B/R 9600 Packed Column Distillation Systems. Fractional Distillation for the Laboratory and Industry

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1 B/R 9600 Packed Column Distillation Systems Fractional Distillation for the Laboratory and Industry

2 9600 Packed Column Distillation Systems The 9600 Packed Column fractional distillation system is designed for challenging separations on batches of 1 to 500 liters. n High Efficiency: These fractional distillation systems have 15 theoretical plates at atmospheric pressure. Distillation columns can be stacked for even higher efficiencies. They are well suited for producing high purity materials and making difficult separations. n Customized for your Application: The 9600 can be configured according to your needs. Automation, vacuum systems, fraction collectors and other accessories can be integrated into the distillation system as needed. The result is a distillation apparatus customized to your specific needs. n Easy to use: Microprocessor control fully automates the distillation process from beginning to end, minimizing the time needed to operate the equipment. Easy programming of parameters makes you feel like a distillation expert. Heating, collecting of distillate and shut down of equipment at completion are all done automatically. Optional control from a PC.

3 9600 Packed Column Features Feature Specification Benefit Distillation Column Diameters 25, 36, 50, 70, 100, 150 mm Large Diameter Provides Maximum Throughput Maximum Theoretical Plates Standard Columns are 15 Plates. 2 or 3 High Efficiency Separation Combined with Low Hold Up Columns can be Stacked for Higher Efficiency Distillation Column Jacket Glass Columns have Vacuum Jacket and Silvered Prevents Heat Loss from Distillation Column (Adiabatic) Mirror Stainless Steel Columns have Insulation Heated Column Jackets are Available Heated Jackets Provide Further Heat Loss Prevention Condenser Inner Coil and Outer Jacket High Surface Area for Efficient Condensing Secondary Condenser Cools Distillate Further Before Going to Receiver Distillate in Receiver is Close to Room Temperature Boiler Heater Electrical Clean, Safe Heating of Boiler Boiler Sizes 1, 2, 3, 5, 12, 22, 50, 72, 100, 200, 300, 500 liters Available in Stainless Steel in all Sizes Available in Glass up to 50 liters Boiler Stirring Optional Promotes Even Boiling and Gentle Heat Transfer Column Packing Types Propak, Helipak, Wiremesh, Raschig Rings, Select the Packing Type that is Best for your Application Structured Packing and More Condensing Bath Optional Circulating Bath Automatically Cools and Heats Condenser Bath C Bath to 100 C Fraction Collector Standard 2 Place Automatically Collect Fractions Optional 4 Place and 8 Place According to Vapor Temperature Vacuum Operation Optional Vacuum System Automatic Control of Vacuum Level mmhg Range Vacuum Reduces Boiling Points. Ideal for Thermally Other Ranges Available Sensitive Samples or High Boiling Materials Automatic Controller Provides Automatic Control of the Entire Start the Distillation and Walk Away Distillation Process PC Optional Control From PC Perform a Distillation from a PC. Analyze Distillation Results using our Data View Program. Safety Marks CE Marked Safe for Laboratory and Industrial Use Listed to UL by ETL Listed to CSA C by ETL C TICK (Australia/NZ) Power (Distillation Unit Only) 1-22 liter (115 V) 15 amps Configured for Local Power Requirements 1-22 liter (220 V) 8 amps and with Local Power Plug, 115 or 220 V, 50/60Hz 50 liter (220V) 15 amps Other Utilities Required Cooling Water or Circulating Bath For Condenser

4 Pressure Sensor Vacuum Control Valve Condenser n Condenser has inner coil and jacket condensing surfaces n Connecting arm to fraction collector is also temperature controlled n Optional Circulating Bath in place of cooling water for the condenser Vacuum System n Vacuum distillation lowers the sample s boiling point, allowing high boiling and sensitive samples to be distilled. n Automatically regulates to programmable vacuum level n Includes vacuum pump, control valve, vacuum sensor and cold tap n Optional automatic cold trap eliminates the need to use dry ice Packed Distillation Column n High throughput n 15 theoretical plate columns n Stacked columns for higher efficiency n Programmable Reflux Ratio 0:1 up to 999:1 Fraction Collector n Automatic collection of fractions by vapor temperature n 2, 4 or 8 fractions for each pressure level Boiling Flask n Glass or stainless steel n Optional stirring heating mantle n Temperature probe for boiling flask liquid Automatic Control n Automatic control of distillation process n Automatic recording of distillation data n Windows based software is intuitive and guides you through the distillation process step by step Optional Stirring Thermowell

5 Optional PC and Software Easy to use distillation programs allow each fraction to have programmable: n Start and finish temperatures n Heating rate for boiling flask. n Reflux ratio n Condenser Temperature Each distillation program also allows for: n Selection of vacuum level n Setting maximum boiling flask temperature n Set equilibration time n Select number of fractions to be collected Distillation Results Log: n Automatically records all the distillation variables twice a minute. Creates a complete report of the distillation. n View Results in tables or graphs. n Results logs are easily downloaded and opened by spread sheets. Process diagram clearly shows the current equipment status.

6 Packed Column Distillation Configured for Your Application Choose from: n Boilers Sizes: 1 to 500 liters n Efficiency: 15 to 50 Theoretical Plates n Materials: Glass or Steel Construction n Pressure Level: Vacuum and/or Atmospheric Distillation n Automatic Control: Dedicated Microprocessor or PC

7 B/R Instrument Corporation B/R Instrument was founded in 1966 by Roger Roark, Sr. and Harry Brown, Jr. The name B/R comes from the first letter of each founder s last name, Brown and Roark BR. Originally a manufacturer of general glassware, the company began to specialize in the manufacture of spinning band distillation systems in 1968 under a DuPont patent. Since then the company has grown steadily in the distillation and laboratory equipment markets and now distributes products to customers throughout the world. Located in Easton, Maryland on the beautiful Eastern Shore of the Chesapeake Bay, the B/R facility encompasses 14,700 square feet (1,370 square meters) and houses manufacturing, sales, engineering, service and administrative divisions. B/R INSTRUMENT Packed Column Distillation: All distillations attempt to separate a lower boiling material (A) from a higher boiling material (B). Packed columns are packed with a material that creates a large surface area within the distillation column. Vapors rise through the column, are condensed by the condenser and fall back down the column. This material is called condensate. The descending condensate wets the packing and is forced into intimate contact with the ascending vapors. This intimate contact causes the vapor to become enriched in the lower boiling material. This process is often called rectification. B/R Instrument Corporation Easton, Maryland USA better.results@brinstrument.com www. brinstrument.com B/R Instrument Corporation