Rotary Evaporator Replacement Glassware

Transcription

1 Rotary Evaporator Replacement Glassware from ce Glass ce Glass, founded in 1936, continues our long tradition of manufacturing high quality specialty glassware. We would like to introduce a new, comprehensive line of glassware to fit today s popular rotary evaporators. This brochure outlines the more widely used glassware sets and component parts to replace your existing glass. ce also offers both custom glass and glass repair services for rotary evaporators. ce Glass rotary evaporator replacement glass, all manufactured in the US to exacting specifications and standards.

2 (Plastic-Coated) (Non-Coated) Condenser C ssembly for Buchi Rotary Evaporators Fits Buchi Models 200/205 and Series Glassware can be ordered either clear plastic-coated or standard non-coated. The C ssembly contains the main glass outer trap body with a inner ball joint bottom connection that attaches to the receiver flasks (which are sold separately). Features standard top and side flange that connects directly to the Buchi rotary evaporator. ssembly C also includes the glass cold trap inner body, 00672, PTFE sealing ring with Viton O-Rings, PTFE lid or cap, PTFE hose barbs and GL threaded caps Note: Some parts are not interchangeable between series and 200/205. Please check your Buchi manual for the correct Buchi part number and match to the ce Glass part below (Plastic Coated) (Non-Coated) (Plastic-Coated) (Non-Coated) C ssembly Plastic-Coated Description Complete C ssembly Complete C ssembly. lso includes 1 x ml receiving flask, stainless steel clamp Plastic-Coated Components Outer trap body only C ssembly Non-Coated Complete C ssembly Complete C ssembly. lso includes 1 x ml receiving flask, stainless steel clamp Individual Components Non-Coated Outer trap body only Cold trap inner body PTFE Lid PTFE seal ring with Viton O-Ring Stopcock/Bottom Stopcock/Top joint adapter (without clip) Stainless steel clamp Glass steam tube (part of Buchi #40016) See page six for individual flask listings ing & Product Information:

3 (Plastic-Coated) (Non-Coated) Condenser CR ssembly for Buchi Rotary Evaporators Fits Buchi Models 200/205 and Series ssembly is very similar to C ssembly except that the bottom joint is 45/40 inner to fit into separate distribution head. Complete CR ssembly includes main glass cold trap outer body, glass cold trap inner body, PTFE cap, PTFE seal ring with Viton O-Rings, GL thread caps and hose barbs Note: Some parts are not interchangeable between series and 200/205. Please check your Buchi manual for the correct Buchi part number and match to the ce Glass part below (Plastic-Coated) (Non-Coated) (Plastic-Coated) (Non-Coated) CR ssembly Plastic-Coated Description Complete CR ssembly Plastic-Coated Components Cold trap condenser body only Lower distribution head with shut-off valve CR ssembly Non-Coated Complete CR ssembly Individual Components Non-Coated Cold trap condenser body only Lower distribution head with shut-off valve Cold trap inner body PTFE Lid PTFE seal ring with Viton O-Ring Stopcock/Distribution Head Stopcock/Top joint adapter (without clip) Stainless steel clamp Glass steam tube (part of Buchi #40016) See page six for individual flask listings (Plastic-Coated) (Non-Coated) For Engineering Support, visit 3

4 4 Condenser ssembly for Buchi Rotary Evaporators (Plastic-Coated) (Non-Coated) Fits Buchi Models 200/205 and Series Complete ssembly includes main glass condenser body with inner coil for angled installation, O-Ring, GL thread caps and hose barbs. Bottom joint is. Note: Some parts are not interchangeable between series and 200/205. Please check your Buchi manual for the correct Buchi part number and match to the ce Glass part below ssembly Plastic-Coated Description Complete ssembly Complete ssembly. lso includes 1 x ml receiving flask, stainless steel clamp 40633/ ssembly Non-Coated Complete ssembly Complete ssembly. lso includes 1 x ml receiving flask, stainless steel clamp (Plastic-Coated) (Non-Coated) Individual Components Non-Coated joint adapter (without clip) Stopcock/Top Stainless steel clamp Glass steam tube (glass part of Buchi #40016) See page six for individual flask listings Custom work or repairs needed? Call ce Glass at ing & Product Information:

5 (Plastic-Coated) (Non-Coated) Condenser V ssembly for Buchi Rotary Evaporators Fits Buchi Models 200/205 and Series Complete V ssembly includes main glass vertical condenser body with inner coil, O-Ring, GL thread caps and hose barbs. Bottom joint is. Note: Some parts are not interchangeable between series and 200/205. Please check your Buchi manual for the correct Buchi part number and match to the ce Glass part below (Plastic-Coated) (Non-Coated) V ssembly Plastic-Coated Description Complete V ssembly Complete V ssembly. lso includes 1 x ml receiving flask, stainless steel clamp 40603/ V ssembly Non-Coated Complete V ssembly Complete V ssembly. lso includes 1 x ml receiving flask, stainless steel clamp Individual Components Non-Coated joint adapter (without clip) Stopcock/Bottom Stainless steel clamp Glass steam tube (glass part of Buchi #40016) See page six for individual flask listings See the ce Glass Catalog for a complete listing of rotary evaporators and glassware. For Engineering Support, visit 5

6 Buchi Replacement Glass Components Long Short Vapor Duct Tubes ( w/o combi clip) Fits Buchi Length, Models () R114-R R114-R R114-R R114-R R114-R R114-R For ssy. V V V V V Buchi Part # * * * * ** ** ** ** ** ** *Same as Buchi part numbers 48160, 48161, and 48164, except the above are without clip. **Same as Buchi part numbers 32340, 32342, 32344, 32339, 32341, 32343, except the above are without clip Flask dapters ( w/o combi clip) Fits Buchi Models / / Stopcocks 3954 Description Stopcock/Bottom Stopcock/Top 3990/6892 Evaporating Flasks P ear shaped w/ s Plastic-Coated, HEVY WLL 3990/6892 Size, ml Non-Coated, HEVY WLL Size, ml ing & Product Information:

7 3994 Plastic Coated, HEVY WLL Size, ml Non-Coated, HEVY WLL Size, ml 3996, 6902 Receiving Flasks Single neck, round bottom Plastic-Coated, HEVY WLL Size, ml / / / /6902 Non-Coated, HEVY WLL Size, ml 3000 Buchi Replacement Glass Components 3994 Drying Flasks Pear shaped w/side indents, neck joint 7 If you don t see your part or component listed here, or if you need a custom component, call or ce Glass and we ll be glad to make it for you. For Engineering Support, visit

8 Rotary Evaporator Replacement Glass Components Large Evaporator Flasks Used with Heidolph 20 Liter Rotary Evaporators. These large flasks are fabricated from blanks selected for balance and quality. Necks are carefully welded to prevent rotational whip. Flasks can be plastic coated upon request. Cap., Liters Overall Height, O.D., Flange B I.D., C Large Receiver Flasks Used with Heidolph 20 Liter Rotary Evaporators. This receiver flask is fabricated from blanks selected for balance and quality. Center neck is a polished 40/25 joint, side neck is a GL-18 thread, supplied with solid cap. t bottom is a 0-10 easy action stopcock with a GL-18 side arm, supplied with a 3/8 hose connection tube. Flasks can be plastic coated upon request. Cap., Liters Overall Hght., 355 Center Neck 40/25 Side Neck GL18 Bottom Outlet 0-10/GL Vapor Tubes for Heidolph 4000 Series Used as replacements with Heidolph 4000 Series Rotary Evaporators. Tube is secured in rotary drive with low-stress plastic clip that seats into groove behind joint. vailable plain or with Firestone Splash Guard to protect against splash-up. -30 is supplied with evaporator. Type Plain Plain Plain Plain w/splash Guard w/splash Guard 24/25 45/50 ing & Product Information:

9 Large Evaporator Flasks For Buchi Rotavapor System Easy replacement select the size and capacity you need 6702 Large Evaporator Flasks These large flasks are fabricated from blanks selected for balance and quality. Necks are carefully welded to prevent rotational whip. Flasks can be plastic coated* upon request. EVPORTOR FLSK Easy Instructions 1. Determine flange size () O.D., (B) I.D., (C) thickness (see diagram). 2. Match flask capacity with overall height and flange size. C B 1. Select Flange Size. OVERLL HEIGHT Flange Size Designation S (Small) M (Medium) L (Large) EL (Extra Large) O.D., (Inches) 90 (3.5) (3.9) 110 (4.3) (5.9) B I.D., (Inches) 67 (2.7) 72 (2.8) 83 (3.3) (4.7) C Thickness () Select Flask Capacity and match with Flange Size. * Plastic coated flasks are transparent, and will withstand temperatures up to C. The coating is resistant to the occasional laboratory solvent or acid splash, but should not be soaked in them. void prolonged contact. Capacity, Liters Overall Height, Flange Size S M M L L EL S M M L EL M M L EL Special size s can be mad e to order. Call or ema il CE GLSS for more information. For Engineering Support, visit 9

10 Rotary Evaporator Replacement Glass Components Stopcocks w/inlet Feed Tube Used in Heidolph 4000 Series Rotary Evaporator condensers and other popular brand rotary evaporator condensers as inlet feed tube to allow continuous feed of volumes exceeding capacity of evaporating flask. Size is 19/38 with 6 O.D. feed tube Traps Rotary Evaporator, Boulanger, Self Washing Self-washing rotary evaporator trap designed by William. Boulanger. Unique design incorporates an inverted, straight, heavy-walled expansion chamber that allows for flow-back of bumped materials. Condensation of evaporated solvent on walls of trap continuously rinses trap during operation. Vacuum stem has two opposing holes, flush with bottom of stem, to allow solvent vapor to rapidly flow out, while allowing condensed solvent to return to flask. This feature means the evaporator shaft is also continuously rinsed and the material returned to the flask. To prevent pooling of the condensate in the shaft trap, the end of the trap has a center hole for complete drainage. When solids are bumped onto the sides of the trap toward the end of solvent evaporation, introduction of a small amount of solvent at top of trap with a swirling motion effectively rinses the material back into the flask. Bottom Capacity, Top Outer Inner ml ing & Product Information:

11 Greatly reduces carry-over from foaming or bumping. pprox. Bottom Overall Capacity, Top Outer Inner Height, ml Traps Rotary Evaporator, nti-splash, Improved Greatly reduces carry-over from foaming or bumping. Two drain holes, close to base of the inner tube, allow solvent to drain back into evaporator flask. Capacity, ml Top Outer Bottom Inner pprox. Overall Height, Traps Rotary Evaporator, nti-climb Upper tubulation prevents migration of film and foam directly into the condenser. Capacity, ml Top Outer Bottom Inner pprox. Overall Height, Rotary Evaporator Replacement Glass Components 6704 Traps Rotary Evaporator, nti-splash 11 For Engineering Support, visit

12 Rotary Evaporator Replacement Glass Components dapters Vial or Bottle, PTFE Used to connect a vial or a bottle to the vapor tube of a rotary evaporator. Fabricated from PTFE, one side is an outer joint with rib for using clamp such as 7598, other end is a outer vial or bottle thread Thread Size dapters Splash Guard, with Fritted Disc, Firestone* medium length joints, top and bottom, that will accept full length joints, plus a coarse porosity ( µ) fritted disc that assures no carry-over in the event of pot splash-up. Overall length is kept to a minimum to effect best distillation. Top Outer 24/25 24/25 24/25 Bottom Inner 24/25 29/26 45/ *Designed by Dr. Raymond Firestone (U.S. Patent No. 4,267,150) dapters Splash Guard, Firestone* medium length joints, top and bottom, that will accept full length joints. When inserted into flask, splash guard combines with flask neck to give best protection against pot splash up. Overall height is kept to a minimum to effect best distillation. Top Outer 24/25 Bottom Inner 24/25 *Designed by Dr. Raymond Firestone (U.S. Patent No. 4,267,150) ing & Product Information:

13 6714 Ingenious rotary evaporator constructed of glass or stainless steel, PTFE and glass-filled PTFE that operates without the devices normally associated with this type of equipment. Use with any lab stirring motor. Hollow glass or Stainless Steel (for larger capacity flasks) 10 O.D. tube, with or at one end for flask and holes drilled near center for vacuum, attaches to laboratory stirring motor. Tube turns inside PTFE bearing held in ce-threds by glass-filled PTFE bushing, compression saddle with O-Ring and lock nut. 2 straight bore stopcock attaches to drying tube and/or McLeod gauge. One arm of 4 bore double oblique stopcock attaches to dry ice trap and vacuum line; other arm is for easy vacuum release and can be connected to a trap. Complete item supplied with joint clamp; does NOT include stirring motor, chuck, flask or splash guard. Instead of connecting motor directly, use CE Flexible Shaft, to get heavy motor out of the way. Optional. For Flask Glass Shaft Stainless Steel Shaft stainless steel shaft is available for heavier flasks Replacement Parts *Designed by Dr. Raymond Firestone (U.S. Patent #4,569,724). Glass Body, only Glass/PTFE Bushing, with O-Ring, only (2) Glass/PTFE Lock Nut, only (2) Compression Saddle with O-Ring, only (2) PTFE Bearing, only (2) Hollow Glass Tube, Hollow Glass Tube, Hollow S-S Tube, Hollow S-S Tube, Splash Guard, Splash Guard, 24/25 Flexible Shaft, 91.4cm, Complete For a full selection of Rotary Evaporators from IK and Heidolph, visit the ce website at or see our new Catalog Rotary Evaporator Replacement Glass Components 6714 Rotary Evaporator Firestone* 13 For Engineering Support, visit

14 Rotary Evaporator Replacement Glass Components Receiving Bottles/Flasks Graduated, round bottom receiving flasks for use as replacement receivers on all glassware sets. ml size graduated in 10mL increments; ml and ml in ml increments. is. Cap., ml O.D., Length below joint, Receiving Tubes/Cylinders Graduated, tapered bottom receiving tube for use as replacement receivers on all glassware sets. ml size graduated in 0.5mL increments from 0-10mL; 5mL increments from 10-mL. is. Cap., ml O.D., 38 Length below joint, 225 Special Note: and 35/25 spherical joint components are interchangeable. See the ce Glass Catalog for a complete listing of rotary evaporators and glassware. ing & Product Information:

15 Glass conversion adapter with or joint to or #25. is used with through -22 or through -134; #25 is used with or connecting adapter to connect vials or flasks to rotary evaporator. Suitable for vacuum work. each item separately ce-thred #25 # dapters Connecting, PTFE PTFE connecting adapter with or #25 ce-thred and GPI thread to connect , -37, -44 or -47 conversion adapter to matching vial for use in rotary evaporator. Suitable for vacuum work. each item separately. Note: FETFE not suitable for use with methylene chloride or acetone. Use Chemraz instead. GPI Thread ce-thred #25 w/fetfe O-Ring w/chemraz O-Ring Multipack Connecting dapter Kit Convenience kit with several PTFE ce-thred to GPI thread adapters to fit various vial sizes version includes the -11 through -24 PTFE adapters listed above version includes the -121 through -134 PTFE adapters listed above. The kit also includes one glass conversion adapter CE Scientific Glass Repair Service Rotary Evaporator Replacement Glass Components dapters Conversion 15 CE Custom Glass Design Service For Engineering Support, visit

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