Nexera-i Specifications Prominence-i Specifications

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Transcription:

C196-E092 LC Systems Specifications Specifications -Series Plus

Specifications MT LC-2030 LC-2030C LC-2030C 3D LC-2030C LT LC-2040C LC-2040C 3D LC-2040C MT LC-2040C 3D MT UV model without sample cooler ( ) ( UV model ) ( PDA model ) ( Detector-less model ) ( UV model ) ( PDA model ) ( UV model ) ( PDA model ) 228-65800-58 228-65801-58 228-65802-58 228-65803-58 228-65804-58 228-65805-58 228-65806-58 228-65807-58 Degassing unit Pumping method Pulsation Flow rate setting range Five Lines: Mobile phase 4 + Rinse solution 1 (Volume 400 µl) Parallel-type double plunger 0.1 MPa (1.0 ml/min,10 MPa, Water) 0.0001 to 10 ml/min Flow rate accuracy ±1% or ±2 µl/min, below whichever is greater (0.01 to 2 ml/min, Specified condition) ±2% (2 to 5 ml/min, Specified condition) ±1% or ±2 µl/min, below whichever is greater (0.01 to 2 ml/min,1 to 40 MPa, Specified condition) ±2% or ±2 µl/min, below whichever is greater (0.01 to 3 ml/min, 40 to 60 MPa, Specified condition) Pump Flow rate precision Configuration Gradient / range of set concentrations < 0.06 %RSD or < 0.02 minsd, below whichever is greater Four-solvent low-pressure gradient 0 to 100%, in 0.1% steps Gradient / concentration accuracy Gradient / concentration precision ±0.5% (0.1 to 2 ml/min, 1 to 20 MPa, Specified condition) ±0.1% (1 ml/min,10 MPa, Specified condition) Maximum pressure 44 MPa (0.0001 to 5 ml/min), 22 MPa (5.0001 to 10 ml/min) 66 MPa (0.0001 to 3 ml/min) 44 MPa (3.0001 to 5 ml/min) 22 MPa (5.0001 to 10 ml/min) System Delay Volume 650 µl (Option: 460 µl, 1100 µl) 460 µl (Option: 650 µl, 1100 µl) Approx. 505 ml (Flow Line 1) Approx. 765 ml (Flow Line 2) Injection method Total-volume sample injection Injection volume accuracy ±1% (50 µl, N = 10) Injection volume setting range 0.1 to 100 µl (Option: 0.1 to 50 µl, 1 to 500 µl, 1 to 2,000 µl) 0.1 to 50 µl (Option: 0.1 to 100 µl, 1 to 500 µl, 1 to 2,000 µl) Autosampler Injection volume reproducibility Cross-contamination Injection cycle time Samples for processing RSD < 0.20% (5.0 2000 µl), RSD < 0.25% (2.0 4.9 µl), RSD < 0.5% (1.0 1.9 µl), RSD < 1.0% (0.5 0.9 µl) 0.0025% (Caffeine, Specified condition) Min. 14 sec (Specified condition) 336 (1 ml), 216 (1.5 ml), 112 (4 ml), 4 (MTP/DWP) Sample cooler Not included 4 to 45 C (Room temperature needs to be 30 C or lower and the humidity 70% or less to go down to 4 C. Room temperature needs to be 15 C or higher to go up to 45 C.) Injection linearity > 0.9999 (1 to 100 µl, Specified condition) > 0.9999 (1 to 50 µl, Standard Sample Loop, Specified condition), > 0.9999 (1 to 100 µl, 100 µl Sample Loop (Option), Specified condition) Heating and cooling method Forced air circulation method Containable column size 6 pieces at 10 cm max., 3 pieces at 10 cm to 30 cm 2 pieces at 30 cm max. Column Oven Temperature control range Temperature control precision Room temperature 12 to 90 C, Setting range 4 to 90 C ±0.1 C Temperature stability ±0.8 C (Specified condition) Flow rate switching valve Max. 1 pc Incompatible with add on 2

Wavelength range Spectrum slit width Wavelength accuracy Wavelength reproducibility Noise level LC-2030 (UV model without sample cooler) LC-2030C (UV model) 228-65800-58 228-65801-58 228-65804-58 190 to 700 nm 8 nm ±1 nm ±0.1 nm LC-2040C (UV model) ±2.5 10 6 AU, (250 nm, Specified condition) MT LC-2040C MT (UV model) 228-65806-58 UV Detector Drift Simultaneous monitoring of 2 wavelengths Linearity Sampling rate Light source Flow cell 100 10 6 AU/h (250 nm, Specified condition) Enable (Any 2 wavelengths of 190 to 370 nm or 371 to 700 nm) Up to 2.5 AU (5%) Up to 100 Hz Deuterium (D2) lamp 12 µl (10 mm, TC), 12 MPa 8 µl (10 mm, TC), 12 MPa Option cell High-Speed: 8 µl (10 mm, TC), Semi-micro: 2.5 µl (5mm, TC) Conventional: 12 µl (10 mm, TC), Semi-micro: 2.5 µl (5 mm, TC) LC-2030C 3D (PDA model) LC-2040C 3D (PDA model) 228-65802-58 228-65805-58 MT LC-2040C 3D MT (PDA model) 228-65807-58 PDA Detector Wavelength range Spectral resolution Slit width Device resolution Number of photodiode array elements Wavelength accuracy Noise level Drift Linearity Sampling rate Light source Flow cell 190 to 800 nm 1.4 nm (Specified condition) 1.2 nm, 8 nm 0.6 nm/pixel 1024 ±1 nm ±3 10 6 AU (250 nm, reference: 350 nm, Specified condition) 500 10 6 AU/h (250 nm, reference: 350 nm, Specified condition) Up to 2 AU (5%) Up to 100 Hz Deuterium (D2) lamp (Standard), tungsten (W) lamp (option) 10 µl (10mm, TC) 12 MPa 8 µl (10mm, TC) 12 MPa Option cell High-Speed: 8 µl (10 mm, TC), Semi-micro: 2.5 µl (5 mm, TC) Conventional: 10 µl (10 mm, TC), Semi-micro: 2.5 µl (5 mm, TC) MT LC-2030 LC-2030C LC-2030C 3D LC-2030C LT LC-2040C LC-2040C 3D LC-2040C MT LC-2040C 3D MT UV model without sample cooler ( ) ( UV model ) ( PDA model ) ( Detector-less model) ( UV model ) ( PDA model ) ( UV model ) ( PDA model ) 228-65800-58 228-65801-58 228-65802-58 228-65803-58 228-65804-58 228-65805-58 228-65806-58 228-65807-58 Miscellaneous Dimensions Weight Available ph range Materials for parts in contact with liquids Workstation W410 H605 D500 mm 58 kg 63 kg 53 kg 63 kg 64 kg 1 to 13 Stainless steel (SUS316L, SUS316), FEP, PEEK, PTFE, perfluoroelastomer, ruby, sapphire, Hastelloy C, GFP, ceramic, PFA, quartz, PPS Stainless steel (SUS316L, SUS316), FEP, PEEK, PTFE, perfluoroelastomer, ruby, sapphire, Hastelloy C, UHMWPE, ceramic, PFA, quartz, PPS LabSolutions LC/GC Ver.5.71 or later, LabSolutions DB/CS Ver.6.31 or later (Incompatible with LCsolution) i-series Plus LC Systems 3

Main Optional Accessories Solvent Delivery Units FCV-11AL FCV-11ALS FCV-11AL Connection Kit 780 µl Mixer Kit 2 ml Mixer Kit Low Volume System Kit Compatible Volume System Kit 228-45048-58 228-45049-91 228-56249-41 228-57313-41 228-57313-42 228-57796-42 228-57796-43 This is the mobile phase selection valve (3 flow lines). An FCV-11AL connection kit is required to connect to an FCV-11AL unit. This is the mobile phase selection valve (1 flow line). An FCV-11AL connection kit is required to connect to an FCV-11AL unit. This kit includes connector cables and other items necessary for connecting FCV-11AL and FCV-11ALS units. This parts set includes a mixer and tubing for using TFA or other UV-absorbing substance as a mobile phase. This parts set includes a mixer and tubing for using TFA or other UV-absorbing substance as a mobile phase. This kit decreases the system volume when using. This kit is used to conform the system volume of to LC-2010. Autosamplers 50 µl Sample Loop 100 µl Sample Loop Optional 500 µl Sample Loop Optional 2 ml Sample Loop UHPLC Fitting (set of 1) UHPLC Fitting (set of 10) Sample Rack Plate for 1 ml Sample Vials (set of 2) Plate for 1.5 ml Sample Vials (set of 2) Plate for 4 ml Sample Vials (set of 2) Metal plate for 1.5ml Sample Vials (set of 1) 228-56074-44 228-56074-42 228-45405-41 228-45405-42 228-56867-41 228-56867-43 228-55735-41 228-56197-41 228-50830-92 228-56197-42 228-61515-42 This sample loop is used for injecting 50 µl volumes. (Standard configuration parts of ) This sample loop is used for injecting 100 µl volumes. (Standard configuration parts of ) This increases the injection volume to 500 µl. This increases the injection volume to 2 ml. Fitting for inlet to high-pressure capacity column Fitting for inlet to high-pressure capacity column Additional sample rack Plate used to place 84 1 ml sample vials Plate used to place 54 1.5 ml sample vials Plate used to place 28 4 ml sample vials Plate used to place 54 1.5 ml sample vials Column Ovens Column Clamp ASSY B5 Column Clamp ASSY B8 FCV-14AH FCV-34AH FCV Mounting Kit CMD CMD Cable 228-15617-91 228-15617-92 228-45014-41 228-45185-41 228-55765-42 228-37281-41 228-39991 This set of clamps is for adding a column with an outside diameter between 6.4 and 9.5 mm. This set of clamps is for adding a column with an outside diameter between 9.5 and 12.7 mm. Automatic column switching valve with 6 positions and 7 ports which is usable at a pressure of 34.3 MPa max. Automatic column switching valve with 6 positions and 7 ports which is usable at a pressure of 100 MPa max. This parts kit is used to secure an FCV-14AH/ 34AH unit inside the column oven. This column management device is used to record information about columns. This cable is used to connect between the CMD and main units. UV Detectors Recycle Valve Flow Cell for UV Detectors High-Speed Cell for UV Detectors Semi-Micro Cell for UV Detectors 228-56808-41 228-56167-41 228-45621-41 228-45605-46 This low-pressure flow-line selection valve is used to recycle mobile phase. This cell is compatible with conventional analysis. (Standard configuration parts of ) This cell is compatible with fast analysis. (Standard configuration parts of ) This cell is compatible with semi-micro analysis. PDA Detectors W Lamp ASSY for PDA Detectors Flow Cell for PDA Detectors High-Speed Cell for PDA Detectors Semi-Micro Cell for PDA Detectors 228-57110-41 228-42593-43 228-45618-54 228-45605-47 This assembly includes a tungsten lamp and its socket used for high-sensitivity analysis in the long-wavelength region. This cell is compatible with conventional analysis. (Standard configuration parts of ) This cell is compatible with fast analysis. (Standard configuration parts of ) This cell is compatible with semi-micro analysis. 4

Other Options Earthquake Reinforcement Kit 1 L Mobile Phase Bottles (set of 5) Optional Detector Attachment Kit Optional Optical Board Camera ASSY for Autosampler Optional AD Board Touch Panel Protecting Sheet Upgrade Kit UV Upgrade Kit PDA 228-56298-41 228-38583-42 228-56245-41 228-55518-41 228-55517-41 228-55519-41 228-59212-41 228-58993-41 228-58993-42 This kit is used to reinforce how the reservoir tray is attached. This is a set of five one-liter reservoir bottles for holding mobile phases. This kit contains a top plate and reservoir tray for installing an additional detector. This board is used to install additional connectors for optical link cables. It is used to install fluorescence detector RF-20A series and other detectors. This camera is installed inside autosamplers. It allows you to monitor the needle action via the computer screen. This is an analog-digital converter board. It is used to input the detector signal as an analog signal, such as when a non-shimadzu detector is connected. Protecting sheet for touch panel. Kit for upgrade from (UV model with sample cooler) to. Kit for upgrade from (PDA model) to. Optional Detector Specifications RID-20A Reflective index measurement range Noise level Drift Range Response Polarity switching Zero adjustment Maximum operating flow rate Temperature control of cell unit Cell capacity Material in contact with liquid Maximum operating pressure Operating temperature range Dimensions and weight RID-20A (228-45104-XX) 1 to 1.75 RIU 2.5 nriu 0.1 µriu/h A mode: 0.01 to 500 µriu P and L modes: 1 to 5000 µriu No filtering, 0.05 to 10 sec, 11 steps With a switch Auto zero, auto optical zero, baseline shift functions 20 ml/min (150 ml/min with an option) 30 to 60 C (0.01 C steps) 9 µl SUS316L, quartz, PTFE, Al 2 O 3, ETFE 0.4 MPa (4 kgf/cm 2 ) 4 to 35 C W260 D420 H140 mm, 12 kg Note: Hexafluoroisopropanol (HFIP) cannot be used as the mobile phase. RF-20A/RF-20AXS Light source Wavelength range Spectral bandwidth Wavelength accuracy Wavelength precision S/N Cell capacity Cell temperature control range Cell temperature setting range Functions Safety measures Operating temperature range Dimensions and weight RF-20A (228-45147-XX) Xenon lamp 0, 200 to 650 nm Water Raman peak S/N 1200 min. Low background S/N > 9000 RF-20Axs (228-45148-XX) Xenon lamp, low-pressure mercury lamp (To check wavelength accuracy) 0, 200 to 750 nm 20 nm ±2 nm ±0.2 nm Water Raman peak S/N 2000 min. Low background S/N > 12000 12 µl, 2 MPa (approx. 20 kgf/cm 2 ), SUS316L, PTFE (fluororesin), quartz 4 to 40 C, 1 C steps (Room temperature 10 C) to 40 C Four-wavelength detection, wavelength scanning Liquid-leakage sensor 4 to 35 C W260 D420 H210 mm, 16 kg W260 D420 H210 mm, 18 kg i-series Plus LC Systems 5

/ Specifications www.shimadzu.com/an/ For Research Use Only. Not for use in diagnostic procedures. This publication may contain references to products that are not available in your country. Please contact us to check the availability of these products in your country. Company names, products/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation, its subsidiaries or its affiliates, whether or not they are used with trademark symbol TM or. Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services, whether or not they are used with trademark symbol TM or. Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own. Shimadzu does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication. Shimadzu Corporation, 2017 Printed in Japan 3655-08703-20AIT