Total QC R&D QC R&D QC Food QC R&D QC QC Food PDA or UV Capillary Type FID Yonezawa
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1 ANALYTICAL EQUIPMENT. HPLC Total 98 Units 2. GC Total 22 Units Total Osaka Yonezawa Chitose Osaka Yonezawa Chitose Total QC R&D QC R&D QC Food QC R&D QC QC Food PDA or UV Capillary Type FID UHPLC TCD 3 2 Head Space Sampler Stability Test Chambers Storage Conditions Osaka 25 C/60%RH Yes 40 C/75%RH Yes Yonezawa Yes Yes Chitose Yes Yes 4. Other Equipment Japanese English Total Site Osaka Yonezawa Chitose API Chitose Food Equipment Management 原 吸光分光光度計 Atomic Absorption Spectrophotometer 2 LC-MS LC/MS 粒度分布測定器 Laser Diffraction Particle Size Analyzer 電気滴定装置 Electrometric Titrator 5 2 フーリエ変換 外分光光度計 FT/IR 4 2 KF 分測定装置 Karl Fischer Titrator 核磁気共鳴 NMR 400MHz 3 3 旋光計 Polarimeter 3 紫外 可視分光光度計 UV Spectrophotometer 4 全有機炭素系 TOC 3 GC-MS GC/MS 電導率計 Conductivity meter 2 蛍光分光光度計 Fluorescence Spectrophotometer 差 査熱量計 Differential scanning calorimetry 差熱天秤 TG-DTA (Thermogravimetric analysis) 融点測定装置 Melting point apparatus 2 2 X 線解析装置 XRD 分光 差計 Spectrophotometer 2 粘度計 Viscometer
2 EQUIPMENTLIST PILOT SITE / OSAKA Controlled area Controlled area VESSEL:Glass-lined 000L VESSEL:Glass-lined 00L DRYER: Blow Dryer DRYER:DBL Cone Cutter Mill VESSEL:Stainless Steel 000L CENTRIFUGE:Stainless Steel (36 i DRYER:Tray Dryer Pin Mill VESSEL:Glass-lined 200L CENTRIFUGE:Stainless Steel (26 i DRYER: Blow Dryer VESSEL:Stainless Steel 200L DRYER:Tray Dryer. VESSEL (m 3 ) (Liter) 2. AUTOCLAVE Reactor Capacity Total Total 500L Hastelloy Steel 0.98 MPa Glass-lined L Stainless Steel 0.49 MPa Stainless Steel Hastelloy 0.5 Teflon-lined FILTER 4. CENTRIFUGE 5. DRYER Glass-lined Nutsche Stainless Steel (26 inch) Double Cone Dryer 3 Stainless Steel Nutsche 4 Stainless Steel (36 inch) 3 Tray Dryer Glass-lined Vacuum 4 Vacuum Tray Dryer 4 Stainless Steel Vacuum Lyophilizer Teflon-lined Hastelloy Steel 6. TANK 7. RESIN COLUMN 8. OTHER EQUIPMENT Stainless Stee Steel GL PE Others 300L 00L Total 2 Humidity Control Device MILLING AND PACKING ROOM 0. UTILITIES 2 Milling and Packing Room Vacuum: Up to 20mm Hg absolute. Nitrogen: Bulk tankers 2 Cutter Mill Water:De-ionized Water system Liquid Nitrogen cooling: to - 75 C Pin Mill Waste Treatment Unit: 54m 3 /day Steam heating: to 50 C Electric Sieve Scrubber: Gas Scrubbers for acid and solvent gases (2) Brine cooling: to - 20 C Gas Scrubbers for solvent gases (2) Water cooling Cooling Towers (2) Gas Scrubbers for alkaline gases (2)
3 EQUIPMENT LIST COMMERCIAL SITE / YONEZAWA PLANT Controlled room 2 DRYER:DBL Cone. VESSEL (m 3 ) (Liter) Reactor Capacity Total Total Glass-lined Stainless Steel AUTOCLAVE 3. DISTILLATION UNIT 700L Stainless Steel 0.8 MPa Centrifugal-flow Thin-film Vacuum Evaporator 500L Stainless Steel 0.8 MPa 000L Stainless Steel 0.2 MPa 500L Stainless Steel 6. 0MPa 300L Stainless Steel 0.8 MPa 4. FILTER 2 Glass-lined Nutsche 5. CENTRIFUGE 6 Stainless Steel Nutsche 3 Stainless Steel (36 inch) Glass-lined Vacuum Stainless Steel (40 inch) 6 Stainless Steel Vacuum Stainless Steel (42 inch) 4 Plate and Frame Presses Teflon-lined (36 inch) 6. DRYER 7. TANK 8. COLUMN Double Cone Dryer Stainless Steel Steel GL Teflon Others Total 4000L 2500L 000L 700L 500L 200L Total Spray Dryer Resin Tray Dryer Silica Gel Vacuum Tray Dryer 9. MILLING AND PACKING ROOM 0. STORAGE. UTILITIES 6 Milling and Packing Room Tank farm consisting of 240m 3 capacity Brine cooling: from -20 to 40 C 4 Cutter Mill for solvents and 80m 3 capacity tanks Liquid nitrogen cooling: to -90 C 2 Hammer Mill for storing acids and alkaline materials. Water: De-ionized Water system (2) 4 Electric Shifter Sieve Purified Water System () Supersonic wave Sieve Scrubber: Gas Scrubbers for acid and solvent gases () Gas Scrubbers for solvent gases () Gas Scrubbers for alkaline gases ()
4 EQUIPMENT LIST COMMERCIAL SITE / YONEZAWA PLANT 2 Controlled area Controlled room VESSEL:Glass-lined 2000L VESSEL:Glass-lined 800L VESSEL:Glass-lined 200L CENTRIFUGE:Stainless Steel (36 inch) 2 DRYER:Vacuum Tray Dryer VESSEL:Glass-lined 3000L 2 VESSEL:Glass-lined 2000L 3 CENTRIFUGE:Stainless Steel,Teflon-lined (36 in 2 DRYER:Vertical Dryer 5 DRYER:DBL Cone. VESSEL (m 3 ) (Liter) Reactor Capacity Total Total Glass-lined Stainless Steel DISTILLATION UNIT 3. FILTER Rotary Evaporator (50L Glass) Teflon-lined Nutsche 5 Stainless Steel Nutsche 3 Stainless Steel Vacuum 4. CENTRIFUGE 5. DRYER 5 Stainless Steel (36 inch) 6 Double Cone Dryer Stainless Steel (42 inch) 3 Vertical Dryer Stainless Steel (48 inch) 2 Vacuum Tray Dryer 2 Rubber-lined (36 inch) Teflon-lined (36 inch) 6. TANK 7. COLUMN Stainless Steel Steel GL PE PP Others Total 6000L Total Resin MILLING AND PACKING ROOM 9. UTILITIES Milling and Packing Room Brine cooling: to - 20 C Water:De-ionized Water system () Purified Water System () Scrubber: Gas Scrubbers for acid and solvent gases () Gas Scrubbers for solvent gases () Gas Scrubbers for alkaline gases ()
5 EQUIPMENT LIST COMMERCIAL SITE / YONEZAWA PLANT 3 & PRODUCT PROCESSING AREA Controlled area 2 DRYER:Nauta Dryer VESSEL:Stainless Steel 3000L VESSEL:Glass-lined 3000L 2 CENTRIFUGE:Stainless Steel (36 inch) Milling and Packing Room. VESSEL (m 3 ) (Liter) Reactor Capacity Total Total Glass-lined Stainless Steel AUTOCLAVE 3. DISTILLATION UNIT 2500L Stainless Stee0.98 MPa Distillation column (0 stages) 4. FILTER 5. CENTRIFUGE 6. DRYER Stainless Steel Nutsche ( F900 / 200L) 3 Stainless Steel (36 inch) Filter Dryer (Stainless Steel / 2400L) PFA Lining (48 inch) 7. TANK 8. MILLING AND PACKING ROOM 9. STORAGE Stainless Steel Steel GL PE PP Others Total Milling and Packing Room Tank farm consisting of 60m 3 capacity Pulverizer for solvents and 20m 3 capacity tanks Pin Mill for storing acids and alkaline materials. PRODUCT PROCESSING AREA 0. UTILITIES Vacuum: Up to 20mm Hg absolute. DRYER Brine cooling: to - 20 C Double Cone Dryer Water:De-ionized Water System () Purified Water System () 2. MILLING AND PACKING ROOM Scrubber: Gas Scrubbers for acid and solvent gases () Vertical Mixer Gas Scrubbers for alkaline gases () Jet Mill Steam heating: to 20 C
6 EQUIPMENT LIST COMMERCIAL SITE / CHITOSE API MANUFACTURE AREA Controlled room VESSEL:Glass-lined 000L CENTRIFUGE:Teflon-lined (36 inch) DRYER:Vibrating Dryer (Stainless Steel / 662L) Controlled room VESSEL:Glass-lined 000L DRYER:Filter Dryer (Stainless Steel / 02 DRYER:Filter Dryer (Hastelloy Steel / 270 High potency area HPLC UF Membrance Concentrator 2 Vacuum Dryger UHPLC 2 Rotary Evaporator 2 Freeze Dryer Explosion-proof LC Filter Integrity Tester (Paulronic / Frosster IV) 2 Square Drying Chamber for Freeze Dryer. VESSEL (m 3 ) (Liter) Reactor Capacity Total Total Glass-lined Stainless Steel FILTER 3. CENTRIFUGE 2 Stainless Steel Nutsche 4 Stainless Steel (30 inch) 2 Teflon-lined Nutsche Stainless Steel (36 inch) 2 Glass-lined Nutsche 4. DRYER 5. TANK Double Cone Dryer (Glass-lined / 880L) 9 Stainless Steel Tray Dryer (Stainless Steel) Filter Dryer (Hastelloy Steel / 050L) 6. OTHER EQUIPMENT 7. UTILITIES Nitrogen Gas Humidity Controller Brine cooling: to - 20 C Steam heating: to 30 C Vacuum: Up to 20mm Hg absolute Nitrogen: Bulk tankers Water:Purified Water System () Scrubber: Gas Scrubbers for acid gases () Gas Scrubbers for solvent gases ()
7 EQUIPMENT LIST COMMERCIAL SITE / CHITOSE PLANT EXTRACT MANUFACTURE AREA MANUFACTURE BUILDING VESSEL: SUS L TANK: 500L MILL: SUS Crusher CONCENTRATOR: Thin-film rotary evaporator 4 VESSEL: SUS 2000L TANK: 000L MILL: Stone SUS Mascolloider CENTRIFUGE: Clarifier VESSEL: SUS 500L CENTRIFUGE(Settler): Decanter VESSEL: SUS 800L STERILIZER: Plate-type Sterilization EXTRACTION BUILDING Explosion-proof area VESSEL: SUS 2000L TANK: SUS36 500L (Chili pepper extract) 3 VESSEL: SUS 000L
8 EQUIPMENT LIST COMMERCIAL SITE / USA KILO LAB / infosdrc@hamari.co.jp / phone / fax VESSEL (Liter) Reactor Capacity Total Jacketed reactor 2 5 Non-jacketed reactor 2 3 Round bottom flask AUTOCLAVE 3. DRYER 0.5 L Parr shaker 2 Vacuum oven 0.5 L Stainless steel bomb 2.0 L Parr shaker 4. OTHER EQUIPMENT 5. ACCESS TO... Lyophilizer (8L) NMR (500 MHz, 400 MHz, 300 MHz ISCO Combi-Flash DSC Agilent 00 LC/MDS VL TGA Agilent 00 with DAD and ELSD detector XRD Agilent 200 for chiral analysis FTIR Metrohm 784 Karl Fisher titrator Melting point apparatus 400 MHz NMR Magnet, associated electronics, air handling compressor GeneVac EZ-2 personal evaporator Perkin-Elmer Model 34 Polarimeter HP 6890 GC with HP 5973 Mass Selective Detector Uvikon XS UV-Vis Spectrophotometer Tekmarr Dohrmann Headspace Autosampler Barnstead NANOpure Diamond Water Purifier Huber Unistat 905 heater/chiller Huber Unistat 385 heater/chiller Buchi R-220 Rotovapor Biotage Alstra Peptide Synthesizer Mettler-Toledo ME203E Analytical Balance
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