TENDER NOTICE NO. 07/2012 INVITATION FOR BIDS / NIT

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1 CSIR-Indian Institute of Petroleum (Council of Scientific & Industrial Research) P.O:I.I.P., MOHKAMPUR, DEHRADUN (UA) INDIA Ph (D), & Fax , Website: ISO 9001 Regd. Institute TENDER NOTICE NO. 07/2012 INVITATION FOR BIDS / NIT 1. Sealed tenders under two bids system ( part-i Technical bid along with EMD and part II Price bid) are invited from the Indian / Foreign manufacturers/ Authorised Distributors or Indian Agents for the supply, installation and commissioning of the following equipments:- S.No Tender No. Description of items Qty Single/ Double bid 1. PUR/1/12-13/ AB-VVDN/ 249 & 317/PO: Gas Chromatograph with FID andtcd Specifications: Hydrocarbons and generic compounds analysis by Flame Ionization Detector (FID) and analysis of gases by Thermal Conductivity Detector (TCD). 2 Nos of split/splitless injectors with provision for on-line/off line analysis using 6-port automatic heated gas sampling valve with 0.25, 0.5, 1.0 ml loop operated series for TCD and FID and separately, with computer, printer and all accessories as per detailed specifications attached. "Detailed specification as per Annexure-A" Bid Security EMD) (in Indian Rupees) Two Double 1,00, (One Lakh only) 2. Interested Bidders may obtain further information from the office of the Controller of Stores & Purchase/Stores & Purchase Officer, Indian Institute of Petroleum, Mohkampur, Haridwar Road, Dehradun , India, Phone No.: Complete Standard bid document may be downloaded by any interested bidder directly from our website free of cost. 4. A Pre-bid Conference will be held Monday on at am hours (IST). All prospective bidders are requested to kindly submit their queries to the address indicated above so as to reach 2.00 pm latest by The bids must reach this office on or before (extended due date ) upto 14:30 hours (IST) and shall be opened on same day at 15:00 hours (IST). 6. All bids must be accompanied by a bid security as specified above and must be delivered to the above office at the date and time indicated above. Bids will be opened in the presence of Bidders' representatives who choose to attend on the specified date and time. In the event of the date specified for bid receipt and opening being declared as a closed holiday for purchaser s office, the due date for submission of bids and opening of bids will be the following working day at the appointed time. 7. The Director, Indian Institute of Petroleum, Dehradun reserves the right to accept any or all tenders either in part or in full or to split the order without assigning any reasons there for. Stores & Purchase Officer 1

2 ANNEXURE-A Technical Specifications of Gas Chromatograph with FID and TCD Quantity Required : Two Nos.* Detailed Specifications Gas Chromatograph with FID and TCD Main Unit With multi ramp (more than 15) temperature programming and advanced electronic pneumatic control (EPC)/electronic flow control (EFC) for carrier and detector gas supply and capable of providing round the clock productivity. Highly precise retention time repeatability (< 0.008%) and area repeatability (< 1%RSD) Full EPC for all inlets and detectors. Injectors 2 no of PTV split/splitless capillary injection port(1no port for TCD and FID to connect series and 1 no port for FID which connecting in series for offline use ) maximum temperature 400 o C, with electronic pressure control for carrier gas and split flow, pressure range psi. temperature programming from ambient to 400 o C. Provision for connecting narrow bore and wide bore fused silica capillary columns. 1 no of packed purge injection port for offline for second TCD. All injection ports should be independently heated. 6-port automatic heated gas sampling valve for on-line analysis with 0.25, 0.5ml and 1 ml loop using GC Transfer Line from a micro reactor (to reduce high pressure to ambient pressure) Oven Temperature range ambient to 450 o C. Multi ramp (more than 18) temperature programming and plateaus with high accuracy, Temperature ramp rate 0.1 to 100 o C per minute or better Temperature set-point resolution should be 1 o C. Fastest cooling down rate for oven (less than 5 minutes for cooling from 400 to 50 o C). Stability & Accuracy: ±0.1 o C Control Through GC keyboard and PC software independently. Full EPC (Electronic Pneumatics Control) for inlets and detectors Detectors One high sensitivity Flame Ionization Detector FID (series connected) should be connectable to capillary column. Auto-ignition, auto-detection and re-ignition features. Maximum temperature of FID should be 450 C or better Detectivity should be 2 pg C/sec or lessthan. Linear dynamic range should be 10 7 or better Flame-out detection/auto re-ignition: standard One Thermal Conductivity Detector (TCD) with pressure safety switch. Maximum temperature of TCD should be 400 C or better Detectivity should be 400 pg tridecane /ml with He carrier or better Linear dynamic range should be 10 5 or better Filament protection: standard Air/He and hydrogen lines should have separate controls for both detectors. Alarm Alarm facility for heater, sensor and gas flow faults. 2

3 Data System Work station with Core2Duo computer with provision for dual channels for the simultaneous collection of data. Software should be M S 32 bit software Windows XP or Vista based and should be capable of report generation through multi-tasking window (complete environment control through software) and data processing with provision for offline data processing. Software should be capable of doing all operations required for running the instrument (complete instrument control through software/pc) Chromatography software The Chromatography software should be a client server based Chromatography data system supporting LIMS integration. The software should be able to acquire data from all the detectors and should have a single point control of all gas chromatographic parameters. The software should have the facility for interactive graphics, tool bar facility for online editing, recalculation, batch data processing, overlay, peak integration, S/N (signal to noise) ratio, programmable integration control, baseline compensation, options for continuous averaging of calibration data, weighted regression etc. All standard chromatographic parameters for qualitative and quantitative analysis should be available. Back-up for all softwares should be provided. Computer details Desk top computer system Core i5(with Turbo Boost), 3.4 GHz, 4.0 GB RAM, 500 GB hard disk, 16X DVD, CD, Combo drive,usb multimedia keyboard, optical USB mouse, 19 LCD-TFT color monitor with latest windows Windows 7 Professional/Windows 8 ( 64 bit) Ultimate and CD back-up from standard supplier like IBM/HP etc. USB port and other standard features. Heavy duty high resolution HP Laser Jet P1606dn printer Purifiers and traps For nitrogen, helium (carrier gas lines) for removing moisture, hydrocarbons, oxygen and other gases in series. For detector gas supplies i.e. for hydrogen and air lines, traps for removing moisture and hydrocarbons. Analytical Columns Capillary columns 1. Column material: 100% Dimethyl polysiloxane, Nonpolar (length 30 meter, 0.53mm, 3.00 u) 2. Column material: Polyethylene Glycol, polar (length 30 meter, 0.53mm, 3.00 u) 3. Column for separation of peremenent gases, H 2, H 2 O and C1 to C5, C6+ Hydrocarbons using TCD and FID Graphite ferule set of 0.53mm, 0.32 mm and 0.22 mm each 2 no. pack Packed columns for GC 1. Separation of N 2, O 2, CO 2, CO, H 2 O and C1-C4 hydrocarbons (Porapak Q, Porapak N, Molecular Sieve, Chromosorb PAW) Cone and ferule (1/4" and1/8") set for packed column 2 no. pack Gas/liquid Syringes Gas tight syringe for gas samples for 100 µl/ 2mL 20 no. each 3

4 Liquid syringe for liquid samples for 10 µl 20 no.each Complete GC Installation KIT required at our site Installation accessory kit, complete with SS 316 tubing, spanners, metal tube cutter, screwdriver, wrench, snoop leak detector, fuses, ferrules, nuts, fuses, septa, jet tool etc. Guarantee At least 24 months comprehensive guarantee from the date of commissioning Training Comprehensive user/maintenance training should be there Complete Installation and Demonstration along with standard /lab reference Detailed circuit diagram, service manual and operation manual to be provided Recommended list of spares for three years. Stores & Purchase Officer 4

5 MINUTES OF MEETING Sub: Pre bid Technical Presentation on Notice No. 07/2012 for PUR/1/12-13/AB-VVDN/249 & 317/PO and PUR/1/12-13/SKM/346/PO Date: 21st January, 2013 at IIP, Dehradun Present: Dr. S. M. Nanoti (Chairman), Dr. S. K. Maity, Dr. Anil K. Sinha, Dr. VVDN Prasad, Jagdish Kumar, Poonam Gupta and Dr. A. Bordoloi Presented by:s. K. Mohanty (Hydrocarbon Solution), A. Tyagi (Bruker) and, A. Rathore (Dani Intruments) The following points have been raised 1. We have discussed three GC (one for SK Maity, one for VVDN Prasad and one for Ankur) in pre bid meeting with three vendors. 2. We have explained our requirements to all the vendors. 3. After discussion with the three vendors we have finalised our technical specifications. 4. We have also made few changes as follows SKM (PUR/1/12-13/SKM/346/PO) a. pressure range for injector was changed from 0 to 150 psi to 0 to 100 psi and maximum temperature for injector was changed from 450 to 400 O C or more. One packed injector port was replaced by GSV. b. One detector for sulfur, nitrogen and phosphorous has replaced by sulphur and nitrogen detector. c. We have made clear clarification of the automated valve in the detail way d. Packed column has been modified as high temperature packed column. VVDN Prasad (PUR/1/12-13/AB-VVDN/249 & 317/PO) e. pressure range for injector was changed from 0 to 150 psi to 0 to 100 psi. One packed injector port was replaced by GSV. f. Two TCD and one FID have been finalized. Ankur (PUR/1/12-13/AB-VVDN/249 & 317/PO) g. pressure range for injector was changed from 0 to 150 psi to 0 to 100. One packed injector port was replaced by GSV. h. Two FID and one TCD have been finalized. Stores & Purchase Officer 5

6 REVISED DETAILED TECHNICAL SPECIFICATIONS AFTER PRE-BID MEETING HELD AT IIP, DEHRADUN ON DUE DATE Submission of bids by 2.30 PM Opening of bids at 3.00 PM 6

7 PUR/1/12-13/VVDN/317/PO: Dt: Revised Detailed Specifications Gas Chromatograph with FID and TCD 1 No. Main Unit With multi ramp (more than 15) temperature programming and advanced electronic pneumatic control (EPC)/electronic flow control (EFC) for carrier and detector gas supply and capable of providing round the clock productivity. Highly precise retention time repeatability (< 0.008%) and area repeatability (< 1%RSD) Full EPC s for all inlets and detectors. Injectors 1 no of GSV and 1 no of PTV (GSV port for TCD and FID to connect in series and PTV port for TCD) maximum temperature 400 o C, with electronic pressure control for carrier gas and split flow, pressure range psi. Temperature programming from ambient to 400 o C. Provision for connecting narrow bore and wide bore fused silica capillary columns. 1 no Split/Splitless Capillary injection port to be connected to either to TCD or TCD+FID in series All injection ports should be independently heated. 6-port automatic heated gas sampling valve for on-line analysis with 0.25, 0.5ml and 1 ml loop using GC Transfer Line from a micro reactor (to reduce high pressure to ambient pressure) Oven Temperature range ambient to 450 o C Multi ramp (more than 18) temperature programming and plateaus with high accuracy, Temperature ramp rate 0.1 to 100 o C per minute or better Temperature set-point resolution should be 1 o C. Fastest cooling rate for oven (less than 5 minutes cooling from 400 to 50 o C). Stability & Accuracy: ±0.1 o C Control Control through GC keyboard and PC software independently. Full EPC (Electronic Pneumatics Control) for inlets and detectors Detectors One high sensitivity Flame Ionization Detector FID connected in series should be connected to capillary column. Auto-ignition, auto-detection and re-ignition features. Maximum temperature of FID should be 450 C or better Detectivity should be 2 pg C/sec or less. Linear dynamic range should be 10 7 or better Flame-out detection/auto re-ignition: standard Two Thermal Conductivity Detectors (TCD) with pressure safety switch. Maximum temperature of TCD should be 400 C or better Detectivity should be 400 pg tridecane /ml with He carrier or better Linear dynamic range should be 10 5 or better Filament protection: standard Air/He and hydrogen lines should have separate controls for both detectors. 7

8 Alarm Alarm facility for heater, sensor and gas flow faults. Data System Work station with Corei5 and above computer with provision for dual channels for the simultaneous collection of data. Software should be Windows 7 (64 bit with DVD ) based and should be capable of report generation through multi-tasking window (complete environment control through software) and data processing with provision for offline data processing. Software should be capable of doing all operations required for running the instrument (complete instrument control through software/pc) Chromatography software The Chromatography software should be a client server based Chromatography data system supporting LIMS (Laboratory Information Management System) integration. The software should be able to acquire data from all the detectors and should have a single point control of all gas chromatographic parameters. The software should have the facility for interactive graphics, tool bar facility for online editing, recalculation, batch data processing, overlay, peak integration, S/N (signal to noise) ratio, programmable integration control, baseline compensation, options for continuous averaging of calibration data, weighted regression etc. All standard chromatographic parameters for qualitative and quantitative analysis should be available. Back-up for all software s should be provided. Computer details Desk top computer system Core i5(with Turbo Boost), 3.4 GHz, 4.0 GB RAM, 500 GB hard disk, 16X DVD, CD, Combo drive, USB multimedia keyboard, optical USB mouse, 19 LCD-TFT color monitor with latest windows Windows 7 Professional/Windows 8 ( 64 bit) Ultimate and CD back-up from standard supplier like IBM/HP etc. USB port and other standard features. HP Laser Jet Pro M1136 MFP printer Purifiers and traps Purifiers and traps for nitrogen, helium carrier gas lines for removing moisture, hydrocarbons, oxygen and other gases in series. Traps for removing moisture and hydrocarbons from hydrogen and air gas lines for detector. Analytical Columns Capillary columns 4. Column material: 100% Dimethyl polysiloxane, Nonpolar (length 30 meter, 0.53mm, 3.00 u) 5. Column material: Polyethylene Glycol, polar (length 30 meter, 0.53mm, 3.00 u) 6. Column for separation of peremenent gases, H 2, H 2 O and C1 to C5, C6+ Hydrocarbons using TCD and FID Graphite ferule set of 0.53mm, 0.32 mm and 0.22 mm each 2 no. pack Packed columns for GC 2. Separation of N 2, O 2, CO 2, CO, H 2 O and C1-C4 hydrocarbons (Porapak Q, Porapak N, Molecular Sieve, Chromosorb PAW) Cone and ferule (1/4" and1/8") set for packed column 2 no. pack 8

9 Gas/liquid Syringes Gas tight syringe for gas samples for 100 µl/ 2mL 20 no. each Liquid syringe for liquid samples for 10 µl 20 no.each Complete GC Installation KIT required at our site Installation accessory kit, complete with SS 316 tubing, spanners, metal tube cutter, screwdriver, wrench, snoop leak detector, fuses, ferrules, nuts, fuses, septa, jet tool heaters and sensors etc. Guarantee At least 24 months comprehensive guarantee from the date of commissioning Training Comprehensive user/maintenance training should be there Complete Installation and Demonstration along with standard /lab reference Detailed circuit diagram, service manual and operation manual to be provided Recommended spares for three years. (Stores & Purchase Officer) 9

10 PUR/1/12-13/AB/249/PO: Dt: Revised Detailed Specifications Gas Chromatograph with FID and TCD 1 No. Main Unit With multi ramp (more than 15) temperature programming and advanced electronic pneumatic control (EPC)/electronic flow control (EFC) for carrier and detector gas supply and capable of providing round the clock productivity. Highly precise retention time repeatability (< 0.008%) and area repeatability (< 1%RSD) Full EPC for all inlets and detectors. Injectors 1 no of PTV and 1 no split/splitless capillary injection port(ptv port for TCD and FID series connected, and split/splitless port for FID).Maximum temperature 400 o C, with electronic pressure control for carrier gas and split flow, pressure range psi. temperature programming from ambient to 400 o C. Provision for connecting narrow bore and wide bore fused silica capillary columns. 1 no gas sampling value to be connected to either to FID or TCD+FID in series. All injection ports should be independently heated. 6-port automatic heated gas sampling valve for on-line analysis with 0.25, 0.5ml and 1 ml loop using GC Transfer Line from a micro reactor (to reduce high pressure to ambient pressure) Oven Temperature range ambient to 450 o C. Multi ramp (more than 18) temperature programming and plateaus with high accuracy, Temperature ramp rate 0.1 to 100 o C per minute or better Temperature set-point resolution should be 1 o C. Fastest cooling down rate for oven (less than 5 minutes for cooling from 400 to 50 o C). Stability & Accuracy: ±0.1 o C Control Through GC keyboard and PC software independently. Full EPC (Electronic Pneumatics Control) for inlets and detectors Detectors Two no high sensitivity Flame Ionization Detector FID connected in series should be connected to capillary column. Auto-ignition, auto-detection and re-ignition features. Maximum temperature of FID should be 450 C or better Detectivity should be 2 pg C/sec or lessthan. Linear dynamic range should be 10 7 or better Flame-out detection/auto re-ignition: standard One Thermal Conductivity Detector (TCD) with pressure safety switch. Maximum temperature of TCD should be 400 C or better Detectivity should be 400 pg tridecane /ml with He carrier or better Linear dynamic range should be 10 5 or better Filament protection: standard Air/He and hydrogen lines should have separate controls for both detectors. 10

11 Alarm Alarm facility for heater, sensor and gas flow faults. Data System Work station with Core i5 and above computer with provision for dual channels for the simultaneous collection of data. Software should be Windows 7 (64 bit with DVD ) based and should be capable of report generation through multi-tasking window (complete environment control through software) and data processing with provision for offline data processing. Software should be capable of doing all operations required for running the instrument (complete instrument control through software/pc) Chromatography software The Chromatography software should be a client server based Chromatography data system supporting LIMS (Laboratory Information Management System) integration. The software should be able to acquire data from all the detectors and should have a single point control of all gas chromatographic parameters. The software should have the facility for interactive graphics, tool bar facility for online editing, recalculation, batch data processing, overlay, peak integration, S/N (signal to noise) ratio, programmable integration control, baseline compensation, options for continuous averaging of calibration data, weighted regression etc. All standard chromatographic parameters for qualitative and quantitative analysis should be available. Back-up for all softwares should be provided. Computer details Desk top computer system Core i5(with Turbo Boost), 3.4 GHz, 4.0 GB RAM, 500 GB hard disk, 16X DVD, CD, Combo drive,usb multimedia keyboard, optical USB mouse, 19 LCD-TFT color monitor with latest windows Windows 7 Professional/Windows 8 ( 64 bit) Ultimate and CD back-up from standard supplier like IBM/HP etc. USB port and other standard features. HP Laser Jet Pro M1136 MFP printer Purifiers and traps For nitrogen, helium (carrier gas lines) for removing moisture, hydrocarbons, oxygen and other gases in series. For detector gas supplies i.e. for hydrogen and air lines, traps for removing moisture and hydrocarbons. Analytical Columns Capillary columns 1. Column material: 100% Dimethyl polysiloxane, Nonpolar (length 30 meter, 0.53mm, 3.00 u) 2. Column material: Polyethylene Glycol, polar (length 30 meter, 0.53mm, 3.00 u) 3. Column for separation of peremenent gases, H 2, H 2 O and C1 to C5, C6+ Hydrocarbons using TCD and FID Graphite ferule set of 0.53mm, 0.32 mm and 0.22 mm each 2 no. pack Packed columns for GC 1. Separation of N 2, O 2, CO 2, CO, H 2 O and C1-C4 hydrocarbons (Porapak Q, Porapak N, Molecular Sieve, Chromosorb PAW) Cone and ferule (1/4" and1/8") set for packed column 2 no. pack 11

12 Gas/liquid Syringes Gas tight syringe for gas samples for 100 µl/ 2mL 20 no. each Liquid syringe for liquid samples for 10 µl 20 no.each Complete GC Installation KIT required at our site Installation accessory kit, complete with SS 316 tubing, spanners, metal tube cutter, screwdriver, wrench, snoop leak detector, fuses, ferrules, nuts, fuses, septa, jet tool heaters and sensors etc. Guarantee At least 24 months comprehensive guarantee from the date of commissioning Training Comprehensive user/maintenance training should be there Complete Installation and Demonstration along with standard /lab reference Detailed circuit diagram, service manual and operation manual to be provided Recommended list of spares for three years. (Stores & Purchase Officer) 12

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