be refilled Standby heating- keeps chamber warm for quicker cycles Ordering Information P/N Economical Analog Sterilizers M Description Electronic E models Model 2340E Model 2340E Model 2340EA Model 2540E Model 2540E Model 2540EA Model 3545E Model 3850E Model 3870E Model 3870EA Number of Stainless Steel Trays Number of Stainless Steel Trays Chamber Diameter 7- in 7- in 9- in 9- in 10- in 10- in in 15- in 15- in Automated Electronic Sterilizers E Chamber Diameter 9- in 9- in 9- in 10- in 10- in 10- in in 15-in 15-in 15-in Voltage 120V 220V 120V 220V 120V 220V 220V 220V 220V Voltage 120V 220V 120V 120V 220V 120V 220V 220V 220V 220V Includes Stand yes yes Includes Stand yes yes yes Accessories Printer, for Models 2340E, 2540E, 3850E, and 3870E Package of 5 rolls printer paper, for EP models Stand, for all 3850 and 3870 models 147

75 EP Models EA Models Technical specifications EP Models help you meet GLP documentation requirements. These sterilizers have a built-in printer that provides a printed summary at the end of each cycle, documenting temperature, elapsed drying and sterilization times, selected cycle, cycle number, real time and date, as well as any errors or interruptions that may have occurred during the cycle. Kwiklave Model 2540EAKP The Kwiklave Model 2540EAKP cuts sterilization time in half perfect for fast instrument turnaround. It offers all standard operating and safety features, plus a special quick cycle. Its advanced heating elements reduces the time needed for the autoclave reach optimal sterilization temperature, reducing overall sterilization time by up to 50%. Ordering Information P/N Description Electronic EP models, with printer Model 2340EP 3 Model 2340EP 3 Model 2340EAP 3 Model 2540EP 4 Model 2540EP 4 Environmental Model 2540EPK 4 Model 2540EAP 4 Kwiklave Model 2540EAKP 4 Model 3545EP 2 Model 3850EP 2 Model 3870EP 2 Model 3870EAP 2 Model 5075EP 2 Accessories - Autoclave Ordering Information P/N Description EA Models are ideal for sterilizing wrapped and sealed instruments. These fully automatic autoclaves are specially designed with preloaded cycles for sterilizing packs, pouches, sealed pipette racks, unwrapped instruments and other contained/wrapped materials. The highly efficient air-driven pump circulates hot air after the sterilization cycle to ensure thorough drying of samples and to reduce overall drying time. Environmental Model 2540EPK Environmental Model 2540EPK meets EPA guidelines and is perfect for environmental labs. In addition to standard features, it includes an accelerated cycle time and a built-in printer for sterilization cycle validation Number of Stainless Steel Trays Package of 5 rolls printer paper, for EP models Stand for 5075EP Stand, for all 3850 and 3870 Bench Top Models Chamber BRITE Sterilizer Cleaner Door Gasket f/1730 Models Door Gasket f/2340 Models Door Gasket f/2540 Models Door Gasket f/3545 Models Door Gasket f/3850 & 3870 Models Chamber Diameter 9- in 9- in 9- in 10- in 10- in 10- in 10- in 10- in in 15- in 15- in 15- in 19- in Voltage 120V 220V 120V 120V 220V 220V 120V 220V 220V 220V 220V 220V 230V Includes Stand yes yes yes 1 phase Model Model 1730 Model 2340 Model 2540 Model 3545 Model 3850 Model 3870 Power Supply Current Phase Chamber Volume Gallons Liters 1,050 W 11 A 1 2 7,5 1,400 W 12 A ,400 W 12 A ,200 W 13.6 A 1 7,8 34,4 2,400 W 13.6 A ,400 W 13.6 A Chamber Dimension Inches 7 x 12 9 x x x x x 27 (Dia. x D) Centimeters 17.8 x x x x x x 68.6 Tray Dimensions Inches 4.7 x 11.6 x x 16.3 x x 16.3 x x 16.1 x 1 14 x 20 x 1 14 x 26 x 1 (W x D x H) Centimeters 12 x 29.5 x 2 17 x 41.5 x 2 17 x 41.5 x x 40.8 x x 50 x x 67 x2.5 Overall Dimensions Inches 17 x 16 x x 20 x x 20 x x 21.5 x x 27 x x 34 x 21 (W x D x H) Centimeters 43.2 x 40.6 x x 50.8 x x 50.8 x x 54.6 x x 68.6 x x 86.4 x 53.3 Reservoir volume Gallons 0,8 0,8 0,8 0,8 1,6 1,6 (W x D x H) Liters Minimum Water Gallons 0,21 0,21 0,21 0,21 0,53 0,53 Volume in Reserivoir Liters 0,8 0,8 0,8 0,8 2 2 Net Weight Pounds Kilograms Erlenmeyer 125 ml Flask Size 500 ml 1 L, short neck 2 L, short neck ml Media Bottle Bottom Tray to Top of Chamber Middle Tray Top Middle Tray Top Tray 5 in 3 3/4 in in 5 in - 3 in 8 1/8 in 6 in 3 3/4 in 2 1/2 in 10 1/4 in /8 in 12 in /8 in 12 in /8 in Voltage 120V (5-15R) 120V OR 220V 220V Nema Plug 220V (6-15R) Max. Allowable Wor bar (40 psi) king Pressure (MAWP) Water Pump Fuse Air Pump Fuse 120V 220V 1.25 amps 2.0 amps 1.25 amps Pounds Shipping Weight Kilograms Cubic Feet 25 6, ,4 48 9, , , ,8 Shipping Volume m 3 0,18 0,27 0,27 0,35 0,63 0,

76 Heidolph Tuttnauer Vertical Autoclaves Technical specifications Sterilize larger volumes in less time Three models cover a wide range of applications for laboratories in research institutes, universities, pharmaceutical, food, chemical and biotechnological industries. The advanced laboratory line provides a single solution for the full spectrum of sterilization needs including liquids, culture media, instruments, glassware, plastics, pipette tips, biological waste, contaminated media and other laboratory items. Advanced Control system for Your Laboratory F software control- Protect your liquid media, save time, save energy: And additional challenge with liquid sterilization is the need 0 to prevent liquid media exposure to high temperatures for a ling time, which may harm the quality of the liquid media. The advanced F0 optional feature minimizes the time liquids are exposed to high temperatures during sterilization there by protecting liquid media, saving your lab time and reducing energy consumption PID (Proportional Integral Differential) pressure control Stores the last 200 cycles in built-in memory Up to 6 temperature sensor and 4 pressure sensors can be connected 30 Identification codes and passwords for access level control The controller and software comply with the 21 CFR part 11 standard In/Out test (enables technical to check each system component separately) Sterilization Temperature range 105 C to 137 C Optional Disinfection/Isothermal Temperature Range 60 C to 105 C Optional Independent Recording for cross-checking cycle measurements Filter replacement notifications based on the number of cycles Optional Fast Liquid Cooling- The chamber is surrounded by coils that are filled with cold tap water to help, rapidly cooling down the chamber to safe temperature, reducing the cycle time and protecting the load by minimizing its exposure to high temperatures (5075ELVC Model only) Sterilization Programs Model 2840ELV Mobile 3870ELV Mobile 5075ELVC P/N Chamber Volume 31L 85 L 160 L "Plug & Play" to operate only with an electric power connection. No need to connect autoclave to building utilities for distilled water, tap water and drain. "Plug & Play" to operate only with an electric power connection. No need to connect autoclave to building utilities for distilled water, tap water and drain. Chamber Dimensions (Dia. x Depth) 28 x 46 cm 38 x 70 cm 50 x 75 cm Mobile is not an option and must be connected to building utilities for distilled water, tap water and drain Overall Dimensions (D x W x H) 54 x 98 x 44cm 73 x x 73cm 110 x 86.6 x 71.5 cm 21 x 39 x 17in 29 x 42 x 29in 43 x 34 x 28 in Max Temperature 135C 135C 135C Chamber Material Stainless Steel 316 Ti (1.4571) Stainless Steel 316 Ti (1.4571) Stainless Steel 316 Ti (1.4571) Housing/Door Material Stainless Steel 304 L Stainless Steel 304 L Stainless Steel 304 L Comes Standard with Units Internal Thermometer included included included Sample Temperature Probes set of 2, included set of 2, included set of 2, included Water-sensing Electrode included included included External Pressure Gauge included included included Printer included included included USB included included included Wire Baskets set of 2 (small) set of 2 (large) set of 2 (large) Wheels w/ lock included included n/a Customer must supply Plug Configurations These units do not come with a plug. Nema (L15-20P & R or L14-20R & P) will need to be installed. These units do not come with a plug. Nema (L15-30P & R or L14-30R & P) will need to be installed. Voltage requirements 230V/ Hz, Single Phase 230V/ Hz, 3-phase 230V/ Hz, 3-phase Amps 15A 20A 30A Power requirements 2.2 KW 6.0 KW 9.0 KW Requirements Compressed Air n/a n/a 1/2" 3-4 Bar (44-58 psi) Tap Water n/a n/a 1/2" 3-4 Bar (29-44 psi) Mineral Free Water RO or Distilled RO or Distilled 1/2" 2-3 Bar (29-44 psi) RO or Distilled Drain n/a n/a 2" Min Withstanding temp of 80C (176F) Sterilization Programs Program Description Temperature Sterilization time (minutes) P/N Desciption For use in D x H (in) Solid Baskets, ideal for medical waste sterilizations 1 Glass 2 Plastic 3 Liquid A 4 Liquid B Waste *Can program 7 Custom Cycles 134 C 121 C 121 C 121 C Wire Basket, small Wire Basket, large Wire Basket, large 3870 ELV x ELV x ELV 18.3 x Solid Basket, small Solid Basket, large Solid Basket, large 3870ELV x ELV x ELV 18.6 x Wire Basket, small 5075ELV 18.3 x Solid Basket, small 5075ELV 18.6 x

77 Heidolph Tuttnauer Autoclaves - Services All Heidolph Tuttnauer sterilizers require general maintenance and cleaning. A sterilizer often requires regulatory compliance at some local, or federal standard based on the application within the operation of the unit. Our factory trained technicians are here to help provide basic product upkeep and to help support your sterilizer through a variety of services offered below: Preventative Maintenance (On Site or In House) Maintenance kit Replacement of: Chamber BRITE, safety valve, door bellow, door gasket, air relief valve, safety valve holder Labor 40% off parts and labor for the year of PM First three hours of Non PM labor is included Preventative maintenance agreements come with discount on parts Part Number Desciption HEIDOLPH SUPPORT CENTER Customer Service: Validation (recommended) On-Site Preventative Maintenance On-Site Preventative Maintenance On-Site Preventative Maintenance On-Site Preventative Maintenance On-Site Preventative Maintenance On-Site Preventative Maintenance IQ/OQ Service- All Models All test cycles include (Temperature, Pressure, Saturated Steam Time) operation Accuracy adjustments accurate to 20 C Solonoid Valve are checked for proper Safety features are tested (4 parameters) Extensive Reports, mapped at 6 positions, Warranty is extended an additional year PM can be added with validation service Part Number We respond in 24 hours or less. Guaranteed! Desciption IQ/OQ Documented proof that facilities and equipment have been delivered and installed in accordance with the requirements and safety regulations stipulated in the design qualifications Consists of: - IQ test plan - IQ extensive report - Installation ELV/C On-Site Preventative Maintenance ELV/C On-Site Preventative Maintenance ELV/C On-Site Prevetnative Maintenance EK On-Site Preventative Maintenance ELV Mobile Preventative Maintenance ELV Mobile Preventative Maintenance Tuttnauer Validation Service Online Support: service@heidolph.com Heidolph Tuttnauer 5075HSG Pre & Post Vacuum Autoclave The 5075HSG is a fully featured 160 liter stand-along pre & post vacuum autoclave. A pre vacuum pump removes the air from the chamber. Then a pules of steam is admitted. This process is repeated 1 to 4 times (as selected). With each cycle of vacuum and steampule the air fraction decreases. This allows for complete Air removal and for faster and more efficient steam penetration throughout the entire load. Autoclave Features High volume water-ring vacuum pump for fast and efficient air removal Stand-by heating mode keeps the autoclave warm and ready for use 316L grade stainless steel chamber and door with electro-polish finish Two RTD load probes for liquid cycles Double locking safety device prevents door from opening at high pressure and high temperature Control lock-out switch prevents start a cycle if door is not properly locked Built-in alpha-numeric printer Mounted on wheels for easy mobility and sterilization on demand Installation, Training and Freight Part Number provided on a case by case basis Contact a Heidolph representative to obtain certified drawings ONLY One chamber size available Model Chamber Dimension (Dia x L) (inches) Chamber Volume (Liters) No. of Shelves 2 Shelf Dimensions W x H x L (inches) Electrical Requirements (Control System, Vacuum Pump) Electrical Requirements (20kW Generator) Plant Steam Supply Cold Water Supply Building Drain *Floor Sink Recommended Heat Load to Room (Btu/Hr) Overal Dimensions W x H x L (inches) Autoclave Weight (Lbs) 5075HSG (Includes Built-In Generator) 19.5 x Small: 11.9 x 0.8 x 27.6 Large: 18.6 x 0.8 x Phase, 120V, 20 AMP 3-Phase, 208V, 56 AMP (Draw) or 3-Phase, 480V, 25 AMP (Draw) N/A 3/4 NPT x 65.4 x Model Erlenmeyer Flask Sterilization Programs Program Bottom Shelf ONLY 250ml 36 1 x 50 1 x ml 24 1 x 18 1 x ml 15 1 x ml 8 1 x ml 7 1 x ml 3 1 x 3 Horizontal Schott Duran 250ml 50 1 x 55 1 x 39 Description 1 Unwrapped Instruments 2 Wrapped Instruments 3 Wrapped Pouches 4 Unwrapped delicate instruments 5 Wrapped delicated instruments P/N ml 36 1 x 32 1 x ml 24 1 x ml 13 1 x ml 8 1 x 5 Temp 1340C (2730F) 1340C (2730F) 1340C (2730F) 1210C (2500F) 1210C (2500F) Steilization time (minutes) Test Programs Test Description 1 Leak test n/a min test time 2 B&D test 1340C (2730F) 4 2 Dry time (minutes) n/a

78 NEW! Large Capacity Autoclaves Specifications The Heidolph Tuttnauer offers an unmatched range of models that are available in three series: Compact, Mid Range, and Large Capacity. The sterilizer chambers range in volume from 120 to 1015 liters. Additional, we design customer sizes and offer the end-user an unlimited amount of upgrades to choose from. Each model is available in either single or double door configurations. Compact & 66 Mid Range Series Model A 66B 66C 66D 66E Chamber Dimensions WxHxL (Inches) 16x16x28 20x20x38 24x24x36 24x24x48 26x26x39 26x26x49 26x26x60 Chamber Volume Cubit Feet (Liter) 4 (120) 9 (250) 12 (340) 16 (450) 15 (430) 19 (540) 23 (660) External Dimensions Cabinet Enclosed WxHxL (Inches) Autoclave Weight Empty Chamber Lbs (kg) Single Hinged Door Single Sliding Door Double Hinged Door Double Sliding Door Single Sliding Door Double Sliding Door 28x75x51 31x75x46 45x75x46 47x75x (499) 1250 (567) 28x75x60 33x75x53 49x75x53 53x75x (798) 1910 (866) 43x75x56 40x75x60 58x75x52 60x75x (1340) 3205 (1454) 43x75x68 40x75x72 58x75x64 60x75x (1451) 3450 (1565) 46x75x71 40x78x67 60x75x66 64x78x (1429) 3400 (1542) 46x75x71 40x78x67 60x75x66 64x78x (1520) 3600 (1633) 46x75x81 40x78x77 60x75x77 64x78x (1610) 3800 (1724) Utility Consumptions / Requirements Model A 66B 66C 66D 66E Plant Steam Supply Pipe Size 3/4" NPT 3/4" NPT 1" NPT 1" NPT 1" NPT 1" NPT 1" NPT PSIG Dynamic % Dry Sturated 48 Lbs/Hr 100 Lbs/Hr 160 Lbs/Hr 203 Lbs/Hr 160 Lbs/Hr 203 Lbs/Hr 246 Lbs/Hr Vapor Condensate Flow Rate Peak 17Lbs/ Peak 22Lbs/ Peak 26Lbs/ Peak 29Lbs/ Peak 26Lbs/ Peak 29Lbs/ Peak 32Lbs/ Free Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. 44 and 55 Compact Series 66 Mid Range Series 69 Large Capacity Series Cold Water Supply PSIG Dynamic, F Contact Heidolph for Recommen- Pipe Size Flow Rate (Peak) 3/4" NPT 4 GPM (15L) 3/4" NPT 8 GPM (30L) 1" NPT 12.5 GPM (47L) 1" NPT 14 GPM (53L) 1" NPT 13.5 GPM (51L) 1" NPT 15 GPM (57L) 1" NPT 19 GPM (72L) Small Laboratory Autoclaves with chamber volumes from 120 to 250 liters. The 44 and 55 series are available with following door options: Medium Laboratory Autoclaves with chamber Volumes from 340 to 660 liters. The 66 series is available with the following door options: Large Laboratory Autoclaves with chamber volumes from 510 to 1015 liters The 69 Series is available with the following door options: ded Water Quality Building Drain Pipe Size Compressed Air Requirements Electrical Requirements (Control System) Electircal requirements (Optional Vacuum Pump) 2" ODT 208V 3.1A 120V 5.9A 2" ODT 208V 3.1A 120V 5.9A 2" ODT 2" ODT 2" ODT PSIG Dynamic, 3.5 SCFM. 3/8" NPT 1- Phase, 120V, 50/60 Hz. 20A 208V 208V 208V 7.6A 7.6A 7.6A 480V 480V 480V 4.3A 4.3A 4.3A 2" ODT 208V 7.6A 480V 4.3A 2" ODT 208V 7.6A 480V 4.3A Fully automatic vertical sliding door Manual Hinged Door Fully Automatic vertical sliding door Hinged door with automatic locking Fully automatic horizontal sliding door Hinged door with automatic locking Electrical Requirements (Optional Steam Generator) Contact a Heidolph representative for specific electrical requirements We offer 2 different models We offer 5 different models We offer 7 different models *Dimensions and weights are approximate and for reference only. *The addition of certain options could impact the above stated utilities *Contact a Heidolph representative to obtain certified drawings. *Due to continuing equipment development, specifications are subject to change without notice *Request an Industrial Checklist from your Heidolph Specialist today

79 Specifications PUREWISE Water Distillers Compact & 69 Mid Range Series Model Chamber Dimensions WxHxL (Inches) Chamber Volume Cubit Feet (Liter) Single Hinged Door 69A 24x36x36 18 (510) 53x75x56 External Dimensions Cabinet Enclosed WxHxL (Inches) Autoclave Weight Empty Chamber Lbs (kg) Single Sliding Door Double Hinged Door Double Sliding Door Single Door 75x75x62 58x75x52 75x75x (1560) Double Door 3740 (1696) Utility Consumptions / Requirements Model Plant Steam Supply PSIG Dynamic % Dry Sturated Vapor Condensate Pipe Size Flow Rate 69A 1 1/4" NPT 235 Lbs/Hr Peak 30Lbs/ 69B 24x36x48 24 (680) 53x75x68 75x75x74 58x75x64 75x75x (1710) 4070 (1846) 69B 1 1/4" NPT 300 Lbs/Hr Peak 32Lbs/ 69C 24x36x60 30 (840) 53x75x80 75x75x86 58x75x75 75x75x (1860) 4400 (1996) 69C 1 1/4" NPT 370 Lbs/Hr Peak 34Lbs/ 69D 24x36x72 36 (1015) 53x75x92 75x75x98 58x75x87 75x75x (2041) 4800 (2177) 69D 1 1/4" NPT 435 Lbs/Hr Peak 36Lbs/ 69E 26x37.5x36 20 (575) 55x75x56 79x75x62 60x75x52 79x75x (1651) 4800 (2177) 69E 1 1/4" NPT 245 Lbs/Hr Peak 31Lbs/ 69F 26x37.5x48 27 (760) 55x75x68 79x75x74 60x75x64 79x75x (1801) 4270 (1937) 69F 1 1/4" NPT 310 Lbs/Hr Peak 33Lbs/ 69G 26x37.5x60 34 (950) 55x75x80 79x75x86 60x75x76 79x75x (1950) 4600 (2087) 69G 1 1/4" NPT 380 Lbs/Hr Peak 35Lbs/ Think wise. Think Pure. Think Tuttnauer. PUREWISE water distillers operate by heating water to 212 F (100 C), which kills bacteria, cysts and or viruses that may be present, and converting it to steam. As the steam rises it leaves behind any solids, salts, heavy metals, etc.; low-boiling, light gases are discharged through the gaseous vent. The steam is then cooled in the stainless steel condenser, where it turns back into high quality, pure water. To further enhance water quality, the distilled water passes through a coconut shell carbon filter to extract any volatile organic compounds (VOCs) and is finally deposited in the unit s GE Lexan polycarbonate collection/storage container. Product features Effectively removes most tap water impurities Automatic shut-off after 1-gallon cycle Rust-proof stainless steel condenser Includes collector/storage bottle UL listing: #28KL Water system is 99% free of impurities East-to-remove boiler for manual fill- no water hookup Unique recessed heating base reduces scale buildup Free Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cycle Avg. Cold Water Supply Pipe Size PSIG Dynamic, F Contact Heidolph for Recommended Water Quality Flow Rate (Peak) Building Drain Pipe Size Compressed Air Requirements 1 1/4" NPT 18 GPM (68L) 3" ODT 1 1/4" NPT 20 GPM (76L) 3" ODT 1 1/4" NPT 1 1/4" NPT 1 1/4" NPT 22 GPM 24 GPM 18 GPM (83L) (91L) (68L) 3" ODT 3" ODT 3" ODT PSIG Dynamic, 3.5 SCFM. 3/8" NPT 1 1/4" NPT 20 GPM (76L) 3" ODT 1 1/4" NPT 22 GPM (83L) 3" ODT Additional product features of Model 7000 series Extra-large capacity Benchtop and floor-standing models available Front- or side-mounting spout for easy dispensing and storage Directly connects to tap water supply for continuous operation Electrical Requirements (Control System) Electircal requirements 208V 208V 208V 1- Phase, 120V, 50/60 Hz. 20A 208V 208V 208V 208V Technical specifications (Optional Vacuum Pump) 18A 120V 9.5A 18A 120V 9.5A 18A 120V 9.5A 18A 120V 9.5A 18A 120V 9.5A 18A 120V 9.5A 18A 120V 9.5A Model Distillate capacity 1 gal/3.8l in 4.5h; 3.5 gal/13.3 L in 18h 8 gal/30.4 L in 28 h 12 gal/45.6 L in 30 h Electrical Requirements (Optional Steam Generator) Contact a Heidolph representative for specific electrical requirements Power supply up to 5gal/18.9L in 24h 115V/ 60 Hz 115V/ 60 Hz 115V/ 60 Hz 115V/ 60 Hz Dimensions 9.5 x 15 x 16 in 11 x 17 x 17 in 11 x 36 x 17 in 11 x 42 x 17 in Benefits of Choosing Tuttnauer (W x H x D) Weight 24.1 x 38.1 x 40.6 cm 10lb/ 4.5kg 28 x 43 x 43 cm 30lb/ 13.5kg 28 x 91 x 43 cm 37lb/ 16.5kg 28 x 107 x 43 cm 44lb/ 20kg The control panel is an advanced microprocessor providing significantly greater accuracy than an electro-mechanical control. The control is isolated and covered to protect it from heat and moisture damage. All Piping is corrosion resistant stainless steel and has unions between components to make maintenance much easier. You do not have to dismantle large sections of piping just to replace a single part. A design that will minimize any down time. Control valves are air driven (pneumatic) and last 4-5 times longer than older style electromagnetic valves The chamber and jacket are 100% stainless steel. The jacket is 304 SS and the chamber is 316L SS for superior corrosion resistance and is very stain resistant for easier maintenance/clean up in event of a spill. The chamber is fully insulated to be energy efficient and prevent heat loss and thermal loading of the work area. The Unit must have a full 2 thickness of rigid, chloride free insulation. This is important in a moisture laden environment. The insulation is then completely covered with corrosion resistant stainless steel cladding to prevent damage and degradation of the insulation. Ordering information P/N Description Benchtop water distiller Model Benchtop water distiller Model Floor-standing water distiller Model Floor-standing water distiller Model Carbon filter cartridge, for Model 9000, change after every 6 months of use

80 Clean & Simple Ultrasonic Baths New Clean & Simple ultrasonic baths feature 60kHz of quiet cleaning power, which is less aggressive to instruments, yet strong enough to remove all surface contamination. Systems are available in 1- and 3-gallon sizes for standard glassware and instruments. A full selection of optional accessories are available to meet your specific needs. For added samples processing and cleaning power, choose an H model. Which features a built-in heating unit. Fill your ultrasonic bath water and drop in two cleaning tablets. Watch them dissolve and clean in about a minute. The tablets create a non-ionic cleaning solution that is non-corrosive, nontoxic, non-caustic and biodegradable. Technical Specifications Model CSU 1 CSU 1H CSU 3 CSU 3H Tank dimensions (W x H x D) External dimensions (W x H x D) Tank capacity 9.4 x 4 x 5.4 in 23.8 x 10.2 x 13.7 cm 12.6 x 8.8 x 9.9 in 32 x 22.2 x 25 cm 0.8 gal/ 3.4 L 9.4 x 4 x 5.4 in 23.8 x 10.2 x 13.7 cm 12.6 x 8.8 x 9.9 in 32 x 22.2 x 25 cm 0.8 gal/ 3.4 L 15.5 x 6 x 9 in 39.4 x 15.2 x 22.9 cm 19 x 13.5 x 16 in 49.3 x 34.3 x 40.6 cm 3.0 gal/ 12.7L 15.5 x 6 x 9 in 39.4 x 15.2 x 22.9 cm 19 x 13.5 x 16 in 49.3 x 34.3 x 40.6 cm 3.0 gal/ 12.7L Ultrasonic bath features Cleaning Tablet features Built-in heater ( H models) for added sample processing and cleaning power High efficiency 60 khz of cavitation for thorough and quiet cleaning Durable vinyl-clad steel housing is easy to clean and resist scratching Stainless steel tank with cover included Full line of accessories available Eliminates handling of heavy 1-gallon containers No bulky storage of premixing Enzymatic solution effectively breaks down protein Use a Reax vortexer in conjunction with an ultrasonic bath to help aid in dissolution of samples Ordering Information P/N Description Ultrasonic baths Model CSU 1, includes bath lid/cover Model CSU 1H, with built-in heater, includes bath lid/cover Model CSU 3, includes bath lid/cover Model CSU 3H, with built-in heater, includes bath lid/cover Accessories CSU 1 spare parts kit, includes beaker holder, 2 glass beakers, bands and beaker lids CSU 3 spare parts kit, includes beaker holder, 2 glass beakers, bands and beaker lids CSU 1 sample basket CSU 3 sample basket Carbon filter cartridge, pkg. of Clean & Simple ultrasonic cleansing tablets, box of 144 tablets

81 Free Up Valuable Fume Hood Real-estate Summary Rotary Evaporators Enclosures 162 Industrial Rotary Evaporators Enclosures 163 Technical Specifications 164 Application Worksheet 165 Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership

82 General Advantages AirClean Systems ductless hoods, workstations and enclosures are designed to protect the operator, the process or both from toxic vapors, fumes, gas and particulate. At the heart of all AitClean Systems chemical hoods, workstations and enclosures is a revolutionary gas phase bonded carbon filter. This unique filter, found only in AirClean Systems safety products, eliminates filer dusting and dead zones associated with traditional granular carbon filters. IOur ductless fume hoods are a true green product, using much less energy and natural resourced than traditional exhaust fume hoods. The average traditional total exhaust fume hood consumes three-and-a-half times the energy of the average U.S. household. This is dues to the hood exhausting room air, forcing the HVAC system to continually heat or cool makeup air coming into the laboratory. Ductless fume hoods eliminate this costly cycle- reducing environmental impact through significantly reduced energy use. Rotary Evaporator Enclosure These systems are engineered specifically for enclosing rotary evaporates, chromatography equipment and robotic equipment while providing unrestricted access for operator interaction. Clear polycarbonate shell and horizontal sliding doors provide visibility for monitoring the equipment, while the AirSafe automatic safety controller maintains airflow and monitors filter condition. At only 24 inches deep and 38 wide, this enclosure takes up very little counter space. Industrial Rotary Evaporator Enclosure The industrial enclosure is designed to protect the operator of industrial rotary evaporators from harmful fumes and vapors. The enclosure is designed to be attached to two 4 HVAC ducting collars and used as full enclosure of the industrial evaporator system This allows for precious walk-in hood space to be used for synthetic chemistry, such as jacket reactors, separation funnels or even waste storage, rather than housing the industrial 20L rotary evaporator. Product Features Designed to provide vapor/fume safety to an industrial evaporator when attached to a exhaust system (HVAC) Made of polycarbonate panels with multiple entry panels/ doors to provide complete access to industrial evaporator while containing vapors Allows operator protection while freeing up the use of a walk-in-hood Ductless Enclosure Features Integral base with deep spill lip Quit operation; < 49 db Horizontal sliding access doors for equipment manipulation Safely encloses rotary evaporator, vacuum pump and waste bottle Dust-free bonded carbon filter Application specific construction materials Approved chemical list filter included in unit Connect to HVAC system thru 4 tubing (Total Exhaust Enclosure ONLY) How the rotary evaporator enclosure works When enclosure doors are closed, room air enters the chamber through access slots at A Air moves evenly through the chamber while pulling fumes into the bonded carbon filter at B Clean air is recirculated into the room at C Approved Chemical List Acetone Acetonitrile Acetic Acid Chloroform Diethylether Dimethylformamide Dimethylsulfoxide Ethanol Ethyl Acetate Hexane Isopropyl Alcohol Methanol Methylene Chloride Tetrahydrofuran Toluene Water

83 Technical specifications Application Worksheet P/N Model Description Width Depth Bench Top Rotary Evaporator Ductless Enclosure Bench Top Rotary Evaporator Total Exhaust Enclosure Industrial Rotary Evaporator Enclosure A P P L I C A T I O N W O R K S H E E T - D U C T L E S S H O O D External Dimensions Internal Dimensions Airflow characteristics Height Width Depth Height Volume of filtered air Linear face velocity CFM 2-Speed n/a supply dependent Max CFM at full opening 60 FLPM average Ductless Hoods and Enclosures are ideal for a variety of applications, but not for all applications. Please complete the following and fax to , Attention: Filter Specialist. Please provide accurate information so that we can best determine if a ductless hood is appropriate for your application and verify the correct filter(s) needed for your application. T h a n k y o u f o r y o u r t i m e a n d i n t e r e s t i n H e i d o l p h / A i r C l e a n S y s t e m s. 1) Describe the process to be completed inside the hood. (ex. solvent mixing, slide staining, dilutions, robotic, etc) Voltage 110V n/a n/a Electrical Current Base 2.0 Polypropylene n/a Polypropylene n/a Open-No Base 2) List all chemicals to be used inside the ductless fume hood. (this will determine filter longevity) Sides Head Assembly Filter Model Filter Type Polycarbonate ABS (required with unit) Bonded Carbon Polycarbonate ABS n/a n/a Polycarbonate n/a n/a n/a Chemical Name Powder or Liquid? Will the composition change? Concentrati on Amt Volume evaporated in 24 hours Frequency (per day, per week) Heated? Y/N Remaining in hood after process? Capped or uncapped? Operation 2 Speed n/a n/a Construction Noise Level < 55 dba n/a n/a Weight 135 lbs. 105 lbs. 300 lbs. * Please contact Heidolph North America for HVAC requirements **All dimensions provided are in Inches units 3) Will any of the above chemical(s) be heated inside of the hood? If yes, to what temperature and for how long? What are you using to heat the chemicals? 4) Describe laboratory environment that hood is to be placed into. (ex. Acidic, Clean room, etc.) 5) Are you trying to protect the operator or process (cannot be both)? 6) What equipment will be used inside of the hood? Explain. (ex. beakers, microscope, robotic, etc.) 7) How many linear feet of hood space are required for your application? 8) What are the dimensions of the available bench top space? 9) Will this be placed on a bench or do you require a cart/bench? 10) Is Ducted an option? 11) Equipment needed by date: Contact: Phone: Fax: Company (provide address) P h o n e : x F a x : E m a i l : n k v a s n i c k h e i d o l p h. c o m w e b - s i t e : w w w. H e i d o l p h N A. c o m

84 Improve the Productivity Of Your Chemistry Radleys laboratory equipment and scientific glassware have been manufactured in Saffron Walden, UK for over 45 yeas. Their innovative tools for chemistry synthesis, process development, work-up and purification are designed to improve the productivity of today s busy chemist, giving them more time to focus on their research. With over 10,000 systems installed worldwide, Radleys has a proven track record. The true innovation of Radleys products is their simplicity, which not only makes them easy to use-but reduces maintenance-ensure a long and productive life. Contact your local Heidolph sales specialist for a trail of any of our synthesis products. We provide a 1 year Warranty on any of the products offered as well as pre and post sales support. Installation and training are provide upon request. Summary Findenser 168 Heat-On Blocks 169 StarFishTM Multi-Experiment Workstation 171 Coot-It Cooling Bowls 173 Carousel 12 Plus Reaction Station 174 Carousel 6 Plus Reaction Station 177 Tornado Plus Overhead Stirring Station 179 Storm & Breeze Heating/Cooling Station 181 GreenHouse Plus Parallel Synthesizer 182 GreenHouse Blowdown Evaporator 183 Reactor-Ready Lab Reactor 184 Leading Safety Standards Superior Ease of Use Reduced Cost of Ownership Reactor-Ready Duo Lab Reactor 185 Reactor-Ready Pilot Lab Reactor 187 Lara controlled Lab Reactor 188 AVA Software

85 NEW! Findenser- Air Condenser The Greener Alternative to Water Condensers Heat-On Blocks Radleys Heat-On blocks are ideal for heating and stirring one or two 10ml to 5L round-bottom flasks. With collaboration of a leading pharmaceutical company, Radleys has created the Findenser. The super air Findenser comprises of an internal vigreux condenser and an external, finned aluminum jacket between which a small amount of water is permanently sealed. Not only does the Findenser provide excellent heat transfer but is also removes the need for water cooling. This system can be used for 95% percent of all common chemistry applications., replacing the need for water cooled condensers. Product Benefits No risk of flooding from running water Eliminate water purchase and disposal costs For Solvent volumes from 5ml up to 1 liter Helps meet sustainable water reduction targets Ordering Information P/N Description Findenser B24 Cone, B24 Socket Findenser B29 Cone, B24 Socket Findenser B19 Cone, B19 Socket Findenser Mini B24 cone, B24 Socket Findenser Mini B19 Cone, B19 Socket Findenser Mini B14 Cone, B14 Socket *Rod & Clamp Kits are available. Contact your local Heidolph North America Specialist for more information How the Findenser Works The Findenser comprises of an internal glass condenser and an external, finned aluminum jacket, between which a small amount of water is permanently sealed The glass condenser is designed to have a greater internal surface area than traditional condensers, giving it increased heat transfer capacity The finned jacket fits around the glass condenser further increasing the external surface area The result is a super air condenser that preforms as well as a traditional water condenser Technical Specifications P/N Description Solvent Volumes 1 L 250 ml Length x Diameter 400mm x 72mm 275mm x 72mm Joints B14, B19, B24 & B29 Weight 1200g 670g Inner or wetted parts Borosilicate glass Finned jacket Anodised aluminium Plug & Seal Acetal & HT Silicone Thermofluid Water Max Solvent pbt 155 C Oven drying Mac Temp 60 C Dishwasher Max Temp 50 C Autoclaving Do Not Autoclave Operating temp rang 0 C to 60 C Say goodbye to oil baths and heating mantles! Heat-On allows you quick and safe personal heating and stirring of your round-bottom flasks, without the risk of fire or personal injury- and let s not forget the messy clean-up associated with using oil. These fluoropolymer coated, chemically resistant blocks fit on all common hotplates up to 145mm in diameter. Their design ensures even heating without the worry of cracked or breaking glass. Flask and tube inserts are available to accommodate a wide variety of sample sizes- and if you need to transport your sample(s) immediately after operation, the optional lifting handles allow you to do so, safely and easily. Not all block designs are the same Test results show that Heat-On heats up to 66% faster and uses 30% less energy than other leading brands of blocks. mple(s) immediately after operation, the optional lifting handles allow you to do so, safely and easily. Heat-On Replace messy oil baths and heating mantles; avoid spills and make your chemistry safer, cleaner and faster Ordering Information Product Features P/N Fluoropolymer-Coated Anodized System Multi-Well Multi-Well Multi-Well Multi-Well Block Block Basic Block Block Basic P/N System Includes: Heat-On Multi-Well Holder Heat-On 25ml insert Heat-On 50ml insert Heat-On 100ml insert Heat-On adaptor plate for 135mm hotplates No oil baths or heating mantles required- safer operation with less clean-up Can be used with all common hotplates up to 145mm in diameter; adaptor for 135mm hotplates included in Heat- On system packages Heats up to 200 C, and even up to 260 C for short periods Solid aluminum for fast and even heat transfer from the hotplate into the sample Lightweight and deep well design for increased surface contact contribute to fast heat transfer with added safetyno sticking or broken flasks to worry about! Fluoropolymer coating for superior chemical resistance; optional anodized coating also available Two prove holes allow use with separate temperature probe Multi-Well flask inserts available for 10ml, 25ml, 100ml and 150ml flasks Multi-tube inserts available for 16mm, 20mm and 24mm tubes and vials Lifting handles available for the safe and easy transport of hot blocks immediately after operation

86 Ordering Information P/N Description P/N Description Fluoropolymer-Coated Anodized Heat-On Multi-Well holder Heat-On Multi-Well holder Heat-On 10ml Insert Heat-On 10ml Insert Heat-On 25ml Insert Heat-On 25ml Insert Heat-On 50ml Insert Heat-On 50ml Insert Heat-On 100ml Insert Heat-On 100ml Insert Heat-On 150ml Insert Heat-On 150ml Insert Heat-On 200ml pear-shaped block Heat-On 200ml pear-shaped block Heat-On 250ml Block Heat-On 250ml Block Heat-On 300ml Peat-Shaped Block Heat-On 300ml Peat-Shaped Block Heat-On 500ml Block Heat-On 500ml Block Heat-On 1L Block Heat-On 1L Block Heat-On 2L Block Heat-On 2L Block Heat-On 3L Block Heat-On 3L Block Heat-On 4L Block Heat-On 5L Block Heat-On 5L Block Heat-On insert, for 8 x 16mm tubes Heat-On insert, for 8 x 16mm tubes Heat-On insert, for 4 x 20mm tubes Heat-On insert, for 4 x 20mm tubes Heat-On insert, for 4 x 24mm tubes Heat-On insert, for 4 x 24mm tubes Accessories P/N Description Heat-On safety lifting handles Heat-On adaptor plate, for 135mm hotplates StarFish Multi-Experiment Workstation The StarFish Multi-Experiment workstation will save you time and reduce clutter on your lab bench by performing multiple experiments at the same time! StarFish is a modular and affordable general-purpose heating and stirring workstation designed to fit on all leading brands of stirring hotplates. It s incredibly easy to use: Simply place the StarFish base plate on to your stirring hotplate, add the MonoBlocks or PolyBlocks best suited for your application, place your samples into the block, and you re ready to go safely and easily. Choose your block design StarFish features exchangeable MonoBlocks and PolyBlocks to accommodate all types of standard glassware from 1-dram vials to 500ml roundbottom flasks. MonoBlocks are single blocks with multiple wells of the same size; they are ideal for experiments that use the same size/type vessel PolyBlocks are pie-shaped segments that you can mix and match (up to five) to accommodate various types/sizes of vessels on the same plate. *Custom blocks are also available, should you have a vessel that is not accommodated by the standard range. Maximize your Heidolph hotplate surface with block accessories Product Features Applications 170 Anodized aluminum for strong chemical resistance and fast heat-up times Interchangeable blocks accommodate all types of tubes and glassware- even flasks- on the same plate Optimized block and plate designs provide the most even heating and stirring- improve results of down stream experiments 5-way and 3-way telescopic clamps come with silicone, Viton or Velcro sealing straps to hold flasks and glass condensers of any size Water and gas/vacuum distribution manifolds distribute cooling water or gas to a maximum of five vessels A wide selection of stirrer options ensures perfect stirring for your particular sample/application Perform simple applications to more complex experiments- easily handles reflux experiments and those requiring inert and vacuum conditions Takes less than 5 minutes to set up Stirring with heating up to 300 C- use any combination of dram or scintillation vial, test tube, beaker, conical and round-bottom flasks up to 500ml Synthesis- us any combination of roundbottom flaks from 5ml-500ml, 1 inch and 24mm test tubes or dram vials Extraction- accommodating any standard round-bottom flask up to 250ml, easily accepts complete glassware assemblies for Soxhlet, liquid-liquid and reflux extraction methods Concentrations- use standard round-bottom flasks, test tubes or dram vials Distillation- easily configure StarFish for all common types of distillation applications, including binary and multicomponent, vacuum regulated, fractional and azeotropic methods Digestion- individual and parallel 171

87 Ordering Information P/N Description StarFish base plates and handles mm, for Radleys mm, for Heidolph Base plate handles, 1 pair MonoBlocks MonoBlock for 40 x 12 mm tubes MonoBlock for 40 x 16 mm tubes MonoBlock for 16 x 24 mm tubes MonoBlock for 16 x 25 mm tubes MonoBlock for 2 ml vials, 40 x 12 mm MonoBlock for 1 dram vials, 40 x 15 mm MonoBlock for 2 dram vials, 40 x 17 mm MonoBlock for 4 dram vials, 20 x 21 mm MonoBlock for 16 x 28 mm vials MonoBlock for 5 x 250 ml flasks MonoBlock for 3 x 500 ml flasks Inserts for MonoBlocks ml Flask Insert ml Flask Insert ml Flask Insert ml Flask Insert ml Flask Insert ml Flask Insert PolyBlocks PolyBlock for 9 x 12 mm tubes PolyBlock for 9 x 16 mm tubes PolyBlock for 3 x 24 mm tubes PolyBlock for 3 x 25 mm tubes PolyBlock for 2 ml vials, 9 x 12 mm PolyBlock for 1 dram vials, 9 x 15 mm PolyBlock for 2 dram vials, 7 x 17 mm PolyBlock for 4 dram vials, 3 x 21 mm PolyBlock for 3 x 28 mm vials PolyBlock for 1 x 250 ml flask StarFish 3- and 5-way clamps Telescopic 3-way clamp, including Velcro Telescopic 3-way clamp, including silicone strap and extended handle Telescopic 5-way clamp, including Velcro Telescopic 5-way clamp, including silicone strap and extended handle Replacement self-adhesive Velcro pads, 10 pcs Replacement Velcro look strips, 200 mm, 5 pcs Silicone strap, 200 mm, 5 pcs Viton strap, 200 mm, 5 pcs StarFish distribution manifolds for gas/vacuum and water Water manifold with connectors Gas/Vacuum manifold with connectors Support rod, 650 mm Split support rod, 650 mm Cool-It Cooling Bowls A new compact, affordable cooling and stirring work station designed to accommodate single round bottom flasks from a 10ml to 2L. Cool-It insulated bowls are designed to proved a round bottom flask from 10ml to 2L with cooling down to -70 C and stirring. Cool-It is designed to fit on a stirring hotplate, for controlled stirring through a magnetic stirring bar in the reaction flask. Cooling is obtains using an appropriate cooling mixture such as dry ice and acetone. Manufactured from a robust HDPE outer with an encapsulated insulating foam core Insulation minimizes condensation on outer surfaces, protecting the hotplate stirrer Unique non-drip pouring spout allows liquid to be easily drained without spilling or splashing solvents Integral handle proved additional support for pouring Lid enhances cooling performance and reduces condensation and ice formation on the flask Robust materials create and almost unbreakable product Optional supporting clamp and stand Ordering Information P/N Description Cool-It Small Bowl + Free Lid Cool-It Large Bowl + Free Lid Adaptor Plate for 135mm Hotplate Choice of two Cool-It bowl sizes Small for flasks to 250ml Large for flasks up to 2L Lid reduces the amount of condensation and frost formation on flasks Prolongs duration and maintains temperature of cooling mixture Reduces the risk of spilling solvents and of spilling very reactive/pyrophoric reagents into cooling mixture

88 Carousel 12 Plus Reaction Station The unique patented Carousel simultaneously heats and cools, stirs and reflux multiple samples under an inert atmosphere. Removable Reflux head allows reaction tubes to be transferred between heated base, cooled base or stand without disconnecting the tubes Chemically resistant PFA caps feature a quick-thread for fast attachment to the glass tubes and easy-on push connections to the stainless steel gas outlets Unique removable PFA insulation plate helps insulate the heated base for faster heating and energy savings of up to 36% Visibility slots allow easier viewing of tube contents during experiments Fluoropolymer coating for chemical resistance and easy cleaning 12 x 1-20 ml samples Central inlet/outlet for vacuum and gas, combined with a radial gas distribution system and gas-tight PFA caps allow reactions under an inert atmosphere Heated directly by the stirring hotplate; Digital temperature control ±0.5 C PFA caps feature a quick-thread for fast attachment to the glass tubes and easy-on push connections to the stainless steel gas outlets Cooled Carousel 12 Plus Reaction Station Offering cost effective low temperature parallel synthesis from ambient down to -78 C Upgrade you Carousel to perform cooled chemistry: The innovative cooled Carousel 12 Plus reservoir is designed to accept the removable reflux/ inerting head from the Carousel 12 Plus; allowing for the reaction tubes to be easily and rapidly transferred between heating and cooling bases. Simultaneously performs up to twelve cooled and stirred reaction to -78 C, with a working volume of 1 ml to 20 ml Fits directly on a standard stirring hotplate Utilizes the single rotating magnetic field of the stirring hotplate to stir all the positions evenly and powerfully Robust HDPE cooling reservoir is compatible with a wide range of cooling mixtures, including dry-ice/acetone for manually controlled cooling from ambient down to -78 C Features a unique non-drip spout and ergonomically designed handle for easy disposal of waste solvents Insulate foam core maintains low temperatures for long periods, while protecting the stirrer from freezing. Also reduces condensation and ice formation on outer surfaces HDPE lid keeps your reaction cooler for longer, minimizes condensation and ice formation on your tubes (maintaining visibility of the contents) and prevents spitting from the cooling mixture The robust HDPE reservoir is virtually unbreakable Water cooled aluminium reflux head provides efficient refluxing within individual reaction tubes Fluoropolymer coating for heightened chemical resistance and easy cleaning Provides 12 heated and stirred glass reaction positions, with a reaction volume of 5 to 20 ml (1 ml with the reduced volume tubes) Quick release water coupling with cut-off valve for ease of connection or removal of cooling water supply to reflux head Visibility slots allow easier viewing of tube contents. Easy to rotate round design gives access to all tubes with no need to lean into the fume cupboard Base design improves heat transfer and provides energy savings. Maximum operating temperature 180 C (220 C for short periods) Unique removable PFA insulation plate helps insulate the heated base for faster heating and energy savings of up to 36 % Rare earth cross shaped stirring bars for more vigorous stirring and a deeper vortex, without jamming Cooled Carousel 12 Plus Reservoir P/N Carousel Stirring Hotplate offers higher temperature, more powerful stirring and digital control Utilises the single rotating magnetic field of the hotplate stirrer to stir all the positions evenly and powerfully Fits on a standard hotplate stirrer so utilizing existing and readily available technology. Compact size has small bench-top footprint0 easy to store Carousel Stand is ideal for use between reactions, when changing tubes and for reactions that require rapid air cooling Viewing slots allow easier viewing of tube contents. Easy to rotate round design gives access to all tubes with no need to lean into the fume cupboard

89 Carousel 12 Plus Systems Everything you need in convenient easy to order systems Ordering Information P/N Description Qty Carousel 12 Plus- Basic System 1 **PN Includes the below Carousel 12 Plus Reaction Station Quick-Thread Glass Reaction Tube, pk Quick-Thread Glass Reaction Tube, pk Easy-On Fluoropolymer Cap, pk Octagonal Stirring Bar 13 mm, pk Cross Shape Stirring Bar 16.5 mm RE, pk PTFE Magnetic Stirring Bar Retriever 350 mm PTFE Magnetic Stirring Bar Evaluation Kit, pk Silicone Seals for All Caps, pk Zinc Plated Wire Rack for 36 x 24 mm Tubes Carousel 12 Plus- Standard System 2 (with stand, stirring hotplate and temp. controller) **PN Includes the below Carousel 12 Plus Reaction Station Quick-Thread Glass Reaction Tube, pk Quick-Thread Glass Reaction Tube, pk Easy-On Fluoropolymer Cap, pk Octagonal Stirring Bar 13 mm, pk Cross Shape Stirring Bar 16.5 mm RE, pk PTFE Magnetic Stirring Bar Retriever 350 mm PTFE Magnetic Stirring Bar Evaluation Kit, pk Silicone Seals for All Caps, pk Zinc Plated Wire Rack for 36 x 24 mm Tubes Carousel 12 Plus Stand Carousel Stirring Hotplate 115V US Plug Carousel Temperature Controller Carousel 12 Plus- Complete System 3 (heated and cooled system) **PN Includes the below Carousel 12 Plus Reaction Station Quick-Thread Glass Reaction Tube, pk Quick-Thread Glass Reaction Tube, pk Easy-On Fluoropolymer Cap, pk Octagonal Stirring Bar 13 mm, pk Cross Shape Stirring Bar 16.5 mm RE, pk PTFE Magnetic Stirring Bar Retriever 350 mm PTFE Magnetic Stirring Bar Evaluation Kit, pk Silicone Seals for All Caps, pk Zinc Plated Wire Rack for 36 x 24 mm Tubes Carousel 12 Plus Stand Carousel Stirring Hotplate 115V US Plug Carousel Temperature Controller Carousel 12 Plus Cooling Reservoir & Lid Digital Thermometer (-250 C to +400 C) & 200 mm Probe Dry Ice Scoop 1 Carousel 6 Plus Reaction Station The Carousel 6 Plus Reaction Station simultaneously heats and stirs up to 6 x 5 ml, 10 ml, 25 ml, 50 ml, 100 ml, 170 ml or 250 ml round-bottom flaks. Flexibility is inherent in its design: choose any combination of flask sizes, with different sidearm combinations and accessories. The Carousel itself fits on a standard hotplate stirrer, and it is compatible with standard rotary and most centrifugal evaporators. With an operating temperature range from ambient to 180 C, a water cooled aluminum reflux head can also provide efficient refluxing with in individual glass reflux necks; combine a radial gas distribution system with gas tight PTFE caps, and you can perform air-sensitive reactions under inert atmospheric conditions. Product Features Solid aluminum base for rapid and even heating of all flasks Fuzzy logic temperature controller is accurate to ±0.5 C Uses the single-rotating magnetic field of the hotplate stirrer to stir all 6 round-bottom flasks evenly and powerfully PTFE guard-ring protects against accidental contact with hot base Removable aluminum inserts in the flux head allow easy removal of flasks and maintain good heat transfer for cooling -Built-in spring clip keeps flasks in position once inserts are removed Acetal quick-release valve coupling allow you to disconnect the reflux head without losing any of the cooling water Cooled Carousel 6 Plus Reaction Station Simultaneously stir and cool reactions from ambient down to -70 C using up to six round-bottom flasks in 5 ml, 10 ml, 25 ml, 50 ml, 100 ml, 170 ml or 250 ml sizes. As with all Radleys Carousel stations, you can use any combination of these flask sizes in the Cooled Carousel, which fits on a standard hotplate stirrer. Product Features Carousel design and technology provides even cooling and the most efficient stirring for your samples HDPE cooling reservoir is compatible with a wide range of freezing mixtures, including dry ice/acetone Insulated foam core maintains low temperatures for long periods, reducing condensation and ice formation on outer surfaces, while it protects the stirrer from freezing Stainless steel central inlet/outlet for vacuum and inert gas, radial gas distribution system and gas-tight PTFE caps for reactions under inert atmosphere Carousel protective cover reduces frost formation, maintains temperature of cooling mixture and reduces risk of solvent spitting **Let us customize your own system based on your needs 250ml Baffled Wide Neck Flask B24/29 Sidearm + Septa Port ( ) 250ml Azeotropic Reaction Flask ( ) 250ml Long Neck Reaction Flask ( ) 250ml Reaction Flask + Reflux Tube + Connecting set ( ) 1000ml Wide Neck Flask B14/23 Sidearm + Septa Port ( ) 100ml Reaction Flask ( ) 250ml Flask with Sidearm ( ) 170ml Reaction Flask ( )

90 Technical specification: Carousel 6 Reaction Stations Heated Cooled P/N Reaction Positions 6 6 Flask sizes (round-bottom) ml 5, 10, 25, 50, 100, 170, 250 5, 10, 25, 50, 100, 170, 250 Stirring speed 0 rpm to 1,110 rpm 0 rpm to 1,110 rpm Temperature range Ambient to 180 C Ambient down to -70 C Temperture accuracy 1 C to -0.5 C NA Inert gas Yes Yes Reflux Yes No Diameter 11.4 in/290 mm 15.3 in/390 mm Height (with reflux) 9 in/230 mm 10.6 in/270 mm Weight 16.7 lb/7.6 kg 2.2 lb/ 3.7 kg Ordering Information Heated Stations 180 C Cooled Stations -78 C P/N Description System 33 System 34 System 35 System 36 System 38 System Carousel 6 Plus Reaction Station x x x x Easy-On PTFE Cap x x x x x Carousel Tech Stirring Hotplate 115V US Plug x x x x Carousel Temperature Controller x x x Tornado Plus Overhead Stirring Station The Tornado is a modular add-on for the Carousel 6 Plus Reaction Station, replacing the magnetic stirring of the stirring hotplate with direct stirring from a single overhead stirrer. For overhead stirring of viscous samples or for the dispersion of delicate solids in solution nothing matches the power and efficiency of the Tornado Overhead Stirring Station. Compatible with all leading brands of overhead stirrers, it evenly distributes high-torque stirring to all flask- from 100 ml to 250 ml- in the Carousel 6 plus reaction Stations. At its most powerful, the Tornado can stir reaction mixtures of up to 10,000 cps at 500 rpm. It can also gently and efficiently disperse delicate solids or resins in low-viscosity solutions. A pinch-grip mechanism enables fast and easy removal/ exchange of the PTFE stirrer shafts, and its unique stirrer sealing system permits usage under an inert atmosphere. A range of PTFE stirrer shafts have been designed for the Tornado. The centrifugal stirrer shafts will fit into any one of the 100 ml and 250 ml flasks. The anchor and propeller stirrer shafts have been specifically designed to fit in the wide neck flasks. Product Features Integrates with Carousel 6 to provide heated and stirred reactions Rapid heating to 180 C, with water cooled reflux head Perform reactions under an inert atmosphere Accepts 50 ml, 100 ml and 250 ml round bottom flasks Uses a single overhead stirrer- save space and money compared to multiple set-ups Two-speed drive for use with both high- and low-viscosity samples Polycarbonate safety guard and optional clamp/stand for added stability during operation Works with all leading brands of overhead stirrers Easy to operate and set up with minimal training time Silicone Septa for PTFE Caps x x x x x x PTFE Magnetic Stirring Bar Retreiver 350mm x x x x x ml Reaction Flask + Reflux Tube + Connecting Set x x x x x B24/29 Rodaviss Sealing Cap x x x x x Rotary Evaporator Adapters Ordinary B29 Socket to x x x x x B24 Cone ml Reaction Flask x x x 250ml Azeotropic Reaction Flask, pk 3 x Aluminium Insert for 100ml reaction Flask, pk 6 x Reaction Flask Support Ring, pk 6 x x x x x Elliptical Stirring Bar 25mm RE, pk 10 x x x x x Tubing for inert Gas or Reflux Cooling 2 meters, 1 pk x x x x x x ml Reaction Flask with B24/29 Sidearm + Septa x x x Port, pk x B24/29 Liquid Additions Dropping Funnel + x x x Pressure Equalising Arm, pk B24/29 Solid Additions Funnel, pk 3 x x x PTFE/Silicone Septa 29mm- B24/29, pk 50 x x Cooled Carousel 6 Plus (Reservoir, Head, x x stand + cover) Protective Cold Temperature Gloves x x Digital Thermometer (-250 C to +400 C) + x x 200mm Probe Dry Ice Scoop x x Cold Temp. Apron 1060mm long Waterproof x x Protective Face Shield x x Technical Specifications Flask sizes (round-bottom) 100 ml and/or 250 ml (with and without sidearms, baffled and wide neck styles) Volume range 20 ml to 150 ml Gear selections 1:1 and 2:1 Stirring speed 0 rpm to 1,000 rpm Maximum viscosity 10,000 cps at 500 rpm Temperature range Ambient up to 180 C Inert gas Yes Reflux Yes Height 23.1 in/587 mm Weight 17.6 lb/8 kg Stirring seal relief pressure 1 bar Tornado fits onto the Carousel 6 Plus with no need for tools

91 Ordering Information Ordering Assistance: Please request a formal quotation. We must verify if you currently have a Carousel or need to start from the beginning. In order to purchase the image on the previous page a series of part number must be ordered, there is no single part number. Item is customized each time. Start With: Carousel 6 Plus Reaction Station Tornado OH Stirrer Station Stand which includes base and support rods Start to customize your system by choosing 1 from each of the following categories: 1) Heidolph magnetic stirring hotplate 2) Choose a temperature controller (based on which hotplate chosen) 3) Additional rod and extension to attach the controller to (varies with type of controller) 4) Reflux Tubes 5) Wide neck flasks To Create a Complete Customized system see above steps 6) Tubing if hooking up to inert gas 7) Silicone seals for PTFE caps 8) Stirrer Shafts (6 required, 1 for each flask) 9) Heidolph overhead stirrer P/N Description Carousel 6 Plus Reaction Station Tornado IS6 Overhead Stirring Station Includes: Drive unit, 6x stirrer guide mechanisms, stirring motor coupling, stirring motor clamp and safety shield Universal support stand Support Rod 500 x 13mm (extra long f/ Tornado) Support Rod f/ hotplate adapter (extension plate) Extra-long sensor probe for Carousel temperature controller (For Heidolph hotplate Hei-Tec & Hei-End only) Magnetic Stirring Hotplates MR Hei-Standard, 115v MR Hei-Tec, 115v MR Hei-End, 115v Stirring Shafts Centrifugal PTFE stirrer shaft, 6 pcs Centrifugal PtFE stirrer shaft Anchor PTFE Stirrer Shaft for 100 ml flask, 6 pcs Anchor PTFE Stirrer Shaft for 100 ml flask Anchor PTFE Stirrer Shaft for 250 ml flasks, 6 pcs Anchor PTFE Stirrer Shaft for 250 ml flasks Propeller PTFE Stirrer shaft, 6 pcs Propeller PTFE Stirrer Shaft Wide Neck Flask with Coupling Wide Neck Reflux Tube + Coupling Coupling for Wide Neck Flasks PTFE Wide Neck Support Collar Nirtrile O-Ring for PTFE Wide Neck Support Collar ml Wide Neck Flask ml Wide Neck Flask ml Wide Neck Flask Wide Neck Flasks with Sidearms ml Wide Neck Flask B14/23 Sidearm + Septa Port ml Wide Neck Flask B14/23 Sidearm + Septa Port ml Wide Neck Flask 2xB14/23 Sidearms + Septa Port ml Wide Neck Flask B24/29 Sidearm + Septa Port ml Wide Neck Flask 2xB24/29 Sidearms + Septa Port Wide Neck Flasks with Baffles + Sidearms ml Baffled Wide Neck Flask B14/23 Sidearm + Septa Port ml Baffled Wide Neck Flask 2xB14/23 Sidearms + Septa Port ml Baffled Wide Neck Flask B24/29 Sidearm + Speta Port ml Baffled Wide Neck Flask 2xB24/29 Sidearms + Septa Port Storm Heating/Cooling Work Station Combined with a suitable heating/cooling circulator the powerful Storm can provide Controlled heating and Cooling for your Carousel 6 and Tornado for -65 C to +200 C. Ideal for steady state reactions over a large temperature range. Add-on module designed to accept the Carousel 6/Tornado combination or single Heat-On blocks Controlled heating and/or cooling of up to six 250 ml samples simultaneously Created with sophisticated computer modeling techniques Storm s internal fluid path has been carefully designed to maximize heat transfer and minimize surface variation. This results in a small Delta-T, thus Storm is ideal for steady stat reaction over a large temperature range Use of circulator to program temperature gradients (max. thermo fluid range -85 C to +235 C) Powerful mechanical overhead stirring can mix even viscous samples Storm including PTFE Cover Plate P/N Breeze Heating/Cooling Work Station The compact Breeze provides rapid controlled heating and cooling from -30 C to +165 C, making it ideal for applications requiring control by solution temperature. Ideal for control by solution temperature. Heating/cooling module designed to accept the Carousel 6/Tornado combination, single Heat-On blocks and other suitable glass or metal vessels directly on to the blocks top plate The Breeze s compact footprint and mass makes it more responsive to changes in thermo fluid temperature and therefore ideal for application that require more accurate solution control Controlled heating and/or cooling of up to six 250ml samples simultaneously using the Carousel 6 and Tornado combination Use a minichiller or circulator to program precise temperature gradients (maximum thermo fluid range -85 C to +235 C) Affordable, lightweight and compact Breeze Workstation and Stand P/N

92 GreenHouse Plus Parallel Synthesizer The patented GreenHouse Plus Parallel synthesizer was designed with the help of scientists at GlaxoSmithKline to perform up to 24 reactions in parallel with the volume range from 0.5 ml to 7 ml per reaction tube. Its removable reaction block hold 24 glass reaction tubes in the same position as a standard 24-well micro plate, enabling the rapid transfer of samples to and from plates with a multichannel pipette or robotic pipetting system. Each tube position is clearly marked on the reflux top, reaction block and reactor base for easy sample identification. The GreenHouse Plus uses V-Mag stirring bar technology that ensures that the PTFE stirring bar in each reaction tube provides uniform and efficient stirring of all samples. Product Features Developed with and tested by chemists at GlaxoSmithKline Lightweight and compact All aluminum parts are nickel=plated for strong chemical resistance, with reflux fingers in solid nickel Removable reaction block features a standard MPT footprint for use with multichannel pipettes and robotic pipetting systems Fits on standard stirring hotplates For up to 24 x 16 mm glass reaction tubes with working volumes from 0.5 ml to 7 ml Heats reactions to 150 C; cools reactions down to -70 C when using the optional cooling reservoir Temperature accuracy within ±0.5 C ensured when using the Carousel digital temperature controller sold separately Cooling reservoir can be filled with acetone/dry ice or other solvent/dry ice combinations; insulated foam core maintains low temperatures for long periods while protecting the stirrer from freezing, also reduces condensation and ice formation on outer surfaces Perform reflux reactions while under an inert atmosphere with the combined reflux and additions head Nickel-plated pressure relief valve vents at 4 psi to 6 psi for added safety Fully compatible with GreenHouse Work-Up System and most centrifugal evaporators, facilitating down-stream applications No moving parts make setup easy and operation virtually maintenance-free! GreenHouse Blowdown Evaporator Turn your existing GreenHouse Parallel Synthesizer (see previous page) into a parallel evaporator, or simply use this system as your own personal benchtop evaporator. The GreenHouse Blowdown uses a precisely controlled flow of inert gas combined with digitally controlled heating to carefully evaporate your samples. Interchangeable plates with either 8 or 24 hollow pins deliver an equal flow of gas to each tube, vial or well. The absence of any vacuum avoids bumping, further protecting your sample during evaporation. Tests show that the greenhouse Blowdown can evaporate 8 vials, each containing 5 ml of methanol in only 22 minutes. Product Features Use as a stand-alone personal evaporator Or upgrade your existing GreenHousel parallel Synthesizer to a Blowdown evaporator system Compatible with GreenHouse reaction tubes, various glass vials, and 8- or 24-well MTP s Ideal for evaporation of HPLC fractions in vials or microplates Environmentally friendly enclosed design contains evaporating solvent, allowing subsequent trapping and collection of solvent via a high-performance glass condenser Easy to operate and set up with minimal training time Technical Specifications Working volume 0.5 ml -7.0 ml Reaction positions 24 (MTP format) Well diameter 16 mm Stirring speed 0 rpm to 1,100 rpm Temperature range Ambient to 150 C Temperature accuracy Better than 0.5 C Time to max. heat-up 30 min Inert gas Yes Reflux Yes Maximum Pressure 3 psi Ordering Information P/N Description System 16 System 17 System 18 System 19 System 20 System Technical Specifications Reaction positions 24 (MTP format) Colume range 0.5 ml to 7 ml Stirring speed 0 rpm to 1,100 rpm Temperature range, cooling Ambient down to -70 C Temperature range, heating Ambient up to 150 C Time to max. heat-up 30 min Temperature stability ±0.5 C Base diameter 6.9 in/176 mm Top diameter 7.5 in/190 mm Well diameter 0.49 in/12.5 mm Height 7 in/180 mm Weight 8.8 lb/4 kg Maximum operating pressure 3 psi Ordering Information P/N Description System 27 System GreenHouse Plus Parallel Synthesizer (includes head, base, glass cylinder and two reaction x x blocks) GreenHouse Plus reaction block GreenHouse Plus reaction tube, 100 pcs x x Pivot ring stirring bar, 15 mm, 40 pcs x x Silicone septum mat, 3 pcs PTFE-faced silicone septum mar, 3 pcs Pre-slit PTFE-faced silicone septum mar, 3 pcs PTFE-faced butyl rubber septum mat, 3 pcs GreenHouse Plus septum mat evaluation kit, x x 4 pcs GreenHouse cooling reservoir x Carousel Tech Stirring Hotplate 115V US Plug x x Carousel Temperature Controller x x Digital Thermometer (-250 C to +400 C) + x 200mm Probe GreenHouse Blowdown head x x x x x x Long Blowdwon pin plate 6 x 4, for GreenHouse tube x x x x x x Blowdown pin plate 6 x 4 x x x x x Blowdown pin plate 4 x 2 x x x GreenHouse Blowdwon base adaptor x x x x x x Blowdown stand-alone base x x Flowmeter with stand, 2 to 27 L/min x x x Gas connection tubing, 5 m x x x Blowdown condenser x x x x x x Gas inlet tee piece, 10 mm Gas inlet barbed connector, 10 mm Blowdown 150ml reservoir x x x x x x GreenHouse glass cylinder x x x x AT01 rack 4 x 2, for 27.8 mm OD vials x x x AT02 rack 6 x 4, for 13 mm OD vials x x x x x AT03 rack 6 x 4 for 13.8 OD vials x x x AT05 rack 4 x 2, for 24.3 mm OD vials x x x AT06 rack 6 x 4, for 15 mm OD vials x x x AT07 rack 4 x 2, for 23.8 mm OD vials Carousel Tech Stirring Hotplate 115V US Plug x x Carousel Temperature Controller x x 183

93 Reactor-Ready Lab Reactor Patented, low cost, multi-volume lab reaction station for glass reaction vessels from 250ml to 5 liters. The Reactor-Ready is designed as a universal reactor work station that can be used for different vessel sizes and different experiments. Reactor-Ready can easily and quickly be configured to suit the chemistry and scale you need for each project. The beauty of Reactor-Ready is that this one reactor work station can replace many, saving you money and fume hood space. Reactor-Ready Duo Lab Reactor Supports two glass reaction vessels of different or similar volume from 100 ml to 5 liters The Reactor-Ready Duo shares the same unique features as the Reactor-Ready, except that it supports two separate jacketed glass reaction vessels. The system can be configured to operate with a single thermo regulator which controls the temperature of both vessels simultaneously; or with two thermo regulators which would control the temperature of each vessel independently. Product Features Quick-release vessel clamp allows rapid vessel exchange Range of single and double jacketed glass vessels including 250 ml, 500 ml, 1 liter, 2 liter and 5 liter Support system accepts all leading brands of overhead stirrer and allows easy, tool free adjustment Triple support stand features heavy duty stainless steel support rods for maximum strength, stability and to minimize vibration Glassware accessories include condensers, dropping funnels etc. Self aligning stirrer coupling engages without the need for tools Quick-release hose coupling allows rapid exchange of vessels Hose manifolds allow easy thermo fluid drain down Temperature rand: -60 C to +190 C (subject to thermo regulator) Thermo fluid Connections: M24 Vacuum to 1 mbar / 5psi How to order a Reactor-Ready 1) Select the Reactor-Ready Core system, Includes: Stand with base, drip tray, support rods, bosses and all clamps Vessel to framework insulated hoses with quick release connections Upper & lower drain-down manifolds PTFE Stirrer guide and coupling Glass reaction vessel lid with Rodaviss sealing caps Vessel FEP O-ring seal and PTFE centering collar 2x Stainless steel vessel support collars 2) Choose a Vessel Kit or Kits you require by selecting the vessel volume & style, Includes: Reaction Vessel PTFE Anchor Stirrer Sidearm Couplings PT200 PTFE Temperature Probe with Lemo Connector PTFE Temperature Probe Adapter Reactor Ready Core System P/N Important: Vessel Kit and Overhead Stirrer sold separately. Hoses to connect the Reactor-Ready framework to your thermo regulator are NOT included. You will require hoses with an M24 x 1.5 female connection or appropriate adapters. Product Features Rapid exchange of both vessels independently, with quick-release vessel clamp and hose couplings Choice of manifold kits allow two vessels to run from a single thermo regulator or two separate thermo regulators System accepts two overhead stirrers which can be operated and moved independently Robust heavy-duty framework features solid stainless steel support rods Two separate quick-release damps support each of the vessels independently Large drip tray will retain vessel contents Manifold & Hose kits much be ordered separately Applications Parallel synthesis or reaction optimization: Use similar or different size vessels and vary stirring speed, stirrer shape and temperature between vessels. Two stage reaction: Transfer reactant from one vessel to the other using vacuum or a pump Single reaction vessel: Using the second vessel as either a receiving or feed vessel (where reagents can be pre-heated or pre-cooled prior to addition) Use optional Control Software to control fluid transfer between vessels How to order a Reactor-Ready Duo 1) Select the Reactor-Ready Core Duo system, Includes: Duo stand with base, drip tray, support rods, bosses and all clamps 2x PTFE Stirrer guides and couplings 2x Glass reaction vessel lids with Rodaviss sealing caps 2x Vessel FEP O-ring seal and PTFE centering collars 2x Stainless steel vessel support collars 2) Choose Manifold & Hose Kit for on or two circulators Reactor-Ready Duo Core P/N Double Circulator Manifold & Hose Kit P/N ) Select the Heidolph Overhead Stirrer you require 4) If you need a thermo regulator, hoses, hose adapters, thermo fluid or accessory glassware, then select from the accessory list 3) Choose the Vessel Kit or Kits you require by selecting the vessel volume & style 4) Select the Heidolph Overhead Stirrer you require 5) If you need automation, add the Control Software and Data Hub 5) If you need a thermo regulator, hoses, hose adapters, thermo fluid or accessory glassware, then select from the accessory list Standard Reaction Vessel Kit 6) If you need automation, add the Control Software and Data Hub Single Circulator Manifold & Hose Kit P/N

94 Reactor-Ready Pilot Lab Reactor Ordering Information P/N Description Core Systems Reactor-Ready Core System Reactor-Ready Duo Core System Manifold & Hose Kits Double Circulator Manifold & Hose Kit, Includes: R/H & L/H Upper Reutrn Manifold with Vent Valve, R/H & L/H Lower Supply Manifold with Drain Valve, 4x Quick-Release Insulated Hoses 60cm, 4x Sealing Caps for Hoses Single Circulator Manifold & Hose Kit, Includes: Central Upper Return Manifold with Vent Valve, Central Lower Supply Manifold with Drain Valve, 4x Quick-Release Insulated Hoses 70cm, 4x Sealing Caps for Hoses, 4x Stainless steel blanking plugs Standard Reaction Vessel Kits, Includes: Glass Reaction Vessel, PTFE anchor stirrer paddle, PTFE Pt 100 Temp Probe (w/lemo plug for connection to the thermoregulator) and PTFE temperautre probe adapter ml Single Jacketed Vessel Kit ml Vacuum Jacketed Vessel kit ml Single Jacketed Vessel Kit ml Vacuum Jacketed Vessel Kit ml Single Jacketed Vessel Kit ml Vacuum Jacketed Vessel Kit ml Single Jacketed Vessel Kit ml Vacuum Jacketed Vessel Kit ml Single Jacketed Vessel Kit ml Vacuum Jacketed Vessel Kit Process Reaction Vessel Kits, Includes: Process vessel, turbine stirrer paddle, PTFE Pt 100 temp probe (w/lemo plug for connection to the thermoregulator) and PTFE Temperature probe adapter ml Single Jacketed Process Vessel Kit ml Vacuum Jacketed Process Vessel Kit ml Single Jacketed Process Vessel Kit ml Vacuum Jacketed Process Vessel Kit ml Single Jacketed Process Vessel Kit ml Vacuum Jacketed Process Vessel Kit ml Single Jacketed Process Vessel Kit ml Vacuum Jacketed Process Vessel Kit ml Single Jacketed Process Vessel Kit ml Vacuum Jacketed Process Vessel Kit ml Single Jacketed Process Vessel Kit ml Vacuum Jacketed Process Vessel Kit *Contact your local Heidolph North America Specialist for more information Save space, time, money and prove your chemistry The Reactor-Ready Pilot is designed as a universal reactor work station that can be used for different vessel sizes and different projects. Reactor-Ready Pilot is ideal for process development, scale-up, pilot and kilo labs. Product Features Rapid vessel exchange with quick-release vessel clamp and wide bore hose couplings. Range of single and vacuum jacketed vessels from 5 liters to 20 liters Dn200vessel flange Accepts all leading brands of overhead stirrer and allows easy, tool free adjustment Compact stainless steel framework accepts all vessel sizes Self aligning stirrer coupling engages without the need for tolls Temperature rang: -60 C to +230 C Innovative hose manifolds allow easy thermo fluid drain down Wide range of accessory glassware including condensers, dropping Vessel manufactures at 1.25 to 1 ratio of internal height to diameter to mimic plant scale reactors How to Order Reactor-Ready Pilot 1) Select the reactor-ready Pilot Core, Includes: Base frame, support rods, vessel clamp, I-beam & stirrer support bosses Vessel to manifold insulated hoses with quick-release connections Lower inlet manifold with drain Upper outlet manifold with vent PTFE Stirrer guide Stainless steel stirrer drive coupling One aluminum vessel support collar FEP flange O-ring and PTFE centering collar 2) Choose the lid you require 3) Choose the Vessel Kit or Kits you require by selecting the vessel volume & style 4) Select the Heidolph Overhead Stirrer you require 5) If you need a thermo regulator, hoses, hose adapters, thermo fluid or accessory glassware, then select from the accessory list 6) If you need automation, add the Control Software and Data Hub Ordering Information P/N Description Core System Reactor-Ready Pilot Core System Glass Lids Neck Lid DN200-1xB19, 1xB24, 1xB29, 2xB34, 1xB Neck Lid DN200-1xB19, 1xB24, 1xB29, 3xB34, 1xB45 Reaction Vessel Kits, Includes: process vessel, turbine stirrer paddle, PTFE Pt100 temp probe with Lemo plug and PTFE Temperature probe adapter L Single Jacketed Pilot Process Vessel Kit L Vacuum Jacketed Pilot Process Vessel kit L Single Jacketed Pilot Process Vessel Kit L Vacuum Jacketed Pilot Process Vessel Kit L Single Jacketed Pilot Process Vessel Kit L Vacuum Jacketed Pilot Process Vessel Kit L Single Jacketed Pilot Process Vessel Kit L Vacuum Jacketed Pilot Process Vessel Kit 187

95 Lara Controlled Lab Reactor AVA Software Setting new standard in flexibility and simplicity in process automation. Not your conventional Reactor Lara allows the user to replace multiple reaction set-ups in several fume hoods with a single automated system; saving money, space, increasing your productivity and making process automation much more accessible. ID Cat No. Description RR20302/US AVA Level 1 Software Kit - US Plug (Kit includes controller, data hub & AVA installed) RR20304/US AVA Level 2 Software Kit - US Plug (Kit includes controller, data hub & AVA installed) RR20306/US AVA Level 3 Software Kit - US Plug (Kit includes controller, data hub & AVA installed) Standard, process & custom vessels from 100ml to 10L Vacuum Jacketed vessel options that are not the norm with conventional reactors Choice of popular stir paddles Hose Couplings: Quick release, connect in seconds, chemical resistant, NO Tools and no fuss Versatile Framework: Compact footprint, built in drip tray Jacked Drain Down: Drain down in seconds with simple push button operation Integral stirrer: simple alignment, hinged action, low profile Patented Stirring Coupling Quick Release Vessel clamp: self centering, quick release and change vessel in minutes as opposed to hours Control Software: log and control the Reactor and your third party devises, such as thermal regulator, peristaltic pump, balances, ph meters, etc. LCD remote control: stirring speed and torque measurement RR20308/US AVA Level 4 Software Kit - US Plug (Kit includes controller, data hub & AVA installed) AVA Software Only RR20111/US AVA Software Level Yr AVA Care RR20112/US AVA Software Level Yr AVA Care RR20113/US AVA Software Level Yr AVA Care RR20114/US AVA Software Level Yr AVA Care AVA Upgrades RR20120/US AVA Software Upgrade Level 1 to 2 + 1Yr AVA Care RR20121/US AVA Software Upgrade Level 1 to 3 + 1Yr AVA Care RR20122/US AVA Software Upgrade Level 1 to 4 + 1Yr AVA Care RR20123/US AVA Software Upgrade Level 2 to 3 + 1Yr AVA Care RR20124/US AVA Software Upgrade Level 2 to 4 + 1Yr AVA Care RR20125/US AVA Software Upgrade Level 3 to 4 + 1Yr AVA Care AVA Care Support RR20141/US AVA Care Level 1-1 Year RR20142/US AVA Care Level 2-1 Year RR20143/US AVA Care Level 3-1 Year RR20144/US AVA Care Level 4-1 Year New Driver Device Integration RR20217/US Driver Configuration Service Controllers RR20250/US Laptop Controller - US Plug Data Hub & Accessories Thermo Regulators for any of our Lab Reactor Options: Reactor Ready, Duo and Pilot To compliment your Reactor Heidoph offers a variety of user friendly temperature control instruments. The perfect pairing will increase the efficiency of your workflow. All packages have been provided based on the most optimal results depending on which vessel size is chosen. We offer complete packages to stand alone units. Packages include fittings, insulated tubing, and 10 liters of thermal bath fluid RR20200/US Data Hub 4 Port - US Plug RR20202/US Data Hub 2 Port - US Plug RR20454/US Ethernet Switch (for up to 4 Data Hubs, 16 x RS232 ports) - US Plug Let us customize a complete system including reactor, vessels, software and thermal regulator. P/N Description Temp Recommended Voltage Heater Range for: Hei-Therm R Regulator CF41 Pkg C 115V/ 60Hz 1 kw Up to 1L vessel Hei-Therm R Regulator CF41-1 Pkg C 230V/ 50Hz 2 kw Up to 1L vessel Hei-Therm R Regulator P-A30 Pkg C 208V/ 60 Hz 2.3 kw Up to 1L vessel Hei-Therm R Regulator P-A40 Pkg C 208V/ 60Hz 2.3 kw 2-5L vessel Hei-Therm R Regulator P-A80 Pkg C 208V/ 60Hz 1.5 kw 5L vessel Hei-Therm R Regulator P-A80t Pkg C 08V/ 60Hz/ 3 ph 2.8 kw 5L vessel Hei-Therm R Regulator FP51-SL C 230V/ 60Hz/ 3 ph 3.0 kw Up to 20L vessel

96 ISO Certificate Your Contacts at Heidolph North America Contact Information North America Sales Director Steve Drayer Business Development Director Jason Paloskey Product & Marketing Manager Nicole Kvasnicka x 111 nkvasnicka@heidolph.com Channel Manager Sterilization Joe Bystron x 115 jbystron@heidolph.com Applied Markets Director Field Sales for: Oregon, Washington, Alaska, Hawaii Michael Bishop mbishop@heidolph.com Applied Markets Specialist Field Sales: Colorado, Utah Ezra Pryor epryor@heidolph.com New Jersey, Eastern Pennsylvania, Virginia, Maryland, Delaware, District of Columbia, Southern New York Andrew Ungerleider aungerleider@heidolph.com Connecticut, Rhode Island, Massachusetts, Maine, Vermont, New Hampshire, Eastern Upstate New York Trevor White twhite@heidolph.com Michigan, Ohio, Tennessee, Kentucky, Western Pennsylvania, West Virginia, Western New York Clayton Zelazowski czelazowski@heidolph.com North Carolina, South Carolina, Georgia, Florida, Alabama Benny Karaulic bkaraulic@heidolph.com Southern California, Southern Nevada, Arizona Rand Norberg rnorberg@heidolph.com Northern California, Northern Nevada Shawn Azari sazari@heidolph.com Texas, Louisiana, Oklahoma, Mississippi, Arkansas, New Mexico Zach Hightower zhightower@heidolph.com Montana, Wyoming, Idaho OPEN sales@heidolph.com Illinois, Indiana, Wisconsin, Minnesota, Kansas, Iowa, North Dakota, South Dakota, Missouri, Nebraska, Puerto Rico, US Virgin Islands Franklin Limpin flimpin@heidolph.com Canada Denis Gosselin dgosselin@heidolph.com Please contact the local Heidolph Sales Specialist to arrange any product demonstrations,application support, product trials, product specifications, etc

97 Notes Imprint Published by: Heidolph Instruments GmbH & Co. KG Walpersdorfer Straße 12 D Schwabach Publication date: 01/2017 Copyright 2017, Heidolph Instruments GmbH & Co. KG Not to be reproduced in part or in its entirety without the approval of the publisher. Images are shown for illustration only and may include other equipment or accessories in use. All the data provided is subject to technical changes and errors

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