Rozsah akreditácie. Predmet Vlastnosť Druh Označenie neistota U
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1 akreditácie Strana 1/6 Polložka Názov akreditovaného subjektu: Štátny veterinárny a potravinový ústav Laboratóriá odboru hygieny potravín a krmív Akademická 3, Nitra akreditácie skúšobného laboratória: Laboratórium - typ 2 ( laboratórium môže modifikovať, optimalizovať v tomto rozsahu uvedené skúšobné metódy). 1. Krmivo suché vlhkosť vážková Výnos MP SR č. A (0,30 20) č. 1497/4/ (CHK 1) 2. Krmivo a potraviny obsah dusíkatých látok Kjeldahlova Výnos MP SR č. B1 (CHK 2) (0,50 65) 3. Krmivo obsah tuku extrakčná Výnos MP SR č. C1 (0,20 25) suché (CHK 3) g/100 g 4. číslo kyslosti titračná Výnos MP č. C2 (1,20 120) tuku (HK 4) mg KOH/ g 5. obsah rozpustných titračná podľa Výnos MP SR č. F7 (0,06 10) chloridov ako NaCl Volharda (CHK 5) 6. obsah popola vážková Výnos MP SR č. H1 (0,03 20) (CHK 6) 7. obsah vlákniny vážková (CHK 7) (0,70 55) 8. kyslosť vodného titračná Výnos MP SR č. J1 (11, ) výluhu, celková (CHK 8) mg KOH/ 100 g kyslosť 9. Bryndza, prírodné tavené syry, plesňové syry, tvarohy Mlieko konzumné, smotana, kvasené mliečne výrobky, kyslo-mliečne, kvasené ochutené výrobky Majonéza Mrazené smotanové a mliečne krémy, sladené a nesladené zahustené mlieko obsah sušiny vážková STN STN (CHP 9A) obsah sušiny STN /B STN /C (CHP 9B) obsah sušiny STN (vody) (CHP 9C) obsah sušiny STN STN (CHP 9D) (0,30 58) (0,20 58) (0,60 30) (0,50 35) Mäso a mäsové výrobky obsah vody STN ISO 1442 (CHP 9E) (0,80 80) Živočíšne tuky obsah vody STN (0,01 5) (CHP 9F) Polotovary a hotové jedlá obsah vody STN (0,80 90) (CHP 9G) Ryby, rybacie výrobky obsah vody STN (0,70 80) (sušiny) (CHP 9H) Sušené mlieko, mliečne obsah vody STN (0,20 10) výrobky (CHP 9I) 10. Maslo obsah vody vážková STN ISO 3727 (0,20 30) (CHP 10, 11) 11. obsah beztukovej extrakčná (0,30 5) sušiny 10 % 10 % 1 7 % 8 % 9 %
2 Strana 2/6 12. Bryndza, prírodné tavené syry, plesňové syry, tvarohy, Sušené mlieko, tekuté mlieko, kyslomliečne výrobky bez prísad obsah tuku extrakčná STN (0,20 60) podľa Schnid (CHP 12) Bodzinského Zahustené sladené a nesladené mlieko Tekuté mliečne a kyslomliečne s prídavkom stabilizátorov Mrazené mliečne výrobky obsah tuku obsah tuku extrakčná podľa Rose Gottliebe STN STN (CHP 13A) STN ISO 1737 (CHP 13B) extrakčná STN podľa (CHP 14A) Weibulla STN (CHP 14B) 15. Mäso, mäsové výrobky obsah tuku extrakčná STN (CHP 15A) Konzervy, polotovary, STN hotové jedlá (HP 15B) Majonézy, majonézové STN krémy, nátierky (CHP 15C) 16. Bryndza, prírodné tavené obsah NaCl titračná podľa STN syry, plesňové syry, tvarohy Volharda (CHP 16A) Majonézy, majonézové STN omáčky (CHP 16B) 17. Mäso, jedlé droby surové údené, obsah NaCl titračná podľa STN polotovary a hotové jedlá, Mohra (CHP 17A) mäsové výrobky, konzervy Ryby, rybacie výrobky STN (CHP 17B) 18. Tvarohy, syry, bryndza ph potencio- STN metrická (CHP 18A) Mäsové výrobky STN (CHP 18B) 19. Mäsové výrobky, konzervy, obsah fotometrická SNT bravčová slanina, údená, dusitanov, (CHP 19) mäso a jedlé droby surové dusičnanov údené, tvarohy, syry 20. Živočíšne tuky peroxidové titračná - STN číslo jodometria (CHP 20) 21. Živočíšne tuky číslo kyslosti titračná - STN EN ISO 660 tuku alkalimetria (CHP 21) 22. Med obsah polarimetrická STN sacharózy (CHP 22) 23. Med kyslosť titračná STN (CHP 23) 24. Med obsah hydroxymetylfurfuralu fotometrická STN (CHP 24) 25. Med obsah vody refraktometrická STN (CHP 25) 26. Med obsah popola vážková STN (CHP 26) 27. Mlieko konzumné metóda podľa STN a trvanlivé peroxidázy Storcha (CHP 27) (0,60 35) (0,80 20) (0,40 20) (0,70 70) (0,30 50) (1,20 40) ( ) ( ) ( ) 5 % 6 % 5 % ( ) (2,0 10) (2,0 10) 1% (2,0 100) (0,50 10) mmol/ kg (0,01 10) mg KOH/ g (0,40 10) (0,03 5) ml NaOH/100 g (0,07 5) ml/ 100 g 6 % Veterinárne metodiky 7 % 6% 5 % (0,04 25) (0,04 2) 8 %
3 Strana 3/6 28. Mlieko konzumné a trvanlivé fosfatest STN fosfatázy (CHP 28) 29. Hydinové mäso obsah cudzej vody chemická STN (CHP 29) 30. Krmivo druh a množstvo húb Biologický materiál Koža, stery Laboratórne priestory Požívatiny, suroviny mikromycét dermatofytov mikromycét počet kvasiniek počet plesní 31. Krmivo snetí 32. Požívatiny, suroviny 33. Požívatiny a suroviny živočíšneho 34. Požívatiny, suroviny salmonel obsah Enterobacteriaceae obsah Staphylococcus aureus, Kolagulázopozitívnych stafylokokov 35. Mlieko a mliečne výrobky Listeria 36. Požívatiny, suroviny živočíšneho a rastlinného 37. Požívatiny, suroviny živočíšneho a rastlinného 38. Požívatiny, suroviny živočíšneho a rastlinného monocytogenes Listeria monocytogenes obsah koliformných baktérií celkový počet (0,5 10) MYK 30A (5 50) MYK 30B MYK 30C MYK 30D STN ISO 7954 (MYK 30E) Návod na použitie Fosfatest Biolacta Texel Olsztyn Poľsko (5 50) 40 % Veterinárne vyšetrovacie metodiky, 1975 Veterinárne vyšetrovacie metodiky, 1975 Beladičová V. PP pri lab. diagnostike dermatomykóz zvierat 20 % mikroskopická MYK 31 Veterinárne vyšetrovacie metodiky, 1975 STN EN ISO 6579 STN ISO 7402 (HP 33) STN EN ISO (HP 34 A) STN EN ISO (HP 34 B) STN ISO (HP 35) 6 40 % STN EN ISO STN ISO 4832 (HP 37) STN EN ISO 4833 (30 300) 4 30 %
4 Strana 4/6 obsah MP ŠVS SR KTJ/ 36 % Escherichia č. 4344/99 coli (CSN ISO ) 39. Požívatiny, suroviny 40. Mlieko s predĺž. trvan. celkový počet pri 21 C 41. Požívatiny, suroviny, pitná voda obsah anaeróbnych sporulujúcich mikróbov, sulfidredukujúcich klostrídií, Clostridium perfringens 42. Konzervy obsah anaeróbnych sporulujúcich mikróbov 43. Požívatiny, suroviny živočíšneho a rastlinného obsah enterokokov 44. Ryby a produkty rybolovu Vibrio parahaemolyticus 45. Požívatiny a suroviny termotolerantných živočíšneho baktérií r.campylobacter 46. Pitná voda obsah Escherichia coli, koliformných baktérií 47. Pitná voda obsah enterokokov 48 Pitná voda obsah kultivovateľných pri 36 a 22 C 49 Požívatiny, suroviny, pitná voda obsah Pseudomonas aeruginosa 50. Povrch zariadení a plôch počet dôkaz MP ŠVS SR č. 7693/1999 (HP 40) (30 300) KTJ/ STN EN KTJ/ STN (HP 42) STN Článok 80, str. 21 (HP 43) 2 25 % 47 % 45 % STN ISO 8914 (HP 44) STN ISO membránová filtrácia membránová filtrácia 51. Mlieko obsah tuku infračervená STN EN ISO STN EN ISO (0 100) KTJ/ filter (0 100) KTJ/ filter STN EN ISO 6222 (0 300) KTJ/ filter STN EN (0 150) KTJ/ ISO/CD (HP 50) 17 % 19 % 15 % 16 % - 25 % (2,50 5,50) Riešenie sporov 52. obsah bielkovín extrakčná podľa Röse Gottlieba infračervená STN A (2,50 5,50) (2,50 4,10)
5 Strana 5/6 Rozší-rená infračervená (4,70 5,80) 53. Mlieko obsah laktózy 54. obsah sušiny infračervená vážková 55. obsah beztukovej sušiny (BTS) infračervená STN , čl. 38 STN , čl teplota tuhnutia kryoskopická STN EN ISO (NRLM 6) 57. špecifická laktodenzimetrická STN , čl. 63 hmotnosť (NRLM 8) 58. titračná kyslosť titračná podľa STN , čl. 58 Soxhlet-Henkela (NRLM 9) 59. celkový počet STN ISO 4833 (NRLM 5A) (C ) 60. Mlieko počet STN ISO 4832 koliformných (NRLM 5B) baktérií (PKB) 61. počet somatických buniek (PSB) fluorescenčná optická elektronická STN EN ISO (NRLM 4B) (10,20 14,80) (11,50 12,70) (8,00 9,70) 0,8 % 0,8 % (-0,408 0,6 % -0,600) C (1,028 1,033) 0, g/ cm 3 (6,2 7,8) 0 SH (15 300) 3 ( ) 10 3 / ml 4 10 % Riešenie sporov 62. rezíduí inhibičných látok (RIL) 63. Mlieko, mliečne výrobky antiinfekčných látok (Chloramfenikol, Sulfonamidové Tetracyklinové Aminoglykozidové Makrolidové Novobiocin, Spektinomycin, Beta-Laktámové antibiotiká mikroskopická STN EN ISO referenčná (NRLM 4A) Delvotest SP Delvotest návod na použitie (NRLM 7) CHARM II RHCL 63 (Návod na použitie - Analyzátor RIL CHARM II 6600 CHARM II System Maintenance Instructions C2MAINT3 10/18/94) 1) ( ) 10 % / ml
6 Strana 6/6 Pol 64. Látky v kvapalnom stave s hustotou od 0,8 kg.dm -3 do 1,5 kg.dm -3 (požívatiny a suroviny živočíšneho a rastlinného, zložky životného prostredia, vodné roztoky) Pevné látky s maximálnou tvrdosťou do stupňa 4 o MOHSE a sypké látky so zrnitosťou max.. 4 mm (požívatiny a suroviny, zložky životného prostredia, odpady) 1) Objemová LRR 64 ( ) 15% aktivita (STN ) Bq./ kg alebo rádionuklidov (STN IEC 61452) Bq/dm 3 vyžarujúcich (ISO 10703) žiarenie gama 11% Hmotnostná aktivita rádionuklidov vyžarujúcich žiarenie gama polovodičová gamaspektrometria v rozsahu energií fotónov (0,1 až 1,9) MeV ( ) Bq./ kg alebo Bq/ dm 3 ( ) Bq./ kg - alebo Bq/ dm 3 - Material Safety Data Sheet, Reviewed on 03/25/ Supplement: CHARM Test for Antimicrobial Drugs in Cheese, Condensed Milk, Cream, Individual Cow Milk, Powdered Milk, Flavored Milk, Whey, Pasteurized and Homogenized White Milk, Dec CHARM II Beta-lactam Test, Sequential Assay, Dec CHARM II Sulfa Drug Test for Sulfonamides at Maximum Residue Limits, Competetive Assay, July CHARM II Tetracycline Drug Test for Detection of Tetracyclines at Maximum Residue Limits, Competetive Assay, 10/98 - CHARM II Aminoglycoside Test for Gentamycin and Neomycin at U.S. Tolerance/Safe Levels(T/SL) or Maximum Residue Limits, Competetive Assay, Nov CHARM II Macrolide Test for Detection of Macrolides at U.S. Tolerance/Safe Levels( T(SLs) and Maximum Residue Limits, Sequential Assay, Aug CHARM II Aminoglycoside Test for Gentamycin, Streptomycin and Dihydrostreptomycin at Maximum Residue Limits, Competetive Assay, July CHARM II Test for Novobiocin (Competetive assay), 12/01 - CHARM II Test for Spectinomycin (Sequential Assay), 10/03 - CHARM II Test for Chloramphenicol (Sequential Assay) with Sensitivity to 0,1 ppb Chloramphenicol, Mar ) - DEBERTIN, K. - HELMER, R.G.: Gamma- and X-ray Spectrometry with Semiconductor Detectors. Elsevier Sci.Publishers, Amsterdam, 1988, 399 str. - EG&G ORTEC: Model A66-B32 ver.4.12 Gamma Vision for Windows 95/NT (Manual). Oak Ridge, 1998, 364 str. - NUCLEAR DATA: ND66/78 Multichannel Analyzer / Remote Terminal. Operator's Manual. Schaumburg, 1985, 476 str. Poznámka: rozšírená bola stanovená pre faktor pokrytia k = 2, čo zodpovedá konfidenčnej pravdepodobnosti 95 %. Petriho miska *** 8%
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